Production Method 1

421-83-0

96284-27-4

74010-26-7

117559-35-0

85272-31-7

78393-18-7

Reaction Conditions

1.1 Solvents: tert-Butyl methyl ether ;  -78 °C; -78 °C → rt

Reference

Synthesis and crystal structures of tBu-substituted disiloxanes tBu2SiX-O-SiYtBu2 (X = Y = OH, Br; X = OH, Y = H) and of the adducts tBu3SiOH.(HO3SCF3)0.5.H2O and tBu3SiOLi.(LiO3SCF3)2.(H2O)2

Lerner, H.-W.; Scholz, S.; Wiberg, N.; Polborn, K.; Bolte, M.; et al, Zeitschrift fuer Anorganische und Allgemeine Chemie, 2005, 631(10), 1863-1870

Tetra-tert-butyldisiloxane-1,3-diol Raw materials

• Trifluoromethanesulfonyl chloride
• Silanediol, bis(1,1-dimethylethyl)-, monolithium salt (9CI)

Tetra-tert-butyldisiloxane-1,3-diol Preparation Products

• ditert-butyl-chloro-[ditert-butyl(chloro)silyl]oxysilane (117559-35-0)
• Di-tert-butylsilyl Bis(trifluoromethanesulfonate) (85272-31-7)
• Cyclotrisiloxane, hexakis(1,1-dimethylethyl)- (78393-18-7)
• Tetra-tert-butyldisiloxane-1,3-diol (74010-26-7)

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