Production Method 1

619-84-1

24424-99-5

593-51-1

1942884-35-6

Reaction Conditions

1.1R:Et3N, R:4-DMAP, R:EtN=C=N(CH2)3NMe2 ?HCl, S:CH2Cl2, 2 h, rt
1.2R:NaHCO3, rt
1.3C:4-DMAP, S:MeCN, rt; 3 h, 40°C
1.4R:NaHCO3, S:H2O

Reference

Nickel-Catalyzed Decarbonylative Borylation of Amides: Evidence for Acyl C-N Bond Activation

By Hu, Jiefeng et al, Angewandte Chemie, 2016, 55(30), 8718-8722

Carbamic acid, N-[4-(dimethylamino)benzoyl]-N-methyl-, 1,1-dimethylethyl ester Raw materials

• 4-(Dimethylamino)benzoic acid
• Di-tert-butyl dicarbonate
• Methylammonium Chloride

Carbamic acid, N-[4-(dimethylamino)benzoyl]-N-methyl-, 1,1-dimethylethyl ester Preparation Products

• Carbamic acid, N-[4-(dimethylamino)benzoyl]-N-methyl-, 1,1-dimethylethyl ester (1942884-35-6)

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