Production Method 1

36098-65-4

1111-72-4

2417951-50-7

64577-25-9

Reaction Conditions

1.1R:18-Crown-6, S:DMF, 48 h, 135°C, 1 atm
1.2R:HCl, S:H2O, acidify

Reference

Direct reversible decarboxylation from stable organic acids in dimethylformamide solution

By Kong, Duanyang et al, Science (Washington, 2020, 369(6503), 557-561

Production Method 2

36098-65-4

1111-72-4

2417951-50-7

64577-25-9

Reaction Conditions

1.1R:18-Crown-6, S:DMF, 48 h, 135°C, 1 atm
1.2R:HCl, S:H2O, acidify

Reference

Direct reversible decarboxylation from stable organic acids in solution

By Kong, Duanyang et al, ChemRxiv, 2020, From ChemRxiv, 1-11

Raw materials

• Propanedioic acid, 2-(phenylmethyl)-, potassium salt (1:2)
• Carbon-13C dioxide

Preparation Products

• HYDROCINNAMIC ACID(1-13C, 99%) (64577-25-9)
• (2417951-50-7)

• 1. Fate of Sb(v) and Sb(iii) species along a gradient of pH and oxygen concentration in the Carnoulès mine waters (Southern France)
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• 2. Emerging 2D hybrid nanomaterials: towards enhanced sensitive and selective conductometric gas sensors at room temperature
  Hanie Hashtroudi,Ian D. R. Mackinnon J. Mater. Chem. C, 2020,8, 13108-13126
• 3. Emergence of microfluidic wearable technologies
  Joo Chuan Yeo,Kenry Lab Chip, 2016,16, 4082-4090
• 4. Evolution and characterization of a benzylguanine-binding RNA aptamer?
  J. Xu,T. J. Carrocci,A. A. Hoskins Chem. Commun., 2016,52, 549-552
• 5. Excellent kinetics of single-phase Gd-doped ceria fuel electrodes in solid oxide cells?
  Andreas Nenning,Manuel Holzmann,Jürgen Fleig,Alexander K. Opitz Mater. Adv., 2021,2, 5422-5431

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