- Method for preparing high-purity 2-chloro-3-aminopyridine hydrochloride, China, , ,
Cas no 94770-75-9 (2-Chloro-pyridin-3-yl-amine Hydrochloride)
94770-75-9 structure
Product Name:2-Chloro-pyridin-3-yl-amine Hydrochloride
CAS No:94770-75-9
MF:C5H6Cl2N2
MW:165.020538806915
MDL:MFCD04114114
CID:803490
PubChem ID:101548
Update Time:2024-03-01
2-Chloro-pyridin-3-yl-amine Hydrochloride Chemical and Physical Properties
Names and Identifiers
-
- 2-Chloropyridin-3-amine hydrochloride
- 2-Chloro-3-pyridinamine hydrochloride
- 3-AMINO-2-CHLOROPYRIDINE
- 3-Pyridinamine,2-chloro-, hydrochloride (1:1)
- 2-CHLORO-3-AMINOPYRIDINE
- 2-CHLORO-3-PYRIDYLAMINE
- 2-CHLORO-B-PYRIDYLAMINE
- 2-CHLOROPYRIDIN-3-AMINE
- 2-CHLORO-PYRIDIN-3-YLAMINE
- 2-CHLORO-PYRIDIN-3-YL-AMINE HCL
- 3-AMINOCHLOROPYRIDINE
- 3-Pyridinamine, 2-chloro-, monohydrochloride (9CI)
- 2-Chloro-pyridin-3-ylamine hydrochloride
- 2-Chloro-pyridin-3-yl-amine Hydrochloride
-
- MDL： MFCD04114114
- Inchi： 1S/C5H5ClN2.ClH/c6-5-4(7)2-1-3-8-5;/h1-3H,7H2;1H
- InChI Key： NEQIRASUEZEXJF-UHFFFAOYSA-N
- SMILES： Cl.ClC1C(N)=CC=CN=1
Computed Properties
- Exact Mass: 163.99100
- Monoisotopic Mass: 418.30830982g/mol
- Isotope Atom Count: 0
- Hydrogen Bond Donor Count: 0
- Hydrogen Bond Acceptor Count: 4
- Heavy Atom Count: 30
- Rotatable Bond Count: 18
- Complexity: 460
- Covalently-Bonded Unit Count: 1
- Defined Atom Stereocenter Count: 0
- Undefined Atom Stereocenter Count : 1
- Defined Bond Stereocenter Count: 0
- Undefined Bond Stereocenter Count: 0
- XLogP3: 9
- Topological Polar Surface Area: 52.6?2
Experimental Properties
- Melting Point: 76-78?°C(lit.)
- PSA: 38.91000
- LogP: 2.70040
2-Chloro-pyridin-3-yl-amine Hydrochloride Security Information
- Signal Word：warning
- Hazard Statement： H303+H313+H333
- Warning Statement： P264+P280+P305+P351+P338+P337+P313
- Hazardous Material transportation number：UN 2811 6.1/PG 1
- WGK Germany：3
- Hazard Category Code： 36/37/38
- Safety Instruction： 26-36
-
Hazardous Material Identification：
- Storage Condition：storage at -4℃ (1-2weeks), longer storage period at -20℃ (1-2years)
2-Chloro-pyridin-3-yl-amine Hydrochloride Customs Data
- HS CODE：2933399090
- Customs Data：
China Customs Code:
2933399090Overview:
2933399090. Other compounds with non fused pyridine rings in structure. VAT:17.0%. Tax refund rate:13.0%. Regulatory conditions:nothing. MFN tariff:6.5%. general tariff:20.0%
Declaration elements:
Product Name, component content, use to, Please indicate the appearance of Urotropine, 6- caprolactam please indicate the appearance, Signing date
Summary:
2933399090. other compounds containing an unfused pyridine ring (whether or not hydrogenated) in the structure. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0%
2-Chloro-pyridin-3-yl-amine Hydrochloride Pricemore >>
| Related Categories | No. | Product Name | Cas No. | Purity | Specification | Price | update time | Inquiry |
|---|---|---|---|---|---|---|---|---|
| TRC | C429343-10mg |
2-Chloro-pyridin-3-yl-amine Hydrochloride |
94770-75-9 | 10mg |
$ 50.00 | 2022-06-06 | ||
| TRC | C429343-50mg |
2-Chloro-pyridin-3-yl-amine Hydrochloride |
94770-75-9 | 50mg |
$ 65.00 | 2022-06-06 | ||
| TRC | C429343-100mg |
2-Chloro-pyridin-3-yl-amine Hydrochloride |
94770-75-9 | 100mg |
$ 80.00 | 2022-06-06 | ||
| JIE DA WEI （ SHANG HAI ） YI YAO KE JI FA ZHAN Co., Ltd. | 69R0118S-100g |
2-Chloro-pyridin-3-ylamine hydrochloride |
94770-75-9 | 96% | 100g |
296.81CNY | 2021-05-08 | |
| JIE DA WEI （ SHANG HAI ） YI YAO KE JI FA ZHAN Co., Ltd. | 69R0118S-500g |
2-Chloro-pyridin-3-ylamine hydrochloride |
94770-75-9 | 96% | 500g |
1187.26CNY | 2021-05-08 | |
| JIE DA WEI （ SHANG HAI ） YI YAO KE JI FA ZHAN Co., Ltd. | 69R0118S-100g |
2-Chloro-pyridin-3-ylamine hydrochloride |
94770-75-9 | 96% | 100g |
￥306.04 | 2025-04-11 | |
| JIE DA WEI （ SHANG HAI ） YI YAO KE JI FA ZHAN Co., Ltd. | 69R0118S-500g |
2-Chloro-pyridin-3-ylamine hydrochloride |
94770-75-9 | 96% | 500g |
￥1224.15 | 2025-04-11 | |
| eNovation Chemicals LLC | Y1131699-500g |
2-Chloro-pyridin-3-ylamine hydrochloride |
94770-75-9 | 96% | 500g |
$220 | 2022-11-01 | |
| SHANG HAI HAO HONG Biomedical Technology Co., Ltd. | 1538028-100g |
2-Chloropyridin-3-amine hydrochloride |
94770-75-9 | 98% | 100g |
￥444.00 | 2024-04-24 | |
| SHANG HAI HAO HONG Biomedical Technology Co., Ltd. | 1538028-500g |
2-Chloropyridin-3-amine hydrochloride |
94770-75-9 | 98% | 500g |
￥1424.00 | 2024-04-24 |
2-Chloro-pyridin-3-yl-amine Hydrochloride Production Method
Production Method 1
Reaction Conditions
1.1 Reagents: Hydrochloric acid , Hydrogen peroxide Solvents: Water ; 0 - 5 °C; 3 h, 15 - 20 °C
1.2 Reagents: Sodium sulfite Solvents: Water
1.3 Reagents: Sodium hydroxide Solvents: Water ; pH 4 - 5, < 40 °C
1.4 Reagents: Hydrochloric acid Solvents: Ethyl acetate ; pH 1 - 2, 40 °C → 85 °C; 2 h, 80 - 85 °C
1.2 Reagents: Sodium sulfite Solvents: Water
1.3 Reagents: Sodium hydroxide Solvents: Water ; pH 4 - 5, < 40 °C
1.4 Reagents: Hydrochloric acid Solvents: Ethyl acetate ; pH 1 - 2, 40 °C → 85 °C; 2 h, 80 - 85 °C
Reference
Production Method 2
Reaction Conditions
1.1 Reagents: Hydrochloric acid , Chlorine Solvents: Water ; 45 s, 30 °C
Reference
- Green preparation of 2-chloro-3-aminopyridine and its hydrochloride, China, , ,
2-Chloro-pyridin-3-yl-amine Hydrochloride Raw materials
2-Chloro-pyridin-3-yl-amine Hydrochloride Preparation Products
2-Chloro-pyridin-3-yl-amine Hydrochloride Suppliers
Amadis Chemical Company Limited
Gold Member
Audited Supplier
(CAS:94770-75-9)2-Chloro-pyridin-3-yl-amine Hydrochloride
Order Number:A1046129
Stock Status:in Stock
Quantity:500g
Purity:99%
Pricing Information Last Updated:Thursday, 29 August 2024 17:21
Price ($):153.0
Email:[email protected]
Suzhou Senfeida Chemical Co., Ltd
Gold Member
Audited Supplier
(CAS:94770-75-9)3-AMINO-2-CHLOROPYRIDINE
Order Number:sfd14944
Stock Status:in Stock
Quantity:200KG
Purity:99%
Pricing Information Last Updated:Friday, 19 July 2024 14:37
Price ($):discuss personally
Email:[email protected]
Jiangsu Xinsu New Materials Co., Ltd
Gold Member
Audited Supplier
(CAS:94770-75-9)
Order Number:SFD1119
Stock Status:in Stock
Quantity:25KG,200KG,1000KG
Purity:99%
Pricing Information Last Updated:Wednesday, 11 December 2024 17:02
Price ($):
Email:[email protected]
2-Chloro-pyridin-3-yl-amine Hydrochloride Related Literature
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Christopher J. Harrison,Kyle J. Berean,Enrico Della Gaspera,Jian Zhen Ou,Richard B. Kaner,Kourosh Kalantar-zadeh,Torben Daeneke Nanoscale, 2016,8, 16276-16283
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Eléonore Resongles,Corinne Casiot,Fran?oise Elbaz-Poulichet,Rémi Freydier,Odile Bruneel,Christine Piot,Sophie Delpoux,Aurélie Volant,Angélique Desoeuvre Environ. Sci.: Processes Impacts, 2013,15, 1536-1544
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Gaurav J. Shah,Eric P.-Y. Chiou,Ming C. Wu,Chang-Jin “CJ” Kim Lab Chip, 2009,9, 1732-1739
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Tao Wang,Yangyang Liu,Yue Deng,Hongbo Fu,Jianmin Chen Environ. Sci.: Nano, 2018,5, 1821-1833
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