Production Method 1

5445-17-0

79-42-5

Reaction Conditions

1.1 Reagents: 2669091-24-9 Catalysts: Tetrabutylammonium bromide ;  12 h, rt
1.2 Reagents: Hydrochloric acid Solvents: Water ;  pH 2, rt

Reference

A convenient synthesis of thiol, trithiocarbonate and disulphide

Gondi, Sudershan R.; Rissing, Christiana Julia; Son, David Y., ChemRxiv, 2021, 1, 1-23

Production Method 2

79-42-5

Reaction Conditions

1.1 Reagents: Sodium carbonate Solvents: Water ;  neutralized
1.2 Reagents: Sodium thiosulfate ;  rt → 90 °C; 5 h, 80 - 90 °C
1.3 Reagents: Sulfuric acid ;  2.5 h, 50 - 90 °C
1.4 1 h, 20 - 40 °C; 40 °C → 90 °C; 1 h, 60 - 90 °C

Reference

Clean synthesis process of 2-mercaptopropionic acid

Zhang, Peng; Wu, Kuixia; Qi, Xin, Shanghai Huagong, 2014, 39(2), 17-20

Production Method 3

6431-92-1

79-42-5

Reaction Conditions

1.1 Reagents: Ammonia Solvents: Methanol ;  0 °C; 0 °C → rt; 1 h, rt
1.2 Reagents: Hydrochloric acid Solvents: Water ;  acidified

Reference

Isothiourea-catalysed enantioselective Michael addition of N-heterocyclic pronucleophiles to α,β-unsaturated aryl esters

Shu, Chang; Liu, Honglei; Slawin, Alexandra M. Z.; Carpenter-Warren, Cameron; Smith, Andrew D., Chemical Science, 2020, 11(1), 241-247

Production Method 4

79-42-5

79-42-5

Reaction Conditions

1.1 Reagents: Gold Solvents: Ethanol ;  10 min, rt

Reference

Electrochemical Reduction of CO2 at Functionalized Au Electrodes

Fang, Yuxin; Flake, John C., Journal of the American Chemical Society, 2017, 139(9), 3399-3405

Production Method 5

79-42-5

16056-34-1

79-42-5

Reaction Conditions

1.1 Reagents: Ammonium acetate Solvents: Water ;  overnight, rt

Reference

Analytical developments for the determination of monomethylmercury complexes with low molecular mass thiols by reverse phase liquid chromatography hyphenated to inductively coupled plasma mass spectrometry

Bouchet, Sylvain; Bjoern, Erik, Journal of Chromatography A, 2014, 1339, 50-58

Production Method 6

383400-97-3

79-42-5

Reaction Conditions

1.1 Reagents: Trifluoroacetic acid ,  Triethylsilane Solvents: Dichloromethane

Reference

S-4-Methoxytrityl mercapto acids: synthesis and application

Mourtas, S.; Gatos, D.; Kalaitzi, V.; Katakalou, C.; Barlos, K., Tetrahedron Letters, 2001, 42(39), 6965-6967

Production Method 7

51440-83-6

79-42-5

Reaction Conditions

1.1 Reagents: Ammonium hydroxide Solvents: Ethanol ,  Water

Reference

Studies on organic thio acids. V

Biilmann, Einar, Justus Liebigs Annalen der Chemie, 1906, 348, 120-143

Production Method 8

79-42-5

2768-02-7

79-42-5

Reaction Conditions

1.1 Catalysts: Azobisisobutyronitrile Solvents: Isopropanol ;  1 d, rt; 1 d, 60 °C

Reference

Transparent polyvinylsilsesquioxane aerogels: investigations on synthetic parameters and surface modification

Shimizu, Taiyo; Kanamori, Kazuyoshi ; Nakanishi, Kazuki, Journal of Sol-Gel Science and Technology, 2017, 82(1), 2-14

Production Method 9

6431-92-1

79-42-5

Reaction Conditions

1.1 Reagents: Ammonia Solvents: Methanol
1.2 Reagents: Hydrochloric acid

Reference

Highly enantioselective construction of tertiary thioethers and alcohols via phosphine-catalyzed asymmetric γ-addition reactions of 5H-thiazol-4-ones and 5H-oxazol-4-ones: scope and mechanistic understandings

