Production Method 1

97294-78-5

Reaction Conditions

Reference

Preparation of triazine derivatives as herbicides

, Japan, , ,

Production Method 2

39151-19-4

97294-78-5

Reaction Conditions

1.1 Reagents: Formic acid ,  Formamide Solvents: Formamide ;  20 h, 170 °C; 170 °C → rt
1.2 Reagents: Hydrochloric acid Solvents: Water ;  rt → reflux; 30 h, reflux; cooled

Reference

Preparation of piperazinylarylamines as 5-HT6 modulators

, World Intellectual Property Organization, , ,

Production Method 3

39151-19-4

97294-78-5

Reaction Conditions

1.1 Reagents: Sodium acetate ,  O-Methylhydroxylamine hydrochloride Solvents: Ethanol ,  Water ;  3 h, 70 °C
1.2 Reagents: (T-4)-Trihydro(tetrahydrofuran)boron Solvents: Tetrahydrofuran ;  10 min, rt; 2.5 h, 70 °C; 70 °C → rt
1.3 Reagents: Hydrochloric acid Solvents: Diethyl ether ;  rt; 1 h, 40 °C

Reference

Preparation of 5-benzylisoquinoline derivatives as ROCK kinase for the treatment of cardiovascular diseases

, France, , ,

Production Method 4

97294-77-4

97294-78-5

Reaction Conditions

1.1 Reagents: Hydrogen Catalysts: Palladium Solvents: Methanol ,  Hydrochloric acid

Reference

Synthesis and activity of 5-(aminomethyl)-1,3-cyclohexanediones: enolic analogs of γ-aminobutyric acid

Mann, Andre; Humblet, Christine; Chambon, Jean Pierre; Schlichter, Remy; Desarmenien, Michel; et al, Journal of Medicinal Chemistry, 1985, 28(10), 1440-6

1-(3,5-dimethoxyphenyl)ethan-1-amine Raw materials

• 3′,5′-Dimethoxyacetophenone
• 3,5-Dimethoxyacetophenone oxime

1-(3,5-dimethoxyphenyl)ethan-1-amine Preparation Products

• 1-(3,5-dimethoxyphenyl)ethan-1-amine (97294-78-5)

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• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Dimethoxybenzenes
• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Methoxybenzenes Dimethoxybenzenes

• 14692-29-6(Strontium acetate hemihydrate)
• 6298-96-0(1-(4-Methoxyphenyl)ethanamine)
• 62409-13-6(1-(3-Methoxyphenyl)ethanamine)
• 752924-21-3(3-Methoxybenzhydrylamine)
• 19293-62-0(4,4'-Dimethoxybenzhydrylamine)
• 332062-08-5(Fmoc-S-3-amino-4,4-diphenyl-butyric acid)
• 1270529-38-8(1,2,3,4,5,6-Hexahydro-[2,3]bipyridinyl-6-ol)
• 2680771-01-9(4-cyclopentyl-3-{(prop-2-en-1-yloxy)carbonylamino}butanoic acid)
• 2098070-20-1(2-(3-(Pyridin-3-yl)-1H-pyrazol-1-yl)acetimidamide)
• 1444113-98-7(N-(3-cyanothiolan-3-yl)-2-[(2,2,2-trifluoroethyl)sulfanyl]pyridine-4-carboxamide)