Production Method 1

134-84-9

94341-55-6

Reaction Conditions

1.1 Reagents: Ammonia Solvents: Methanol ,  Tetrahydrofuran ;  -33 °C

Reference

Parallel synthesis of DAPT derivatives and their γ-secretase-inhibitory activity

Kan, Toshiyuki; Tominari, Yusuke; Rikimaru, Kentaro; Morohashi, Yuichi; Natsugari, Hideaki; et al, Bioorganic & Medicinal Chemistry Letters, 2004, 14(8), 1983-1985

Production Method 2

94341-52-3

94341-55-6

Reaction Conditions

1.1 Reagents: Triphenylphosphine Solvents: Tetrahydrofuran ,  Water ;  1 h, rt → 60 °C

Reference

Ugi reaction-assisted rapid assembly of affinity-based probes against potential protein tyrosine phosphatases

Ge, Jingyan; Cheng, Xiamin; Tan, Lay Pheng; Yao, Shao Q., Chemical Communications (Cambridge, 2012, 48(37), 4453-4455

Production Method 3

24095-40-7

94341-55-6

Reaction Conditions

1.1 Reagents: Potassium carbonate Solvents: Dichloromethane ,  Water ;  20 min, 1 mbar, 35 °C

Reference

Synthesis of photoactivable oligosaccharide derivatives from 1,2-cyclic carbamate building blocks and study of their interaction with carbohydrate-binding proteins

Podvalnyy, Nikita M. ; Chesnov, Serge; Nanni, Paolo; Gut, Melanie ; Holland, Jason P. ; et al, Carbohydrate Research, 2021, 508,

Production Method 4

94341-52-3

94341-55-6

Reaction Conditions

1.1 Reagents: Triphenylphosphine ,  Water

Reference

Preparation of an antibacterial hydrophilic compounds for fixation to fabrics, plastic, rubber or other materials without damaging mechanical properties of raw materials

, United States, , ,

Production Method 5

94341-52-3

94341-55-6

Reaction Conditions

1.1 Reagents: Triphenylphosphine Solvents: Water

Reference

Antistatic compound, surface treatment method thereof, material, and modified material

, China, , ,

Production Method 6

94341-52-3

94341-55-6

Reaction Conditions

1.1 Reagents: Triphenylphosphine ,  Water

Reference

Preparation of antibacterial hydrophilic compounds useful for polymer material modification

, China, , ,

Production Method 7

94341-52-3

94341-55-6

Reaction Conditions

1.1 Reagents: Triphenylphosphine Solvents: Methanol ,  Water ;  18 h, rt
1.2 Reagents: Hydrochloric acid Solvents: Water ;  acidified, rt

Reference

Interaction Studies between Carbonic Anhydrase and a Sulfonamide Inhibitor by Experimental and Theoretical Approaches

Pagnozzi, Daniela; Pala, Nicolino; Biosa, Grazia; Dallocchio, Roberto; Dessi, Alessandro; et al, ACS Medicinal Chemistry Letters, 2022, 13(2), 271-277

Production Method 8

1170077-68-5

94341-55-6

Reaction Conditions

1.1 Reagents: Hydrochloric acid Solvents: Ethanol ,  Water ;  2 h, 80 °C

Reference

Preparation of 4-oxo-2-thioxo-1,2,3,4-tetrahydro-7-quinazolinecarboxamide derivatives as inhibitors of HIF prolyl hydroxylase

, World Intellectual Property Organization, , ,

Production Method 9

94341-52-3

94341-55-6

Reaction Conditions

1.1 Reagents: Poly(methylhydrosiloxane) Catalysts: Triphenylphosphine Solvents: Cyclopentyl methyl ether ;  20 h, 110 °C
1.2 Reagents: Water ;  15 min, 110 °C

Reference

Sustainable organophosphorus-catalysed Staudinger reduction

Lenstra, Danny C.; Lenting, Peter E.; Mecinovic, Jasmin, Green Chemistry, 2018, 20(19), 4418-4422

Production Method 10

32752-54-8

94341-55-6

Reaction Conditions

1.1 Reagents: Sodium azide Catalysts: Tetrabutylammonium iodide Solvents: Dimethyl sulfoxide ;  8 h, rt

Reference

Structure-Activity Relationships in the Binding of Chemically Derivatized CD4 to gp120 from Human Immunodeficiency Virus

Xie, Hui; Ng, Danny; Savinov, Sergey N.; Dey, Barna; Kwong, Peter D.; et al, Journal of Medicinal Chemistry, 2007, 50(20), 4898-4908

Production Method 11

94341-55-6

Reaction Conditions

Reference

A chemoselective conversion of alkyl and aryl azides to amines with sodium hydrogen telluride

Suzuki, Hitomi; Takaoka, Koji, Chemistry Letters, 1984, (10), 1733-6

Production Method 12

94341-52-3

94341-55-6

Reaction Conditions

1.1 Solvents: Tetrahydrofuran ;  15 h, 60 °C

Reference

Ortho-Phosphinoarenesulfonamide-Mediated Staudinger Reduction of Aryl and Alkyl Azides

Li, Xingzhuo; Wang, Zhenguo; Luo, Wenjun ; Wang, Zixu; Yin, Keshu; et al, Molecules, 2022, 27(17),

Methanone, [4-(aminomethyl)phenyl]phenyl- Raw materials

• 1-[(4-Benzoylphenyl)methyl]-3,5,7-triaza-1-azoniatricyclo[3.3.1.13,7]decane bromide (1:1)
• 4-Benzoyl benzylamine Hydrochloride
• 4-Methylbenzophenone
• 4-(Bromomethyl)benzophenone
• Methanone, [4-(azidomethyl)phenyl]phenyl-

Methanone, [4-(aminomethyl)phenyl]phenyl- Preparation Products

• Methanone, [4-(aminomethyl)phenyl]phenyl- (94341-55-6)

• 1. Excimer–monomer switch: a reaction-based approach for selective detection of fluoride?
  Qiao Song,Angela Bamesberger,Lingyun Yang,Haley Houtwed,Haishi Cao Analyst, 2014,139, 3588-3592
• 2. Ester-mediated peptide formation promoted by deep eutectic solvents: a facile pathway to proto-peptides?
  Chen-Yu Chien,Sheng-Sheng Yu Chem. Commun., 2020,56, 11949-11952
• 3. Evolution in surface coverage of CH3NH3PbI3?XClXvia heat assisted solvent vapour treatment and their effects on photovoltaic performance of devices
  Dhirendra K. Chaudhary,Pramendra Kumar,Lokendra Kumar RSC Adv., 2016,6, 94731-94738
• 4. Excimer and exciplex formation in a pair of bright phosphorescent isomers constructed from Cu3(pyrazolate)3 and Cu3I3 coordination luminophores?
  Shun-Ze Zhan,Mian Li,Xiao-Ping Zhou,Dan Li,Seik Weng Ng RSC Adv., 2011,1, 1457-1459
• 5. Dissolution of cork biopolymers in biocompatible ionic liquids
  Helga Garcia,Rui Ferreira,Marija Petkovic,Jamie L. Ferguson,Maria C. Leit?o,H. Q. Nimal Gunaratne,Luís Paulo N. Rebelo Green Chem., 2010,12, 367-369

• 2098070-20-1(2-(3-(Pyridin-3-yl)-1H-pyrazol-1-yl)acetimidamide)
• 2680771-01-9(4-cyclopentyl-3-{(prop-2-en-1-yloxy)carbonylamino}butanoic acid)
• 1444113-98-7(N-(3-cyanothiolan-3-yl)-2-[(2,2,2-trifluoroethyl)sulfanyl]pyridine-4-carboxamide)
• 332062-08-5(Fmoc-S-3-amino-4,4-diphenyl-butyric acid)
• 1270529-38-8(1,2,3,4,5,6-Hexahydro-[2,3]bipyridinyl-6-ol)
• 941977-17-9(N'-(3-chloro-2-methylphenyl)-N-2-(dimethylamino)-2-(naphthalen-1-yl)ethylethanediamide)
• 2138166-62-6(2,2-Difluoro-3-[methyl(2-methylbutyl)amino]propanoic acid)
• 89640-58-4(2-Iodo-4-nitrophenylhydrazine)
• 1449132-38-0(3-Fluoro-5-(2-fluoro-5-methylbenzylcarbamoyl)benzeneboronic acid)
• 2034271-14-0(2-(1H-indol-3-yl)-N-{[6-(thiophen-2-yl)-[1,2,4]triazolo[4,3-b]pyridazin-3-yl]methyl}acetamide)