Production Method 1

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Dichloromethane ;  0 °C; 0 °C → rt; 12 h, rt

Reference

Acid- and Base-Switched Palladium-Catalyzed γ-C(sp3)-H Alkylation and Alkenylation of Neopentylamine

Zhang, Jinquan ; Zhang, Shuaizhong; Zou, Hongbin, Organic Letters, 2021, 23(9), 3466-3471

Production Method 2

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Dichloromethane ;  rt → 0 °C
1.2 Solvents: Dichloromethane ;  30 min, 0 °C; 0 °C → rt; overnight, rt

Reference

Synthesis of α,ω-heterotelechelic PVP for bioconjugation, via a one-pot orthogonal end-group modification procedure

Reader, Paul. W.; Pfukwa, Rueben; Jokonya, Simbarashe; Arnott, Gareth E.; Klumperman, Bert, Polymer Chemistry, 2016, 7(42), 6450-6456

Production Method 3

7446-81-3

937-41-7

Reaction Conditions

1.1 Reagents: (Diethylamino)sulfur trifluoride Catalysts: 4-(Dimethylamino)pyridine Solvents: Acetonitrile ;  rt; 24 h, rt

Reference

Acylation of phenols to phenolic esters with organic salts

Zhang, Zhanrong; Zhao, Ziwei; Liu, Mingyang; Liu, Huizhen; Li, Qian; et al, Green Chemistry, 2022, 24(24), 9763-9771

Production Method 4

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Dichloromethane ;  rt → 0 °C
1.2 0 °C; 1 h, 0 °C; 1 h, rt

Reference

Process for preparation of 6-hydroxy-1-indanone

, China, , ,

Production Method 5

37181-39-8

167257-54-7

937-41-7

Reaction Conditions

1.1 Reagents: Potassium fluoride ,  18-Crown-6 Solvents: Dichloromethane ;  4 h, rt

Reference

O-Arylation of carboxylic acids using (phenyl)[2-(trimethylsilyl)phenyl]iodonium triflate as a precursor of arynes

Xue, Jian; Huang, Xian, Synthetic Communications, 2007, 37(13), 2179-2185

Production Method 6

937-41-7

Reaction Conditions

1.1 Reagents: Thionyl chloride ;  rt; 1 h, heated; 20 min, reflux

Reference

Heat-resistant and salt-resistant betaine-type acrylic polymer fluid loss reducer and preparation method

, China, , ,

Production Method 7

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Potassium carbonate Solvents: Acetone ,  Water ;  4 h, 0 °C

Reference

Development of n-type semiconductor based on cyclopentene- or cyclohexene-fused [C60]-fullerene derivatives

Yamane, Yu; Sugawara, Kiyotaka; Nakamura, Naoshi; Hayase, Shuichi; Nokami, Toshiki; et al, Journal of Organic Chemistry, 2015, 80(9), 4638-4649

Production Method 8

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Dichloromethane ;  0.5 h, 0 °C; 0 °C → rt; 10 h, rt
1.2 Reagents: Water

Reference

Amine-accelerated manganese-catalyzed aromatic C-H conjugate addition to α,β-unsaturated carbonyls

Zhou, Bingwei; Ma, Pengchen; Chen, Hui; Wang, Congyang, Chemical Communications (Cambridge, 2014, 50(93), 14558-14561

Production Method 9

124654-80-4

937-41-7

Reaction Conditions

1.1 Reagents: Sodium carbonate ,  Hantzsch ester Solvents: Dimethyl sulfoxide ;  2.5 h, rt

Reference

Hantzsch Ester as a Photosensitizer for the Visible-Light-Induced Debromination of Vicinal Dibromo Compounds

Chen, Wenxin; Tao, Huachen; Huang, Wenhao; Wang, Guoqiang; Li, Shuhua; et al, Chemistry - A European Journal, 2016, 22(28), 9546-9550

Production Method 10

937-41-7

Reaction Conditions

1.1 Catalysts: Cesium carbonate ;  1 h, 25 °C

Reference

Preparation of the (meth) acrylate

, Japan, , ,

Production Method 11

625-36-5

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine ,  Phosphorus pentoxide Solvents: Toluene

Reference

Preparation of acrylate esters

, World Intellectual Property Organization, , ,

Production Method 12

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Dichloromethane ;  20 min, 0 °C; 2 h, 0 °C

Reference

Synthesis of 2-amino-3-[(3-(benzyloxy)-3-oxopropyl)thio]propanoic acid

Jin, Biao; Zhang, Jing-dong; Wang, Si-hong, Huaxue Shiji, 2018, 40(10), 1002-1004

Production Method 13

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Dichloromethane ;  0 °C; 0 °C → rt; overnight, rt

Reference

1,4-Diazabicyclo[2.2.2]octane-Promoted Aminotrifluoromethylthiolation of α,β-Unsaturated Carbonyl Compounds: N-Trifluoromethylthio-4-nitrophthalimide Acts as Both the Nitrogen and SCF3 Sources

Xiao, Qing; He, Qijie; Li, Juncheng; Wang, Jun, Organic Letters, 2015, 17(24), 6090-6093

Production Method 14

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ;  20 min, -30 °C; 2 h, -30 °C

