Production Method 1

6972-27-6

93787-99-6

Reaction Conditions

Reference

Phase-transfer catalyzed preparation of 6-alkoxy and 6-thioalkoxy-1,3-dimethyluracils

Gogoi, Mukti; Sandhu, Jagir S.; Baruah, J. N., Indian Journal of Chemistry, 1984, (9), 851-2

Production Method 2

6972-27-6

93787-99-6

Reaction Conditions

1.1 Solvents: Ethanol ;  0.5 min, 60 °C
1.2 Reagents: Hydrochloric acid Solvents: Water ;  pH 6, rt

Reference

Synthesis of substituted uracils by the reactions of halouracils with selenium, sulfur, oxygen, and nitrogen nucleophiles under focused microwave irradiation

Fang, Woei-Ping; Cheng, Yuh-Tsyr; Cheng, Yann-Ru; Cherng, Yie-Jia, Tetrahedron, 2005, 61(12), 3107-3113

Production Method 3

6972-27-6

93787-99-6

Reaction Conditions

1.1 Reagents: Sodium carbonate Solvents: Ethanol ;  28 h, reflux

Reference

Chemical models and their mechanistic implications for the transformation of 6-cyanouridine 5'-monophosphate catalyzed by orotidine 5'-monophosphate decarboxylase

Wu, Yuen-Jen; Liao, Chen-Chieh; Jen, Cheng-Hung; Shih, Yu-Chiao; Chien, Tun-Cheng, Chemical Communications (Cambridge, 2010, 46(26), 4821-4823

Production Method 4

49846-86-8

93787-99-6

Reaction Conditions

Reference

Chemical models and their mechanistic implications for the transformation of 6-cyanouridine 5'-monophosphate catalyzed by orotidine 5'-monophosphate decarboxylase

Chien, Tun-Cheng; Jen, Cheng-Hung; Wu, Yuen-Jen; Liao, Chen-Chieh, Nucleic Acids Symposium Series, 2008, 52(1), 297-298

Production Method 5

49846-86-8

93787-99-6

5770-46-7

Reaction Conditions

1.1 Catalysts: 4-(Dimethylamino)pyridine Solvents: Ethanol ;  24 h, reflux

Reference

Study on the synthesis of 6-alkylaminouridines via the nucleophilic aromatic substitution reaction of 6-cyanouridine derivatives

Lin, Jian-Bang; He, Jhih-Li; Shih, Yu-Chiao; Chien, Tun-Cheng, Tetrahedron Letters, 2011, 52(31), 3969-3972

6-Ethoxy-1,3-dimethylpyrimidine-2,4(1H,3H)-dione Raw materials

• 6-chloro-1,3-dimethyl-1,2,3,4-tetrahydropyrimidine-2,4-dione
• 1,3-Dimethyl-6-cyanouracil

6-Ethoxy-1,3-dimethylpyrimidine-2,4(1H,3H)-dione Preparation Products

• 6-BUTYLAMINO-1,3-DIMETHYLURACIL (5770-46-7)
• 6-Ethoxy-1,3-dimethylpyrimidine-2,4(1H,3H)-dione (93787-99-6)

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• 5. Evidence of CO2 molecule acting as an electron acceptor on a nanoporous metal–organic-framework MIL-53 or Cr3+(OH)(O2C–C6H4–CO2)?
  Alexandre Vimont,Arnaud Travert,Philippe Bazin,Jean-Claude Lavalley,Marco Daturi,Christian Serre,Gérard Férey,Sandrine Bourrelly,Philip L. Llewellyn Chem. Commun., 2007, 3291-3293

• Solvents and Organic Chemicals Organic Compounds Organoheterocyclic compounds Diazines Pyrimidones
• Solvents and Organic Chemicals Organic Compounds Organoheterocyclic compounds Diazines Pyrimidines and pyrimidine derivatives Pyrimidones

• 29458-38-6(6-Methoxypyrimidine-2,4(1H,3H)-dione)
• 60271-06-9(2,4(1H,3H)-Pyrimidinedione, 6-ethoxy-3-methyl-)
• 105556-07-8(2,4(1H,3H)-Pyrimidinedione, 1,3-dimethyl-6-(2-oxopropoxy)-)
• 136819-96-0(1-[(prop-2-en-1-yloxy)methyl]pyrimidine-2,4(1H,3H)-dione)
• 4097-20-5(6-methoxy-1,3-dimethyl-2,4(1h,3h)-pyrimidinedione)
• 857475-91-3(6-Ethoxypyrimidine-2,4(1H,3H)-dione)
• 131194-00-8(2,4(1H,3H)-Pyrimidinedione,1-[(2-hydroxyethoxy)methyl]-6-methoxy-5-methyl-)
• 882872-13-1(6-Hydroxy-3-methylpyrimidine-2,4(1H,3H)-dione)
• 36161-39-4(6-Methoxy-1-methylpyrimidine-2,4(1H,3H)-dione)
• 60271-08-1(2,4(1H,3H)-Pyrimidinedione, 6-ethoxy-3-ethyl-)