Production Method 1

127368-12-1

943-15-7

118297-28-2

127420-20-6

Reaction Conditions

1.1 Reagents: Nitrogen dioxide Solvents: Acetic anhydride

Reference

The nitration of p-cymene with nitrogen dioxide in acetic anhydride

Hartshorn, Michael P.; Robinson, Ward T.; Waller, A. Grant; Wright, Graeme J., Australian Journal of Chemistry, 1989, 42(12), 2143-60

Production Method 2

52834-93-2

127368-12-1

943-15-7

127420-18-2

127368-10-9

118297-28-2

127420-20-6

Reaction Conditions

1.1 Reagents: Nitrogen dioxide Solvents: Acetic anhydride

Reference

Reactions of 4-methyl-1-(1'-methylethyl)-4-nitrocyclohexa-2,5-dien-1-yl acetates with nitrogen dioxide; towards a mechanism for the formation of polynitro cyclohexenyl esters on reaction of p-cymene with nitrogen dioxide in acetic anhydride

Abell, Andrew D.; Hartshorn, Michael P.; Robinson, Ward T.; Waller, A. Grant; Wright, Graeme J., Australian Journal of Chemistry, 1989, 42(12), 2225-42

4-Cyclohexene-1,3-diol, 2-methyl-5-(1-methylethyl)-2,6-dinitro-, 1-nitrate, (1α,2α,3α,6β)- Raw materials

• 2,5-Cyclohexadien-1-ol, 4-methyl-1-(1-methylethyl)-4-nitro-, acetate (ester), trans- (9CI)

4-Cyclohexene-1,3-diol, 2-methyl-5-(1-methylethyl)-2,6-dinitro-, 1-nitrate, (1α,2α,3α,6β)- Preparation Products

• 2-Nitro-4-cymene (943-15-7)
• 3-Cyclohexen-1-ol, 2-methyl-5-(1-methylethyl)-2,3,5,6-tetranitro-, nitrate (ester), (1α,2α,5α,6β)- (127420-18-2)
• 4-Cyclohexene-1,3-diol, 2-methyl-5-(1-methylethyl)-2,6-dinitro-, 1-nitrate, (1α,2α,3α,6β)- (127368-12-1)
• 3-Cyclohexen-1-ol, 2-methyl-5-(1-methylethyl)-2,5,6-trinitro-, nitrate (ester), (1α,2α,5β,6β)- (127368-10-9)
• (118297-28-2)
• 4-Cyclohexene-1,3-diol, 2-methyl-5-(1-methylethyl)-2,6-dinitro-, 1-nitrate, (1α,2α,3β,6β)- (127420-20-6)

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