Reference

Antimicrobial activity of p-hydroxyphenyl acrylate derivatives

Kim, Jung Hee; Park, Eun-Soo; Shim, Jae Hun; Kim, Mal-Nam; Moon, Woong-Sik; et al, Journal of Agricultural and Food Chemistry, 2004, 52(25), 7480-7483

Production Method 15

814-68-6

937-41-7

Reaction Conditions

1.1 Solvents: Pyridine

Reference

Preparation of aromatic acrylates by reaction of acryloyl chloride with phenols

Magagnini, Pier L.; Pizzirani, Giovanna, Gazzetta Chimica Italiana, 1966, 96(8-9), 1035-45

Production Method 16

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Catalysts: 4-(Dimethylamino)pyridine Solvents: Dichloromethane ;  6 h, rt
1.2 Reagents: Sodium bicarbonate

Reference

Palladium-catalyzed anti-Markovnikov oxidative acetalization of activated olefins with iron(III) sulphate as the reoxidant

Fernandes, Rodney A.; Yadav, Sandhya S.; Kumar, Praveen, Organic & Biomolecular Chemistry, 2022, 20(2), 427-443

Production Method 17

937-41-7

Reaction Conditions

1.1 Reagents: Thionyl chloride ;  rt; 1 h, heated

Reference

Synthesis and Micellar Behaviors of an Anionic Polymerizable Surfactant

Ma, Lihua; Guo, Yongjun; Feng, Rusheng; Xiang, Panpan; Li, Chunhui, Journal of the Chinese Chemical Society (Weinheim, 2014, 61(5), 583-588

Production Method 18

937-41-7

Reaction Conditions

1.1 Reagents: Di-tert-butyl dicarbonate Catalysts: Sulfuric acid magnesium salt (1:1) ,  Lithium bromide ;  24 h, 25 °C

Reference

Preparation of carboxylate esters in the presence of dicarbonates, magnesium compounds, and alkali metal compounds

, World Intellectual Property Organization, , ,

Production Method 19

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Dichloromethane ;  24 h, rt

Reference

Different reaction patterns in the Baylis-Hillman reaction of aryl aldehydes with phenyl vinyl ketone, phenyl acrylate and phenyl thioacrylate

Shi, Min; Li, Chao-Qun; Jiang, Jian-Kang, Molecules, 2002, 7(10), 721-733

Production Method 20

814-68-6

937-41-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Dichloromethane ;  0 °C; 0 °C → rt; 5 h, rt

Reference

Direct Synthesis of Adipic Esters and Adiponitrile via Photoassisted Cobalt-Catalyzed Alkene Hydrodimerization

Ren, Cheng; Ji, Guanghao; Li, Xiankai; Zhang, Jing, Chemistry - A European Journal, 2022, 28(53),

Phenyl acrylate Raw materials

• Acryloyl chloride
• Propanoic acid, 2,3-dibromo-, phenyl ester
• Phenyl[2-(trimethylsilyl)phenyl]iodonium
• 3-chloropropanoyl chloride
• Sodium acrylate

Phenyl acrylate Preparation Products

• Phenyl acrylate (937-41-7)

• 1. An amorphous carbon nitride/NiO/CoN-based composite: a highly efficient nonprecious electrode for supercapacitors and the oxygen evolution reaction?
  Huifang Yang,Haoran Guo,Peidong Fan,Xinpan Li,Wenlu Ren,Rui Song Nanoscale, 2020,12, 7024-7034
• 2. An apparatus for testing water by measurement of its electrical conductivity
  Analyst, 1912,37, 538-543
• 3. An amphipathic trans-acting phosphorothioate RNA element delivers an uncharged phosphorodiamidate morpholino sequence in mdx mouse myotubes?
  H. V. Jain,D. Verthelyi,S. L. Beaucage RSC Adv., 2017,7, 42519-42528
• 4. An analyte-triggered artificial peroxidase system based on dimanganese complex for a versatile enzyme assay?
  Suji Lee,Min Su Han Chem. Commun., 2021,57, 9450-9453
• 5. An all-solid-state imprinted polymer-based potentiometric sensor for determination of bisphenol S?
  Rongning Liang,Tanji Yin,Ruiqing Yao,Wei Qin RSC Adv., 2016,6, 73308-73312

• Solvents and Organic Chemicals Organic Compounds Benzenoids Phenol esters Phenol esters
• Solvents and Organic Chemicals Organic Compounds Benzenoids Phenol esters
• Solvents and Organic Chemicals Organic Compounds Acids/Esters

• 20069-66-3(alpha-naphthyl acrylate)
• 31263-13-5(2-Butenedioic acid(2E)-, bis(4-methoxyphenyl) ester (9CI))
• 52684-34-1(2-Propenoic acid, 2-naphthalenyl ester)
• 55673-53-5(2-Butenoic acid, phenyl ester, (2E)-)
• 6338-19-8(2-Butenedioic acid(2E)-, 1,4-diphenyl ester)
• 4513-44-4(p-methoxyphenyl acrylate)
• 35289-72-6(2-Propenoic acid,1,1'-(1,3-phenylene) ester)
• 3233-36-1(2-Propenoic acid,4-hydroxyphenyl ester)
• 50283-25-5(Catechol diacrylate)
• 6729-79-9(2-Propenoic acid,1,1'-(1,4-phenylene) ester)