Production Method 1

348-57-2

3132-92-1

804498-72-4

Reaction Conditions

1.1 Reagents: Magnesium Solvents: Tetrahydrofuran ;  rt → 60 °C
1.2 Catalysts: Iodine Solvents: Tetrahydrofuran ;  30 min, reflux; 15 h, 65 °C; 65 °C → rt
1.3 Reagents: Water ;  rt
2.1 Reagents: Boron trifluoride etherate Solvents: Dichloromethane ;  0 °C; 30 min, 0 °C; 0 °C → rt; 2 h, rt

Reference

Structural Modifications of Nile Red Carbon Monoxide Fluorescent Probe: Sensing Mechanism and Applications

Madea, Dominik; et al, Journal of Organic Chemistry, 2020, 85(5), 3473-3489

Production Method 2

173276-82-9

3132-92-1

804498-72-4

Reaction Conditions

1.1 Reagents: Boron trifluoride etherate Solvents: Dichloromethane ;  1.5 h, 0 °C → rt

Reference

Synthesis of monofluorinated 1-(naphthalen-1-yl)piperazines

Repine, Joseph T.; et al, Tetrahedron Letters, 2007, 48(31), 5539-5541

Production Method 3

173276-82-9

3132-92-1

804498-72-4

Reaction Conditions

1.1 Reagents: Boron trifluoride etherate Solvents: Dichloromethane ;  0 °C; 30 min, 0 °C; 0 °C → rt; 2 h, rt

Reference

Structural Modifications of Nile Red Carbon Monoxide Fluorescent Probe: Sensing Mechanism and Applications

Madea, Dominik; et al, Journal of Organic Chemistry, 2020, 85(5), 3473-3489

Production Method 4

348-57-2

3132-92-1

804498-72-4

Reaction Conditions

1.1 Reagents: Magnesium Solvents: Tetrahydrofuran ;  2 h, 65 °C; 15 h, 65 °C
2.1 Reagents: Hydrochloric acid Solvents: Ethanol ;  2 h, reflux

Reference

Synthesis of monofluorinated 1-(naphthalen-1-yl)piperazines

Repine, Joseph T.; et al, Tetrahedron Letters, 2007, 48(31), 5539-5541

7-Fluoronaphthalen-1-ol Raw materials

• 1-Bromo-2,4-difluorobenzene
• 1,4-Epoxynaphthalene,6-fluoro-1,4-dihydro-

7-Fluoronaphthalen-1-ol Preparation Products

• 6-Fluoronaphthalen-1-ol (804498-72-4)
• 7-Fluoronaphthalen-1-ol (3132-92-1)

• 1. Essential effect of the electrolyte on the mechanical and chemical degradation of LiNi0.8Co0.15Al0.05O2 cathodes upon long-term cycling??
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• 3. Dissociative electron attachment to HGaF4 Lewis–Br?nsted superacid
  Marcin Czapla,Jack Simons Phys. Chem. Chem. Phys., 2018,20, 21739-21745
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• 5. Fate of single walled carbon nanotubes in wetland ecosystems?
  Joseph H. Bisesi,Tara Sabo-Attwood Environ. Sci.: Nano, 2014,1, 574-583

• Solvents and Organic Chemicals Organic Compounds Benzenoids Naphthalenes Naphthols and derivatives

• 56874-95-4(2-FLUORO-1-NAPHTHOL)
• 13916-98-8(8-Fluoronaphthalen-2-OL)
• 13101-83-2(2-Naphthalenol,6-fluoro-)
• 61761-32-8(5-Fluoronaphthalen-1-ol)
• 383155-01-9(1-Naphthalenol,8-fluoro-(9CI))
• 371-41-5(4-Fluorophenol)
• 62576-77-6(Phenol, 4-fluoro-, compd. with benzene (1:1))
• 8068-44-8(6-Fluoronaphthalen-1-ol)
• 741693-88-9(5-Fluoro-2-naphthalenol)
• 315-53-7(4-Fluoro-1-naphthalenol)