Production Method 1

27094-65-1

96-15-1

Reaction Conditions

1.1 Reagents: Urea ,  Potassium carbonate Catalysts: 1,3-Bis(diphenylphosphino)propane ,  Chloro(η5-2,4-cyclopentadien-1-yl)[1,1′-(1,2-ethanediyl)bis[1,1-diphenylphosphin… Solvents: Diglyme ;  12 h, 160 °C

Reference

Amination of aliphatic alcohols with urea catalyzed by ruthenium complexes: effect of supporting ligands

Dindar, Sara; Nemati Kharat, Ali, Journal of Coordination Chemistry, 2020, 73(13), 1954-1966

Production Method 2

116-53-0

27094-65-1

1113-57-1

96-15-1

Reaction Conditions

1.1 Reagents: Hydrogen ,  Ammonia Catalysts: Aluminum magnesium oxide (Al2MgO4) ,  Ruthenium tungsten oxide Solvents: Cyclopentyl methyl ether ;  6 bar, rt → 200 °C; 6.5 h, 50 bar, 200 °C

Reference

One-pot reductive amination of carboxylic acids: a sustainable method for primary amine synthesis

Coeck, Robin; De Vos, Dirk E., Green Chemistry, 2020, 22(15), 5105-5114

1-Butanamine,2-methyl-N-(2-methylbutyl)- Raw materials

• 2-Methylbutanoic acid

1-Butanamine,2-methyl-N-(2-methylbutyl)- Preparation Products

• 2-methylbutanamide (1113-57-1)
• 2-methylbutan-1-amine (96-15-1)
• 1-Butanamine,2-methyl-N-(2-methylbutyl)- (27094-65-1)

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