Production Method 1

81502-74-1

Reaction Conditions

1.1 Reagents: Trifluoroacetic acid ;  0 °C; 20 h, 120 °C; 30 min, 150 °C; 150 °C → 120 °C
1.2 Reagents: Hydrochloric acid Solvents: Water ;  30 min, 120 °C

Reference

Acridine-Functionalized Covalent Organic Frameworks (COFs) as Photocatalysts for Metallaphotocatalytic C-N Cross-Coupling

Traxler, Michael; et al, Angewandte Chemie, 2022, 61(21),

Production Method 2

81502-74-1

Reaction Conditions

1.1 Reagents: Trifluoroacetic acid ;  16 h, 130 °C; 130 °C → 150 °C; 3 h, 150 °C; 150 °C → 120 °C
1.2 Reagents: Hydrochloric acid Solvents: Water ;  30 min, 105 °C; overnight, 105 °C → rt

Reference

Chiral, triformylphenol-derived salen-type [4 + 6] organic cages

Petryk, M.; et al, Organic & Biomolecular Chemistry, 2016, 14(31), 7495-7499

Production Method 3

81502-74-1

Reaction Conditions

1.1 Reagents: Trifluoroacetic acid ;  0 °C; 20 h, 0 °C → 125 °C; 125 °C → 150 °C; 3 h, 150 °C; 150 °C → 100 °C
1.2 Reagents: Hydrochloric acid Solvents: Water ;  30 min, 100 °C

Reference

Photochemical Amplifier Based on Self-Immolative Dendritic Spacers

Kastrati, Agonist; et al, Journal of Organic Chemistry, 2019, 84(12), 7776-7785

Production Method 4

123-08-0

81502-74-1

Reaction Conditions

1.1 Reagents: Trifluoroacetic acid
1.2 Reagents: Hydrochloric acid Solvents: Water

Reference

A convenient one-step synthesis of 2-hydroxy-1,3,5-benzenetricarbaldehyde

Anderson, Andrew A.; et al, Synthetic Communications, 2000, 30(17), 3227-3232

TFP Raw materials

• 4-Hydroxybenzaldehyde

TFP Preparation Products

• TFP (81502-74-1)

• 1. Emerging 2D hybrid nanomaterials: towards enhanced sensitive and selective conductometric gas sensors at room temperature
  Hanie Hashtroudi,Ian D. R. Mackinnon J. Mater. Chem. C, 2020,8, 13108-13126
• 2. Exceptionally high temperature spin crossover in amide-functionalised 2,6-bis(pyrazol-1-yl)pyridine iron(ii) complex revealed by variable temperature Raman spectroscopy and single crystal X-ray diffraction?
  Max Attwood,Hiroki Akutsu,Lee Martin,Toby J. Blundell,Pierre Le Maguere,Scott S. Turner Dalton Trans., 2021,50, 11843-11851
• 3. Fate of Sb(v) and Sb(iii) species along a gradient of pH and oxygen concentration in the Carnoulès mine waters (Southern France)
  Eléonore Resongles,Corinne Casiot,Fran?oise Elbaz-Poulichet,Rémi Freydier,Odile Bruneel,Christine Piot,Sophie Delpoux,Aurélie Volant,Angélique Desoeuvre Environ. Sci.: Processes Impacts, 2013,15, 1536-1544
• 4. Excellent kinetics of single-phase Gd-doped ceria fuel electrodes in solid oxide cells?
  Andreas Nenning,Manuel Holzmann,Jürgen Fleig,Alexander K. Opitz Mater. Adv., 2021,2, 5422-5431
• 5. Emergence of microfluidic wearable technologies
  Joo Chuan Yeo,Kenry Lab Chip, 2016,16, 4082-4090

• Solvents and Organic Chemicals Organic Compounds Organic oxygen compounds Organooxygen compounds Carbonyl compounds Aldehydes
• Solvents and Organic Chemicals Organic Compounds Aldehyde/Ketone

• 14283-80-8(Lanthanum,tris[2-(hydroxy-kO)benzaldehydato-kO]-)
• 27761-48-4(Benzaldehyde,2-hydroxy-, lithium salt (1:1))
• 1194-98-5(2,5-Dihydroxybenzaldehyde)
• 14523-25-2(Copper, bis[2-(hydroxy-kO)benzaldehydato-kO]-)
• 14263-01-5(Nickel, bis[2-(hydroxy-kO)benzaldehydato-kO]-)
• 90-02-8(2-Hydroxybenzaldehyde)
• 6248-20-0(4-Formyl-2-methylresorcinol)
• 613-84-3(2-Hydroxy-5-methylbenzaldehyde)
• 698-27-1(2-Hydroxy-4-methylbenzaldehyde)
• 28777-87-9(Benzaldehyde, hydroxy-)