Production Method 1

36653-82-4

69-79-4

98064-96-1

Reaction Conditions

1.1R:AcONa
2.1R:PhCH2NH2, S:THF, 6 h, rt
2.2R:AcOH, rt, pH 6-7
3.1R:DBU, S:CH2Cl2, 0°C; 7 h, 0°C
4.1R:BF3-Et2O, S:CH2Cl2, 0°C; 6 h, 0°C
5.1R:NaOMe, S:MeOH, 3 h, rt, pH 10
5.2rt, pH 7

Reference

Solution Properties of Alkyl β-D-Maltosides

By Li, Zhencao et al, Journal of Surfactants and Detergents, 2019, 22(4), 731-742

Production Method 2

36653-82-4

22352-19-8

98064-96-1

Reaction Conditions

1.1R:BF3-Et2O, S:CH2Cl2, 2 h, 0°C; 0°C → rt
2.1R:NaOMe, S:MeOH, 1 h, rt
2.2R:DOWEX 50W, rt, neutralized

Reference

Hydrophobic tail length, degree of fluorination and headgroup stereochemistry are determinants of the biocompatibility of (fluorinated) carbohydrate surfactants

By Li, Xueshu et al, Colloids and Surfaces, 2009, 73(1), 65-74

Production Method 3

36653-82-4

69-79-4

98064-96-1

793668-50-5

Reaction Conditions

1.1R:Acetyl bromide, R:AcOH, S:H2O, 0.5 h, rt
1.2R:FeCl3, S:MeCN, 1 h, rt
1.3R:KBr, S:PhMe, rt
1.4R:NaOMe, S:MeOH, overnight, rt
1.5R:AcOH, S:H2O, rt

Reference

Simple preparations of alkyl and cycloalkyl α-glycosides of maltose, cellobiose, and lactose

By Koto, Shinkiti et al, Carbohydrate Research, 2004, 339(14), 2415-2424

Hexadecyl β-D-maltoside Raw materials

• hexadecan-1-ol
• Octaacetyl-β-maltose
• (2R,3R,4R,5R)-2,3,5,6-tetrahydroxy-4-{(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yloxy}hexanal

Hexadecyl β-D-maltoside Preparation Products

• α-D-Glucopyranoside, hexadecyl 4-O-α-D-glucopyranosyl- (793668-50-5)
• Hexadecyl β-D-maltoside (98064-96-1)

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• Solvents and Organic Chemicals Organic Compounds Lipids and lipid-like molecules Fatty Acyls Fatty acyl glycosides of mono- and disaccharides
• Solvents and Organic Chemicals Organic Compounds Lipids and lipid-like molecules Fatty Acyls Fatty acyl glycosides Fatty acyl glycosides of mono- and disaccharides
• Other Chemical additives Functional Additives

• 95795-78-1(b-D-Glucopyranoside, ethyl 4-O-b-D-galactopyranosyl-)
• 69557-93-3(3-O-alpha-D-Glucopyranosyl-alpha-L-rhamnopyranose)
• 220585-89-7(a-D-Glucopyranose, 6-O-a-D-galactopyranosyl-, hydrate(9CI))
• 93302-26-2(Methyl D-galactopyranoside)
• 6340-52-9(Methyl 6-deoxy-b-D-glucopyranoside)
• 29781-81-5(a-D-Glucopyranoside, decyl)
• 9042-11-9(2-[6-[4,5-Dihydroxy-2-(hydroxymethyl)-6-methoxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(methoxymethyl)oxane-3,4,5-triol)
• 22416-58-6(Xylotetraose)
• 93911-12-7(Tridecyl β-D-maltopyranoside)
• 89821-88-5(a-L-Mannopyranose,6-deoxy-4-O-(3,6-di-O-methyl-b-D-glucopyranosyl)-2,3-di-O-methyl-)