Production Method 1

535-11-5

871-22-7

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Methanol ,  Benzene

Reference

Additions of electrophilic radicals of electron rich alkenes by the atom transfer method. Surmounting potentially reversible radical atom transfer reactions by irreversible ionic reactions

Curran, Dennis P.; et al, Tetrahedron Letters, 1998, 39(37), 6629-6632

Production Method 2

871-22-7

Reaction Conditions

1.1 Reagents: Hydrochloric acid
2.1 -

Reference

Condensation of α-chloroethyl butyl ether with benzene in the presence of protic and aprotic acids

Ermokhina, V. A.; et al, Sbornik Nauchnykh Trudov - Tashkentskii Gosudarstvennyi Universitet im. V. I. Lenina, 1980, 622, 11-15

Production Method 3

871-22-7

Reaction Conditions

Reference

Product class 6: acyclic and semicyclic O/O acetals

von Angerer, S.; et al, Science of Synthesis, 2007, 29, 303-406

Production Method 4

871-22-7

Reaction Conditions

1.1 Catalysts: Amberlyst 15 ;  5 mbar, 70 °C

Reference

Green Fuel Production Using the PermSMBR Technology

Pereira, Carla S. M.; et al, Industrial & Engineering Chemistry Research, 2012, 51(26), 8928-8938

Production Method 5

871-22-7

Reaction Conditions

1.1 Reagents: Hydrochloric acid

Reference

Synthesis of vinyl butyl acetal of dimethylethynylcarbinol

Kirilyus, I. V.; et al, Teor. Osnovy Pererab. Mineral'n. i Organ. Syr'ya., 1977, (4), 91-6

Production Method 6

871-22-7

Reaction Conditions

1.1 Catalysts: Hydrochloric acid Solvents: Water ;  40 min, 100 °C

Reference

Simultaneous determination of aliphatic acids and aldehydes in aqueous media by reaction gas chromatography

Pervova, M. G.; et al, Journal of Analytical Chemistry, 2016, 71(10), 1041-1045

Production Method 7

871-22-7

Reaction Conditions

1.1 Reagents: Hydroxyamine hydrochloride Solvents: Toluene
2.1 Reagents: Zinc chloride Solvents: Benzene

Reference

Reaction of aliphatic aldoximes and ketoximes with alkoxyethenes

Voronkov, M. G.; et al, Zhurnal Organicheskoi Khimii, 1987, 23(1), 57-60

Production Method 8

871-22-7

876-02-8

13679-43-1

13678-74-5

1197-40-6

19277-56-6

3658-95-5

539-88-8

542-52-9

5921-80-2

1492053-22-1

699-17-2

583-33-5

Reaction Conditions

1.1 Solvents: 1-Butanol ;  48 h, 140 °C

Reference

Production of biomass-derived furanic ethers and levulinate esters using heterogeneous acid catalysts

Neves, Patricia; et al, Green Chemistry, 2013, 15(12), 3367-3376

Production Method 9

1066-54-2

871-22-7

Reaction Conditions

1.1 Catalysts: Gold(1+), (acetonitrile)[bis(1,1-dimethylethyl)[2′,4′,6′-tris(1-methylethyl)[1,1… Solvents: Dichloromethane ;  5 h, 50 °C

Reference

Synthesis, Structure, Reactivity and Catalytic Implications of a Cationic, Acetylide-Bridged Trigold-JohnPhos Species

Grirrane, Abdessamad ; et al, Chemistry - A European Journal, 2020, 26(40), 8810-8818

Production Method 10

871-22-7

Reaction Conditions

1.1 Reagents: 1-Butanol Catalysts: Lithium bromide ,  Lithium bis(trifluoromethanesulfonyl)imide Solvents: 1,2-Dimethoxyethane
1.2 Reagents: Dibutylamine

Reference

Catalysis of electrophilic addition of alcohols to alkoxyalkenes by lithium salts

Trofimov, B. A.; et al, Russian Journal of General Chemistry (Translation of Zhurnal Obshchei Khimii), 2001, 71(2), 319-320

