Production Method 1

14282-76-9

185990-03-8

17881-88-8

885692-91-1

Reaction Conditions

1.1 Solvents: Methyl ether ;  10 min, 30 °C
1.2 30 °C; 1 h, 30 °C; 30 °C → -7 °C
1.3 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  -7 °C

Reference

Boryl substitution of functionalized aryl-, heteroaryl- and alkenyl halides with silylborane and an alkoxy base: expanded scope and mechanistic studies

Yamamoto, Eiji; Ukigai, Satoshi; Ito, Hajime, Chemical Science, 2015, 6(5), 2943-2951

Production Method 2

89827-45-2

185990-03-8

17881-88-8

912824-85-2

Reaction Conditions

1.1 Solvents: Methyl ether ;  10 min, 30 °C
1.2 30 °C; 1 h, 30 °C; 30 °C → -7 °C
1.3 Reagents: Tetrabutylammonium fluoride Solvents: Tetrahydrofuran ;  2 h, -7 °C

Reference

Boryl substitution of functionalized aryl-, heteroaryl- and alkenyl halides with silylborane and an alkoxy base: expanded scope and mechanistic studies

Yamamoto, Eiji; Ukigai, Satoshi; Ito, Hajime, Chemical Science, 2015, 6(5), 2943-2951

Methoxydimethylphenylsilane Raw materials

• 4-Bromodibenzofuran
• 2-Bromo-3-methylthiophene
• dimethyl(phenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

Methoxydimethylphenylsilane Preparation Products

• 4,4,5,5-Tetramethyl-2-(3-methylthiophen-2-yl)-1,3,2-dioxaborolane (885692-91-1)
• Methoxydimethylphenylsilane (17881-88-8)
• 2-(Dibenzob,dfuran-4-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (912824-85-2)

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• Solvents and Organic Chemicals Organic Compounds Organometallic compounds Organometalloid compounds Organosilicon compounds Alkylarylsilanes
• Other Chemical Reagents Organic Metal Reagents

• 2754-32-7(1,4-Bis(hydroxydimethylsilyl)benzene)
• 1825-59-8(Ethoxy(methyl)diphenylsilane)
• 5272-18-4(Dimethylphenylsilanol)
• 1825-58-7(Benzene,(ethoxydimethylsilyl)-)
• 33546-26-8(Benzene,1-(dimethylsilyl)-4-(methoxydimethylsilyl)-)
• 1829-41-0(Methoxytriphenylsilane)
• 51501-87-2(Methoxydimethyl(p-tolyl)silane)
• 131182-68-8(1,4-Bis(methoxydimethylsilyl)benzene)
• 63148-58-3(Silicone oil)
• 1516-80-9(Ethoxy(triphenyl)silane)