Production Method 1

87-62-7

919785-81-2

Reaction Conditions

1.1 Reagents: Potassium carbonate ,  Deuterium Catalysts: 2412806-73-4 Solvents: Dichloromethane ;  12 h, 50 °C

Reference

Mesoionic Carbene-Iridium Complex Catalyzed Ortho-Selective Hydrogen Isotope Exchange of Anilines with High Functional Group Tolerance

Liu, Wei; Cao, Lei; Zhang, Zengyu; Zhang, Gang; Huang, Shiqing; et al, Organic Letters, 2020, 22(6), 2210-2214

Production Method 2

919785-80-1

919785-81-2

Reaction Conditions

1.1 Reagents: Magnesium Solvents: Diethyl ether ;  reflux; 2 h, reflux; reflux → rt
1.2 Reagents: (Azidomethyl)trimethylsilane ;  rt; 3 h, rt
1.3 Reagents: Water ;  rt

Reference

Understanding Structural Isomerization during Ruthenium-Catalyzed Olefin Metathesis: A Deuterium Labeling Study

Courchay, Florence C.; Sworen, John C.; Ghiviriga, Ion; Abboud, Khalil A.; Wagener, Kenneth B., Organometallics, 2006, 25(26), 6074-6086

2,6-Dimethylaniline-D6 Raw materials

• 2,6-Dimethylaniline
• 2-Bromo-1,3-di(methyl-d3)benzene

2,6-Dimethylaniline-D6 Preparation Products

• 2,6-Dimethylaniline-D6 (919785-81-2)

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• 6393-01-7(2,5-Dimethyl-1,4-phenylenediamine)
• 95-68-1(2,4-dimethylaniline)
• 88-05-1(2,4,6-Trimethylaniline (Mesidine), ND25=1,4959)
• 10546-24-4(3-Methylnaphthalen-2-amine)
• 87-62-7(2,6-Dimethylaniline)
• 3102-70-3(2,4,6-Trimethyl-1,3-benzenediamine)
• 194423-47-7(2-Toluidine-d9)
• 332062-08-5(Fmoc-S-3-amino-4,4-diphenyl-butyric acid)
• 1270529-38-8(1,2,3,4,5,6-Hexahydro-[2,3]bipyridinyl-6-ol)
• 2680771-01-9(4-cyclopentyl-3-{(prop-2-en-1-yloxy)carbonylamino}butanoic acid)