Production Method 11

871-22-7

Reaction Conditions

1.1 Reagents: Boron trifluoride etherate ,  Mercuric oxide

Reference

Preparation of acetals or ketals from vinyl-type esters

Croxall, W. J.; et al, Journal of the American Chemical Society, 1948, 70, 2805-7

Production Method 12

3450-47-3

871-22-7

Reaction Conditions

Reference

Condensation of α-chloroethyl butyl ether with benzene in the presence of protic and aprotic acids

Ermokhina, V. A.; et al, Sbornik Nauchnykh Trudov - Tashkentskii Gosudarstvennyi Universitet im. V. I. Lenina, 1980, 622, 11-15

Production Method 13

871-22-7

Reaction Conditions

Reference

Preparation of acetals by the action of alcohols on a vinyl ether in the presence of cation-exchange resins

Mastagli, Pierre; et al, Bulletin de la Societe Chimique de France, 1957, 764, 764-6

Production Method 14

871-22-7

Reaction Conditions

Reference

Role of hydrogen chloride in reactions of three-coordinate phosphorus chlorides with acetals

Gazizov, M. B.; et al, Zhurnal Obshchei Khimii, 1984, 54(5),

Production Method 15

871-22-7

Reaction Conditions

1.1 Catalysts: Trifluoroacetic acid

Reference

Reaction of hemiacetal esters, acetals, and acylals with alcohols or acetic acid

Gallucci, R. R.; et al, Journal of Organic Chemistry, 1982, 47(18), 3517-21

Production Method 16

871-22-7

Reaction Conditions

1.1 Reagents: Water Catalysts: Chloroplatinic acid

Reference

Acetal formation from alcohols and acetylene with platinum and palladium compounds as catalysts

Steinborn, Dirk; et al, Journal of Organometallic Chemistry, 1991, 414(2),

Production Method 17

693-03-8

871-22-7

101581-41-3

Reaction Conditions

Reference

Reaction of exchange of hydroxyl radicals for hydrocarbon radicals of organomagnesium compounds. IV. Reaction of Grignard reagent with acylals

Shostakovskii, M. F.; et al, Zhurnal Obshchei Khimii, 1958, 28, 2339-41

Production Method 18

871-22-7

Reaction Conditions

1.1 Reagents: Zinc chloride Solvents: Benzene

Reference

Reaction of aliphatic aldoximes and ketoximes with alkoxyethenes

Voronkov, M. G.; et al, Zhurnal Organicheskoi Khimii, 1987, 23(1), 57-60

Production Method 19

871-22-7

588-43-2

Reaction Conditions

1.1 Reagents: Benzoyl peroxide Solvents: Cyclohexane

Reference

Preparation of 1-phenylcyclohexa-2,5-diene-1-carboxylates and their use in free-radical mediated syntheses

Baguley, Paul A.; et al, Journal of the Chemical Society, 2002, (3), 304-309

Production Method 20

871-22-7

Reaction Conditions

Reference

O-Methyl N-[2-(vinyloxy)ethyl]carbamate in reactions with alcohols

Nedolya, N. A.; et al, Zhurnal Organicheskoi Khimii, 1994, 30(4), 507-11

Production Method 21

871-22-7

Reaction Conditions

1.1 Reagents: Hydroxyamine hydrochloride Solvents: Toluene
2.1 Reagents: Zinc chloride Solvents: Benzene

Reference

Reaction of aliphatic aldoximes and ketoximes with alkoxyethenes

Voronkov, M. G.; et al, Zhurnal Organicheskoi Khimii, 1987, 23(1), 57-60

Production Method 22

4794-05-2

871-22-7

588-43-2

Reaction Conditions

1.1 Reagents: Butyllithium Solvents: Tetrahydrofuran
1.2 -
1.3 Reagents: Hydrochloric acid Solvents: Water
2.1 Reagents: Benzoyl peroxide Solvents: Cyclohexane

Reference

Preparation of 1-phenylcyclohexa-2,5-diene-1-carboxylates and their use in free-radical mediated syntheses

Baguley, Paul A.; et al, Journal of the Chemical Society, 2002, (3), 304-309

Production Method 23

871-22-7

Reaction Conditions

1.1 Reagents: Trifluoroacetic acid
2.1 -

Reference

O-Methyl N-[2-(vinyloxy)ethyl]carbamate in reactions with alcohols

Nedolya, N. A.; et al, Zhurnal Organicheskoi Khimii, 1994, 30(4), 507-11

1,1'-Ethylidenebis(oxy)bisbutane Raw materials

• N-Butylmagnesium Bromide
• 1-(1-chloroethoxy)butane
• Cyclohexa-2,5-dien-1-ylbenzene
• ethynyltrimethylsilane
• ethyl 2-bromopropanoate

1,1'-Ethylidenebis(oxy)bisbutane Preparation Products

• 4'-Hydroxy-3'-methylacetophenone (876-02-8)
• tributyl orthoformate (588-43-2)
• Furan, 2,2'-methylenebis[5-methyl- (13679-43-1)
• 1-(5-methylfuran-2-yl)propan-2-one (13678-74-5)
• Furan,2,2'-methylenebis- (1197-40-6)
• Benzoic acid,4-methyl-, butyl ester (19277-56-6)
• 1,1-diethoxybutane (3658-95-5)
• Ethyl levulinate (539-88-8)
• Dibutyl carbonate (542-52-9)
• 1,1-Dibutoxybutane (5921-80-2)
• Hexane, 2-butoxy- (101581-41-3)
• 2-Pentanone, 5,5-dibutoxy- (1492053-22-1)
• 1,1'-Ethylidenebis(oxy)bisbutane (871-22-7)
• 4-(furan-2-yl)butan-2-one (699-17-2)
• Butyl 2-furoate (583-33-5)

• 1. Excitable dynamics in the bromate–sulfite–ferrocyanide reaction
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• 2. Establishing the accuracy of position-specific carbon isotope analysis of propane by GC-pyrolysis-GC-IRMS
  ChangjieLiu,PengLiu,XiaofengWang,XiaoqiangLi,JuskeHorita
• 3. Empowering microfluidics by micro-3D printing and solution-based mineral coating?
  Hongxia Li,Aikifa Raza,Qiaoyu Ge,Jin-You Lu,TieJun Zhang Soft Matter, 2020,16, 6841-6849
• 4. Dissolution of cork biopolymers in biocompatible ionic liquids
  Helga Garcia,Rui Ferreira,Marija Petkovic,Jamie L. Ferguson,Maria C. Leit?o,H. Q. Nimal Gunaratne,Luís Paulo N. Rebelo Green Chem., 2010,12, 367-369
• 5. Enabling non-flammable Li-metal batteries via electrolyte functionalization and interface engineering?
  Jing Yu,Yu-Qi Lyu,Jiapeng Liu,Mohammed B. Effat,Junxiong Wu J. Mater. Chem. A, 2019,7, 17995-18002

• Solvents and Organic Chemicals Organic Compounds Organic oxygen compounds Organooxygen compounds Acetals
• Solvents and Organic Chemicals Organic Compounds Organic oxygen compounds Organooxygen compounds Ethers Acetals

• 93941-00-5(Octane,1,1'-[ethylidenebis(oxy)]bis- (9CI))
• 3658-95-5(1,1-diethoxybutane)
• 5405-58-3(ethylidenebis(oxy)dihexane)
• 5921-80-2(1,1-Dibutoxybutane)
• 4469-25-4(1,3-Dioxepane,2-methyl-)
• 13442-89-2(Pentane,1-(1-ethoxyethoxy)-)
• 36693-23-9(Octadecane,1-[1-(octadecyloxy)ethoxy]-)
• 13002-10-3(Butane,1,1'-[propylidenebis(oxy)]bis-)
• 13002-08-9(Pentane,1,1'-[ethylidenebis(oxy)]bis-)
• 54484-73-0(Hexane,1-(1-ethoxyethoxy)-)