Production Method 1

24623-65-2

83816-59-5

Reaction Conditions

1.1 Reagents: Iodine chloride Solvents: Acetic acid ;  rt; 5 h, reflux

Reference

Chiral Fe-Dendrimer-Catalyzed Domino Michael and Aldol Reactions of Chalcones with 1,4-Dithiane-2,5-diol

Kannan, Masanam; et al, ChemistrySelect, 2018, 3(3), 859-863

Production Method 2

88-18-6

83816-59-5

Reaction Conditions

1.1 Reagents: Triethylamine ,  Magnesium chloride Solvents: Tetrahydrofuran ;  4 h, 85 °C
2.1 Reagents: Iodine chloride Solvents: Acetic acid ;  10 h, reflux

Reference

Polyfunctional Conjugated Microporous Polymers for Applications in Direct C-H Arylation of Unactivated Arenes and Aqueous Adsorption of Aromatic Amines

Luo, Kexin; et al, Chemical Research in Chinese Universities, 2020, 36(6), 1302-1309

Production Method 3

88-18-6

83816-59-5

Reaction Conditions

1.1 Reagents: 2,6-Lutidine ,  Tin tetrachloride Solvents: Toluene ;  2 h, rt
1.2 10 h, 100 °C; 100 °C → rt
1.3 Reagents: Hydrochloric acid Solvents: Water ;  pH 2
2.1 Reagents: Iodine chloride Solvents: Acetic acid ;  rt; 5 h, reflux

Reference

Chiral Fe-Dendrimer-Catalyzed Domino Michael and Aldol Reactions of Chalcones with 1,4-Dithiane-2,5-diol

Kannan, Masanam; et al, ChemistrySelect, 2018, 3(3), 859-863

Production Method 4

24623-65-2

83816-59-5

Reaction Conditions

1.1 Reagents: Iodine chloride Solvents: Acetic acid ;  rt; 3 h, rt → reflux

Reference

Self-Assembled Dinuclear Cobalt(II)-Salen Catalyst Through Hydrogen-Bonding and Its Application to Enantioselective Nitro-Aldol (Henry) Reaction

Park, Jongwoo; et al, Journal of the American Chemical Society, 2008, 130(49), 16484-16485

Production Method 5

24623-65-2

83816-59-5

Reaction Conditions

1.1 Reagents: Iodine chloride Solvents: Acetic acid ;  rt; 12 h, reflux

Reference

Efficient cycloaddition of CO2 and epoxides to cyclic carbonates using salen-based covalent organic framework as a heterogeneous catalyst

Tong, Yutao; et al, Journal of Porous Materials, 2022, 29(4), 1253-1263

Production Method 6

88-18-6

83816-59-5

Reaction Conditions

1.1 Reagents: Triethylamine ,  Sulfuric acid magnesium salt (1:1) Solvents: Tetrahydrofuran ;  reflux
2.1 Reagents: Iodine chloride Solvents: Acetic acid ;  reflux

Reference

Synthesis of new chiral Mn(III)-salen complexes as recoverable and reusable homogeneous catalysts for the asymmetric epoxidation of styrenes and chromenes

Chaudhary, Pooja; et al, New Journal of Chemistry, 2022, 46(3), 1308-1318

Benzaldehyde, 3-(1,1-dimethylethyl)-2-hydroxy-5-iodo- Raw materials

• 3-Tert-Butyl-2-hydroxybenzaldehyde
• 2-tert-Butylphenol

Benzaldehyde, 3-(1,1-dimethylethyl)-2-hydroxy-5-iodo- Preparation Products

• Benzaldehyde, 3-(1,1-dimethylethyl)-2-hydroxy-5-iodo- (83816-59-5)

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• 39730-66-0(2-Hydroxy-4-iodo-acetophenone)
• 89209-02-9(Phenol, 2,4-bis(1,1-dimethylethyl)-6-iodo-)
• 71243-12-4(Ethanone, 1-(2,4-dihydroxy-3-iodophenyl)-)
• 175655-10-4(Ethanone, 1-(2-hydroxy-3-iodo-5-methylphenyl)-)
• 7191-41-5(1-(2-Hydroxy-5-iodophenyl)ethanone)
• 62069-33-4(Ethanone, 1-(2,4-dihydroxy-5-iodophenyl)-)
• 60803-25-0(2-Tert-butyl-4-iodophenol)
• 7191-46-0(1-(2-hydroxy-3,5-diiodophenyl)ethan-1-one)
• 86445-79-6(Phenol, 2-(1,1-dimethylethyl)-6-iodo-4-methyl-)
• 60803-26-1(2-(tert-Butyl)-4,6-diiodophenol)