Production Method 1

29968-78-3

83303-98-4

Reaction Conditions

1.1 Reagents: Triethylamine ,  1-Hydroxybenzotriazole ,  1-Ethyl-3-(3′-dimethylaminopropyl)carbodiimide hydrochloride Solvents: Dimethylformamide ;  0 °C; 18 h, 0 °C → rt
1.2 Solvents: Water

Reference

Synthesis of related substance of mirabegron

Zhang, Lei; et al, Zhongguo Yiyao Gongye Zazhi, 2014, 45(1), 9-12

Production Method 2

29968-78-3

83303-98-4

Reaction Conditions

1.1 Reagents: 1-Hydroxybenzotriazole ,  Diisopropylethylamine ,  1-Ethyl-3-(3′-dimethylaminopropyl)carbodiimide hydrochloride Solvents: Dimethylacetamide ;  overnight, 25 °C

Reference

Novel dual inhibitors against FP-2 and PfDHFR as potential antimalarial agents: Design, synthesis and biological evaluation

Chen, Wenhua; et al, Chinese Chemical Letters, 2019, 30(1), 250-254

Production Method 3

24954-67-4

83303-98-4

Reaction Conditions

1.1 Catalysts: Triethylamine

Reference

Synthesis and photooxygenation of some substituted 1-benzyl-3,4-dihydroisoquinolines. Mechanism of enamine photooxygenation

Martin, Ned H.; et al, Helvetica Chimica Acta, 1982, 65(3), 762-74

Benzeneacetamide, N-[2-(4-nitrophenyl)ethyl]- Raw materials

• 2-(4-Nitrophenyl)ethanamine
• 4-Nitrophenethylamine hydrochloride

Benzeneacetamide, N-[2-(4-nitrophenyl)ethyl]- Preparation Products

• Benzeneacetamide, N-[2-(4-nitrophenyl)ethyl]- (83303-98-4)

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• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Phenylacetamides

• 332062-08-5(Fmoc-S-3-amino-4,4-diphenyl-butyric acid)
• 1270529-38-8(1,2,3,4,5,6-Hexahydro-[2,3]bipyridinyl-6-ol)
• 2680771-01-9(4-cyclopentyl-3-{(prop-2-en-1-yloxy)carbonylamino}butanoic acid)
• 2098070-20-1(2-(3-(Pyridin-3-yl)-1H-pyrazol-1-yl)acetimidamide)
• 1444113-98-7(N-(3-cyanothiolan-3-yl)-2-[(2,2,2-trifluoroethyl)sulfanyl]pyridine-4-carboxamide)
• 941977-17-9(N'-(3-chloro-2-methylphenyl)-N-2-(dimethylamino)-2-(naphthalen-1-yl)ethylethanediamide)
• 2138166-62-6(2,2-Difluoro-3-[methyl(2-methylbutyl)amino]propanoic acid)
• 89640-58-4(2-Iodo-4-nitrophenylhydrazine)
• 1449132-38-0(3-Fluoro-5-(2-fluoro-5-methylbenzylcarbamoyl)benzeneboronic acid)
• 2034271-14-0(2-(1H-indol-3-yl)-N-{[6-(thiophen-2-yl)-[1,2,4]triazolo[4,3-b]pyridazin-3-yl]methyl}acetamide)