Wang, Tianli; Yu, Zhaoyuan; Hoon, Ding Long; Huang, Kuo-Wei; Lan, Yu; et al, Chemical Science, 2015, 6(8), 4912-4922

Production Method 10

79-42-5

79-42-5

Reaction Conditions

1.1 Catalysts: 2,2-Dimethoxy-2-phenylacetophenone Solvents: Tetrahydrofuran ;  15 min

Reference

Norbornenyl-Based RAFT Agents for the Preparation of Functional Polymers via Thiol-Ene Chemistry

Stamenovic, Milan M.; Espeel, Pieter; Van Camp, Wim; Du Prez, Filip E., Macromolecules (Washington, 2011, 44(14), 5619-5630

Production Method 11

53907-46-3

79-42-5

Reaction Conditions

Reference

A process for the preparation of 2-mercaptoalkanoate esters as intermediates for agrochemicals, pharmaceuticals, and perfumes

, Japan, , ,

Production Method 12

79-42-5

Reaction Conditions

Reference

Tetra-substituted ethylenes

Ireland, C. J.; Jones, K.; Pizey, J. S.; Johnson, S., Synthetic Communications, 1976, 6(3), 185-91

2-sulfanylpropanoic acid Raw materials

• Methyl DL-2-bromopropionate
• 2-Mercaptopropionic Acid Methyl Ester
• Propanoic acid, 2-(acetylthio)-
• Propanoic acid, 2-[(ethoxythioxomethyl)thio]-
• 2-sulfanylpropanoic acid
• Vinyltrimethoxysilane
• Mercury, methyl-(8CI,9CI)
• Propanoic acid, 2-[[(4-methoxyphenyl)diphenylmethyl]thio]-

2-sulfanylpropanoic acid Preparation Products

• 2-sulfanylpropanoic acid (79-42-5)

• 1. Dissociative dynamics of O2 on Ag(110)?
  Ivor Lon?ari? Phys. Chem. Chem. Phys., 2015,17, 9436-9445
• 2. Exchangeability of amino acid residues with similar physicochemical properties in coiled-coil interactions?
  Guiying Zhang,Maosheng Cheng,Yanni Li,Keliang Liu,Lifeng Cai Chem. Commun., 2013,49, 11086-11088
• 3. Evolution of important glucosinolates in three common Brassica vegetables during their processing into vegetable powder and in vitro gastric digestion
  Nan Fu,Naphaporn Chiewchan,Xiao Dong Chen Food Funct., 2020,11, 211-220
• 4. Fast synthesis of red Li3BaSrLn3(WO4)8:Eu3+ phosphors for white LEDs under near-UV excitation by a microwave-assisted solid state reaction method and photoluminescence studies
  Bo Wei,Zhenyu Liu,Chen Xie,Shu Yang,Wentao Tang,Aiwei Gu,Wing-Tak Wong,Ka-Leung Wong J. Mater. Chem. C, 2015,3, 12322-12327
• 5. Excimer and exciplex formation in a pair of bright phosphorescent isomers constructed from Cu3(pyrazolate)3 and Cu3I3 coordination luminophores?
  Shun-Ze Zhan,Mian Li,Xiao-Ping Zhou,Dan Li,Seik Weng Ng RSC Adv., 2011,1, 1457-1459

• Solvents and Organic Chemicals Organic Compounds Organic acids and derivatives Carboxylic acids and derivatives Carboxylic acids alpha-Mercaptocarboxylic acids
• Solvents and Organic Chemicals Organic Compounds Alcohol/Ether

• 26473-48-3(2-sulfanylbutanoic acid)
• 62289-55-8(Propanoic acid, 2-mercapto-2-methyl-, disodium salt)
• 35440-77-8(Propanoic acid,2-mercapto-, strontium salt (2:1))
• 20461-87-4(2-(ethylthio)propanoic acid)
• 33178-97-1(Propanoic acid,2-(methylthio)-, (R)- (9CI))
• 58809-73-7(2-(Methylthio)propanoic acid)
• 54266-38-5((2-Hydroxyethyl)ammonium 2-mercaptopropionate)
• 4695-31-2(2-Mercaptoisobutyric Acid, 90%)
• 22535-46-2(Propanoic acid,2-mercapto-, sodium salt (1:1))
• 13419-67-5(Propanoic acid,2-mercapto-, ammonium salt (1:1))