Production Method 1

254454-54-1

1765-93-1

2427990-83-6

1044507-64-3

Reaction Conditions

1.1R:Cs2CO3, C:Pd acetylacetonate, C:657408-07-6, S:p-Cymene, S:H2O, 24 h, 100°C

Reference

Synthesis of 2-Aryl Azetidines through Pd-Catalyzed Migration/Coupling of 3-Iodoazetidines and Aryl Boronic Acids

By Yang, Han et al, Organic Letters, 2022, 24(31), 5731-5735

Production Method 2

24424-99-5

405-99-2

1189-71-5

2427990-83-6

Reaction Conditions

1.1S:Et2O, 0°C; 10 min, 0°C; 4 h, rt
2.1R:LiAlH4, S:Et2O, 0°C; 8 h, reflux
3.1R:Et3N, S:CH2Cl2, 12 h, rt

Reference

Photocatalytic Carboxylation of C-N Bonds in Cyclic Amines with CO2 by Consecutive Visible-Light-Induced Electron Transfer

By Chen, Lin et al, Angewandte Chemie, 2023, 62(11), e202217918

1-Azetidinecarboxylic acid, 2-(4-fluorophenyl)-, 1,1-dimethylethyl ester Raw materials

• Di-tert-butyl dicarbonate
• 1-Boc-3-iodoazetidine
• 4-Fluorobenzeneboronic acid
• 1-fluoro-4-vinyl-benzene
• Chlorosulfonyl isocyanate

1-Azetidinecarboxylic acid, 2-(4-fluorophenyl)-, 1,1-dimethylethyl ester Preparation Products

• 1-Azetidinecarboxylic acid, 3-(4-fluorophenyl)-, 1,1-dimethylethyl ester (1044507-64-3)
• 1-Azetidinecarboxylic acid, 2-(4-fluorophenyl)-, 1,1-dimethylethyl ester (2427990-83-6)

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