Preparation of 1,2-bis(3,4-dicyanophenoxymethyl)benzene and the binuclear zinc phthalocyanine derived from it
Mendeleev Communications Pub Date: DOI: 10.1070/MC2002v012n03ABEH001573
Abstract
A method of synthesis of 1,2-bis(3,4-dicyanophenoxymethyl)benzene from the 1,2-bis(hydroxymethyl)benzene and 4-nitrophthalodinitrile is developed. Its tetramerization with Zn(OAc)
2
·2H
2
O gives a binuclear zinc phthalocyanine of a new type, containing fouro-phenylidene bridges. The use of microwave heating decreases reaction time and increases yield.
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Journal Name：Mendeleev Communications
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CAS no.: 89640-58-4
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