Production Method 1

74137-36-3

849062-12-0

1050424-08-2

Reaction Conditions

1.1 Reagents: Butyllithium Solvents: Diethyl ether ,  Hexane ;  30 min, -70 °C
1.2 Reagents: Triisopropyl borate ;  30 min, -70 °C
1.3 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  30 min, -15 °C
1.4 -15 °C → rt
1.5 Reagents: Sulfuric acid Solvents: Water ;  rt

Reference

One-pot generation of lithium (lithiophenyl)trialkoxyborates from substituted dihalobenzenes (Hal = Br, I) and their derivatization with electrophiles

Kurach, Pawel; Lulinski, Sergiusz; Serwatowski, Janusz, European Journal of Organic Chemistry, 2008, (18), 3171-3178

(3-bromo-5-methoxyphenyl)boronic acid Raw materials

• 1,3-dibromo-5-methoxybenzene

(3-bromo-5-methoxyphenyl)boronic acid Preparation Products

• (3-bromo-5-methoxyphenyl)boronic acid (849062-12-0)
• 3-Carboxy-5-methoxyphenylboronic Acid (1050424-08-2)

• 1. An assay for the enzyme N-acetyl-β-d-glucosaminidase (NAGase) based on electrochemical detection using screen-printed carbon electrodes (SPCEs)
  R. M. Pemberton,J. P. Hart,T. T. Mottram Analyst, 2001,126, 1866-1871
• 2. An approach to 7-aza-1-phosphanorbornane complexes: strain promoted rearrangement of 1-iminylphosphirane complexes and cycloaddition with olefins?
  Yang Xu,Min Wang,Donghui Wei,Rongqiang Tian,Zheng Duan,Fran?ois Mathey Dalton Trans., 2019,48, 5523-5526
• 3. An alumina stabilized graphene oxide wrapped SnO2 hollow sphere LIB anode with improved lithium storage?
  Xiang Liu,Qian Sun,A. B. Djuri?i?,Maohai Xie,Baohu Dai,Jinyao Tang,Charles Surya,Changzhong Liao,Kaimin Shih RSC Adv., 2015,5, 100783-100789
• 4. Aggregation of biologically important peptides and proteins: inhibition or acceleration depending on protein and metal ion concentrations
  Benjamin Gabriel Poulson,Kacper Szczepski,Joanna Izabela Lachowicz,Lukasz Jaremko,Abdul-Hamid Emwas,Mariusz Jaremko RSC Adv., 2020,10, 215-227
• 5. An atomic scale study of defects in Co2FeAl
  Ravi Kumar Yadav,R. Govindaraj Phys. Chem. Chem. Phys., 2020,22, 26876-26886

• Other Chemical Reagents Derivatization Reagents
• Solvents and Organic Chemicals Organic Compounds Acids/Esters

• 871126-27-1(3-Bromo-5-propoxyphenylboronic acid)
• 849062-02-8(5-Bromo-3-ethoxyphenylboronic acid)
• 89598-97-0(5-Bromo-2-hydroxyphenylboronic acid)
• 89694-45-1(5-Bromo-2-methoxyphenylboronic acid)
• 1256345-59-1(4-bromo-3-methoxyphenylboronic acid)
• 1072951-48-4(3-Bromo-5-(trifluoromethoxy)phenylboronic acid)
• 89694-44-0(2-Bromo-5-methoxyphenylboronic acid)
• 871125-81-4([3-bromo-5-(propan-2-yloxy)phenyl]boronic acid)
• 352525-82-7(5-Bromo-2-ethoxyphenylboronic acid)
• 889849-21-2((4-Bromo-2-methoxyphenyl)boronic acid)