Solvent-free bromination of 1,3-diketones and β-keto esters with NBS
Green Chemistry Pub Date: 2006-09-05 DOI: 10.1039/B608446J
Abstract
Trituration of N-bromosuccinimide at room temperature with several liquid or solid 1,3-diketones and β-keto esters resulted in high yield conversion to the monobrominated derivatives, and a work-up procedure using only water to remove succinimide was employed. The entire process uses no organic solvent and is therefore more ecologically desirable.
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Journal Name：Green Chemistry
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CAS no.: 89640-58-4
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