Production Method 1

892593-13-4

109-04-6

56-81-5

53258-94-9

91-79-2

1453-90-3

Reaction Conditions

1.1 Reagents: Potassium tert-butoxide ,  Oxygen Catalysts: Cuprous iodide Solvents: Choline chloride ;  12 h, 80 °C; 80 °C → 25 °C
1.2 Reagents: Sodium hydroxide Solvents: Water ;  10 min, 25 °C

Reference

Sustainable and Scalable Two-Step Synthesis of Thenfadil and Some Analogs in Deep Eutectic Solvents: From Laboratory to Industry

Quivelli, Andrea Francesca; Rossi, Federico Vittorio; Vitale, Paola; Garcia-Alvarez, Joaquin; Perna, Filippo Maria ; et al, ACS Sustainable Chemistry & Engineering, 2022, 10(13), 4065-4072

Pyridine, 2,2'-oxybis- Raw materials

• N,N-Dimethyl-N'-(3-thienylmethyl)-1,2-ethanediamine dihydrochloride
• 2-Bromopyridine
• Glycerol

Pyridine, 2,2'-oxybis- Preparation Products

• N-2-(dimethylamino)ethyl-N-(thiophen-3-yl)methylpyridin-2-amine (91-79-2)
• Pyridine, 2,2'-oxybis- (53258-94-9)
• 1,2-Propanediol, 3-(2-pyridinyloxy)- (1453-90-3)

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