- Process for preparation of L-dabsyltryptophan, China, , ,
Cas no 97685-00-2 (Dabsyl-L-tryptophan)
Dabsyl-L-tryptophan structure
Product Name:Dabsyl-L-tryptophan
CAS No:97685-00-2
MF:C25H25N5O4S
MW:491.56210398674
MDL:MFCD00059700
CID:801321
PubChem ID:87567959
Update Time:2024-10-25
Dabsyl-L-tryptophan Chemical and Physical Properties
Names and Identifiers
-
- L-Tryptophan,N-[[4-[[4-(dimethylamino)phenyl]azo]phenyl]sulfonyl]- (9CI)
- Dabsyl-L-tryptophan
- (2S)-2-[[4-[[4-(dimethylamino)phenyl]diazenyl]phenyl]sulfonylamino]-3-(1H-indol-3-yl)propanoic acid
- 4-Dimethylaminoazobenzene-4'-sulfonyl-L-tryptophan
- D1459
- Dbs-Trp-OH
- N-(4-{(E)-[4-(Dimethylamino)phenyl]diazenyl}benzene-1-sulfonyl)-L-tryptophan
- (S,E)-2-(4-((4-(dimethylamino)phenyl)diazenyl)phenylsulfonamido)-3-(1H-indol-3-yl)propanoic acid
- L-Tryptophan, N-[[4-[[4-(dimethylamino)phenyl]azo]phenyl]sulfonyl]- (9CI)
- L
- N-[[4-[2-[4-(Dimethylamino)phenyl]diazenyl]phenyl]sulfonyl]-L-tryptophan (ACI)
- (2S)-2-{4-[(1E)-2-[4-(dimethylamino)phenyl]diazen-1-yl]benzenesulfonamido}-3-(1H-indol-3-yl)propanoic acid
- CS-0201858
- XDA68500
- DTXSID30555053
- Dabsyl-L-tryptophan (Dbs-L-Trp-OH)
- MFCD00059700
- SGKGZXUAHWJTIA-DEOSSOPVSA-N
- 97685-00-2
- D89863
-
- MDL： MFCD00059700
- Inchi： 1S/C25H25N5O4S/c1-30(2)20-11-7-18(8-12-20)27-28-19-9-13-21(14-10-19)35(33,34)29-24(25(31)32)15-17-16-26-23-6-4-3-5-22(17)23/h3-14,16,24,26,29H,15H2,1-2H3,(H,31,32)/t24-/m0/s1
- InChI Key： SGKGZXUAHWJTIA-DEOSSOPVSA-N
- SMILES： C(C1=CNC2C=CC=CC1=2)[C@@H](C(=O)O)NS(C1C=CC(N=NC2C=CC(N(C)C)=CC=2)=CC=1)(=O)=O
Computed Properties
- Exact Mass: 491.16300
- Monoisotopic Mass: 491.16272547g/mol
- Isotope Atom Count: 0
- Hydrogen Bond Donor Count: 3
- Hydrogen Bond Acceptor Count: 8
- Heavy Atom Count: 35
- Rotatable Bond Count: 9
- Complexity: 829
- Covalently-Bonded Unit Count: 1
- Defined Atom Stereocenter Count: 1
- Undefined Atom Stereocenter Count : 0
- Defined Bond Stereocenter Count: 0
- Undefined Bond Stereocenter Count: 0
- XLogP3: 3.8
- Topological Polar Surface Area: 136
Experimental Properties
- Density: 1.353
- Boiling Point: 766.94°C at 760 mmHg
- Flash Point: 417.63°C
- Refractive Index: 1.665
- PSA: 135.60000
- LogP: 6.09520
Dabsyl-L-tryptophan Pricemore >>
| Related Categories | No. | Product Name | Cas No. | Purity | Specification | Price | update time | Inquiry |
|---|---|---|---|---|---|---|---|---|
| SHANG HAI MAI KE LIN SHENG HUA Technology Co., Ltd. | D869835-10mg |
Dabsyl-L-tryptophan |
97685-00-2 | 98% | 10mg |
￥99.00 | 2022-01-11 | |
| SHANG HAI XIAN DING Biotechnology Co., Ltd. | D1459-100mg |
Dabsyl-L-tryptophan |
97685-00-2 | 98.0%(LC) | 100mg |
￥310.0 | 2022-05-30 | |
| abcr | AB171263-100 mg |
Dabsyl-L-tryptophan (Dbs-L-Trp-OH); . |
97685-00-2 | 100 mg |
€177.80 | 2023-07-20 | ||
| SHANG HAI A LA DING SHENG HUA KE JI GU FEN Co., Ltd. | D155330-100MG |
Dabsyl-L-tryptophan |
97685-00-2 | >98.0%(HPLC) | 100MG |
￥594.00 | 2021-05-21 | |
| SHANG HAI A LA DING SHENG HUA KE JI GU FEN Co., Ltd. | D155330-10mg |
Dabsyl-L-tryptophan |
97685-00-2 | >98.0%(HPLC) | 10mg |
￥115.00 | 2021-05-21 | |
| TI XI AI ( SHANG HAI ) HUA CHENG GONG YE FA ZHAN Co., Ltd. | D1459-100MG |
Dabsyl-L-tryptophan |
97685-00-2 | >98.0%(HPLC) | 100mg |
￥310.00 | 2024-04-15 | |
| SHANG HAI A LA DING SHENG HUA KE JI GU FEN Co., Ltd. | D155330-500mg |
Dabsyl-L-tryptophan |
97685-00-2 | 98% | 500mg |
￥1349.90 | 2023-09-03 | |
| Aaron | AR003PX3-100mg |
Dabsyl-L-tryptophan |
97685-00-2 | 98% | 100mg |
$50.00 | 2025-01-22 | |
| Aaron | AR003PX3-500mg |
Dabsyl-L-tryptophan |
97685-00-2 | 98% | 500mg |
$221.00 | 2025-01-22 | |
| 1PlusChem | 1P003POR-100mg |
Dabsyl-L-tryptophan |
97685-00-2 | ≥98% | 100mg |
$128.00 | 2025-02-20 |
Dabsyl-L-tryptophan Production Method
Production Method 1
Reaction Conditions
1.1 Reagents: Triethylamine Solvents: Dichloromethane ; 0 °C; overnight, 25 °C
2.1 Reagents: Potassium hydroxide Solvents: Methanol , Water ; 0 °C; overnight, reflux
2.2 Reagents: Hydrochloric acid Solvents: Water ; pH 3
2.1 Reagents: Potassium hydroxide Solvents: Methanol , Water ; 0 °C; overnight, reflux
2.2 Reagents: Hydrochloric acid Solvents: Water ; pH 3
Reference
Production Method 2
Reaction Conditions
1.1 Reagents: Phosphorus oxychloride ; 100 °C
2.1 Reagents: Triethylamine Solvents: Dichloromethane ; 0 °C; overnight, 25 °C
3.1 Reagents: Potassium hydroxide Solvents: Methanol , Water ; 0 °C; overnight, reflux
3.2 Reagents: Hydrochloric acid Solvents: Water ; pH 3
2.1 Reagents: Triethylamine Solvents: Dichloromethane ; 0 °C; overnight, 25 °C
3.1 Reagents: Potassium hydroxide Solvents: Methanol , Water ; 0 °C; overnight, reflux
3.2 Reagents: Hydrochloric acid Solvents: Water ; pH 3
Reference
- Process for preparation of L-dabsyltryptophan, China, , ,
Production Method 3
Reaction Conditions
1.1 Reagents: Potassium hydroxide Solvents: Methanol , Water ; 0 °C; overnight, reflux
1.2 Reagents: Hydrochloric acid Solvents: Water ; pH 3
1.2 Reagents: Hydrochloric acid Solvents: Water ; pH 3
Reference
- Process for preparation of L-dabsyltryptophan, China, , ,
Production Method 4
Reaction Conditions
Reference
- Comparison of reverse-phase high-performance liquid chromatographic methods for precolumn-derivatized amino acidsMcClung, G.; et al, Journal of Liquid Chromatography, 1988, 11(3), 613-46
Production Method 5
Reaction Conditions
Reference
- Analyses of dansyl and dabsyl amino acids by reverse-phase high-performance liquid chromatographyHigh purity amino acid derivativesMuramoto, Koji; et al, Nippon Suisan Gakkaishi, 1985, 51(5), 817-24
Dabsyl-L-tryptophan Raw materials
- N-[[4-[2-[4-(Dimethylamino)phenyl]diazenyl]phenyl]sulfonyl]-L-tryptophan methyl ester
- Dabsyl chloride
- L-Tryptophan
- Methyl orange
- L-tryptophan methyl ester hydrochloride
Dabsyl-L-tryptophan Preparation Products
Dabsyl-L-tryptophan Related Literature
-
Luis Miguel Azofra,Douglas R. MacFarlane,Chenghua Sun Chem. Commun., 2016,52, 3548-3551
-
James D. Kirkham,Patrick M. