Production Method 1

27784-30-1

930-29-0

Reaction Conditions

1.1 Solvents: Dichloromethane

Reference

Photochemistry of alkyl halides. 10. Vinyl halides and vinylidene dihalides

Kropp, Paul J.; McNeely, Steven A.; Davis, Robert Drummond, Journal of the American Chemical Society, 1983, 105(23), 6907-15

Production Method 2

930-29-0

Reaction Conditions

Reference

Photochemistry of alkyl halides. 3. Generation of vinyl cations

McNeely, Steven A.; Kropp, Paul J., Journal of the American Chemical Society, 1976, 98(14), 4319-20

Production Method 3

930-29-0

Reaction Conditions

Reference

Cleavage of spiran ether bonds by boron halides

Cabiddu, Salvatore; Maccioni, Antonio; Mura, Luigi; Secci, Mario, Rendiconti del Seminario della Facolta di Scienze dell'Universita di Cagliari, 1975, 45(3-4), 113-16

Production Method 4

930-29-0

Reaction Conditions

Reference

Conformation of nonaromatic ring compounds. XLI. Dipole moments and nuclear magnetic resonance spectra of 1,1,2-trihalocyclohexanes and-cyclopentanes

Buys, H. R.; Altona, Cornelis; Havinga, E., Recueil des Travaux Chimiques des Pays-Bas, 1967, 86(11), 1007-17

Production Method 5

120-92-3

930-29-0

39547-03-0

Reaction Conditions

1.1 Reagents: Triphenylphosphine

Reference

Triphenylphosphine-carbon tetrachloride

Taschner, Michael J., e-EROS Encyclopedia of Reagents for Organic Synthesis, 2001, ,

Production Method 6

14874-70-5

1204206-13-2

930-29-0

1204206-16-5

402-43-7

27415-42-5

Reaction Conditions

1.1 Solvents: 1,2-Dichloroethane ;  14 d, 20 °C

Reference

Facile Generation of a Strained Cyclic Vinyl Cation by Thermal Solvolysis of Cyclopent-1-enyl-λ3-bromanes

Miyamoto, Kazunori; Shiro, Motoo; Ochiai, Masahito, Angewandte Chemie, 2009, 48(47), 8931-8934

Production Method 7

120-92-3

930-29-0

Reaction Conditions

1.1 Reagents: Phosphorus trichloride Solvents: Heptane ;  2 h, 70 °C; 0.5 h, 70 °C; 70 °C → 0 °C
1.2 Reagents: Sodium hydroxide Solvents: Water

Reference

Synthesis of cycloalkenyl-1-boronic acid pinacol ester

, China, , ,

Production Method 8

120-92-3

930-29-0

Reaction Conditions

1.1 Reagents: Phosphorus pentachloride Solvents: Heptane ;  2 h, 70 - 74 °C; 0.5 h, 70 - 74 °C; 74 °C → 0 °C
1.2 Reagents: Sodium hydroxide Solvents: Water ;  1 h, 0 °C

Reference

Method for manufacturing cyclopentene/cyclohexene-1-pinacol borate

, China, , ,

Production Method 9

31038-06-9

930-29-0

Reaction Conditions

1.1 Reagents: Zinc Solvents: 1,4-Dioxane

Reference

Polymethylene cycles. XXXVII. Transformations of polyhalo-substituted cyclopentanes

Domnin, N.A.; Obeshchalova, N. V.; Kolinskii, R. Ch., Zhurnal Obshchei Khimii, 1961, 31, 2768-73

Production Method 10

27784-29-8

930-29-0

Reaction Conditions

1.1 Reagents: Sodium tert-butoxide Solvents: tert-Butanol

Reference

Base-induced reactions of methylenecyclobutane derivatives

Erickson, Karen L.; Markstein, Judith; Kim, Kyongtae, Journal of Organic Chemistry, 1971, 36(8), 1024-30

Production Method 11

1427188-61-1

930-29-0

Reaction Conditions

1.1 Reagents: Phosphorus pentachloride Solvents: Diethyl ether ;  0 °C → rt; 3 d, reflux

Reference

The Chemistry of a Non-Interacting Vicinal Frustrated Phosphane/Borane Lewis Pair

Elmer, Lisa-Maria; Kehr, Gerald; Daniliuc, Constantin G.; Siedow, Melanie; Eckert, Hellmut; et al, Chemistry - A European Journal, 2017, 23(25), 6056-6068

Production Method 12

120-92-3

930-29-0

Reaction Conditions

1.1 Reagents: Phosphorus pentachloride Solvents: Toluene

Reference

A photochromic prototype based on difurylperhydrocyclopentene with remarkable photoswitching behavior and in vivo application

Wang, Shangshang; Zhou, Yunyun; Zhu, Liangliang; Zhang, Junji; Zou, Qi; et al, Chemical Communications (Cambridge, 2017, 53(69), 9570-9573

Production Method 13

37722-39-7

930-29-0

Reaction Conditions

Reference

Comparison of syn dehydrohalogenations from trans-1-bromo-2-chlorocycloalkanes promoted by complex base and by potassium tert-butoxide

Croft, Alan P.; Bartsch, Richard A., Tetrahedron Letters, 1983, 24(27), 2737-40

Production Method 14

930-29-0

Reaction Conditions

Reference

Reaction of diazonium salts with transition metals. I. Arylation of olefins with arenediazonium salts catalyzed by zero valent palladium

Kikukawa, Kiyoshi; Matsuda, Tsutomu, Chemistry Letters, 1977, (2), 159-62

Production Method 15

120-92-3

930-29-0

Reaction Conditions

Reference

Molecular rearrangement. VI. Syntheses and oxotropic rearrangements in the cyclopentenyl series

Braude, E. A.; Forbes, W. F., Journal of the Chemical Society, 1951, 1755, 1755-61

Production Method 16

930-29-0

Reaction Conditions

Reference

Comparison of β-Chloro-Activated, Syn and Anti Dehydrochlorinations Induced by Complex Base

Croft, Alan P.; Bartsch, Richard A., Journal of Organic Chemistry, 1994, 59(7), 1930-2

Production Method 17

930-29-0

Reaction Conditions

Reference

Nickel(0)-catalyzed cross-coupling reactions of tricyclo[4.1.0.02,7]hept-1-ylmagnesium bromide and related Grignard reagents with aryl, vinyl, and alkynyl halides

Kottirsch, Georg; Szeimies, Guenter, Chemische Berichte, 1990, 123(7), 1495-505

Production Method 18

930-29-0

Reaction Conditions

Reference

Hydroboration. 57. Hydroboration with 9-borabicyclo[3.3.1]nonane of alkenes containing representative functional groups

Brown, Herbert C.; Chen, Jackson, Journal of Organic Chemistry, 1981, 46(20), 3978-88

Production Method 19

930-29-0

Reaction Conditions

Reference

Intermolecular additions of cyclobutylchlorocarbene

Moss, Robert A.; Fantina, Mary E.; Munjal, Ramesh C., Tetrahedron Letters, 1979, (15), 1277-80

Production Method 20

71690-88-5

930-29-0

27784-29-8

Reaction Conditions

1.1 Solvents: Chloroform-d

Reference

Competitive kinetics of 1,2-carbon and hydride shifts in cyclobutylchlorocarbene

Moss, Robert A.; Ho, Guo Jie, Tetrahedron Letters, 1990, 31(9), 1225-8

1-Chloro-1-cyclopentene Raw materials

• Cyclopentane,1,1-dichloro-
• Borate(1-),tetrafluoro-
• Cyclopentane,1-bromo-2-chloro-, cis- (9CI)
• 1-Cyclopenten-1-yl[4-(trifluoromethyl)phenyl]bromonium
• Cyclopentanone
• (Iodomethylene)cyclobutane
• rel-[(1R,2R)-2-[Bis(2,3,4,5,6-pentafluorophenyl)boryl]cyclopentyl]bis(2,4,6-trimethylphenyl)phosphine
• 3H-DIAZIRINE, 3-CHLORO-3-CYCLOBUTYL-
• (Chloromethylene)cyclobutane

1-Chloro-1-cyclopentene Preparation Products

• Cyclopentane, (dichloromethylene)- (39547-03-0)
• Benzene, 1-bromo-2-(1-cyclopenten-1-yl)-4-(trifluoromethyl)- (1204206-16-5)
• 1-bromo-4-(trifluoromethyl)benzene (402-43-7)
• Cyclopentene, 1-fluoro- (27415-42-5)
• 1-Chloro-1-cyclopentene (930-29-0)
• (Chloromethylene)cyclobutane (27784-29-8)

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