Production Method 1

6602-33-1

79491-45-5

Reaction Conditions

1.1 Reagents: Potassium carbonate Solvents: Dimethyl sulfoxide ;  2 h, reflux
1.2 Solvents: Water ;  30 min, 50 °C

Reference

Lead identification of benzimidazolone and azabenzimidazolone arylsulfonamides as CC-chemokine receptor 4 (CCR4) antagonists

Miah, Afjal H.; Abas, Hossay; Begg, Malcolm; Marsh, Benjamin J.; O'Flynn, Daniel E.; et al, Bioorganic & Medicinal Chemistry, 2014, 22(15), 4298-4311

Production Method 2

6602-33-1

79491-45-5

Reaction Conditions

1.1 Reagents: Potassium carbonate Solvents: Dimethyl sulfoxide ;  1.5 h, 70 °C

Reference

Phosphoinositide-3-kinase inhibitors: Evaluation of substituted alcohols as replacements for the piperazine sulfonamide portion of AMG 511

Lanman, Brian A.; Reed, Anthony B.; Cee, Victor J.; Hong, Fang-Tsao; Pettus, Liping H.; et al, Bioorganic & Medicinal Chemistry Letters, 2014, 24(24), 5630-5634

Production Method 3

6602-33-1

79491-45-5

Reaction Conditions

1.1 Catalysts: Potassium carbonate

Reference

Synthetic uses of the sequential ring positional reactivity in pyridin-3-ol and derivatives

Clark, Gary J.; Deady, Leslie W., Australian Journal of Chemistry, 1981, 34(4), 927-32

2,6-dibromo-3-methoxy-pyridine Raw materials

• 2,6-Dibromo-3-hydroxypyridine

2,6-dibromo-3-methoxy-pyridine Preparation Products

• 2,6-dibromo-3-methoxy-pyridine (79491-45-5)

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• 24100-18-3(2-Bromo-3-methoxypyridine)
• 104819-52-5(2-Bromo-3,4-dimethoxypyridine)
• 1185315-90-5(2-Bromo-5-methoxypyridine-d3)
• 149966-41-6(2-Bromo-3,5-dimethoxy-pyridine)
• 313657-71-5(2-((2-Bromopyridin-3-yl)oxy)ethanol)
• 89694-54-2(2-Bromo-3-ethoxypyridine)
• 6602-32-0(2-bromopyridin-3-ol)
• 162271-10-5(2-bromo-3-(methoxymethoxy)pyridine)
• 6602-33-1(2,6-Dibromo-3-hydroxypyridine)
• 105170-27-2(2-Bromo-5-methoxypyridine)