Production Method 1

4979-18-4

769108-87-4

4702-09-4

Reaction Conditions

1.1 Reagents: Triethylamine ,  Hydrogen Catalysts: Palladium Solvents: Ethanol ;  rt → 70 °C; 6 h, 70 °C

Reference

Total synthesis of matrine alkaloids

Magann, Nicholas L.; Westley, Erin; Sowden, Madison J.; Gardiner, Michael G.; Sherburn, Michael S., ChemRxiv, 2022, 1, 1-5

Production Method 2

4979-18-4

769108-87-4

4702-09-4

Reaction Conditions

1.1 Reagents: Triethylamine ,  Hydrogen Catalysts: Palladium Solvents: Ethanol ;  rt → 70 °C; 6 h, 70 °C

Reference

Total Synthesis of Matrine Alkaloids

Magann, Nicholas L. ; Westley, Erin; Sowden, Madison J.; Gardiner, Michael G.; Sherburn, Michael S., Journal of the American Chemical Society, 2022, 144(43), 19695-19699

(+)-Matrin Preparation Products

• Matrine Impurity 7 (769108-87-4)
• (+)-Matrin (4702-09-4)
• (+)-Matrin (4979-18-4)

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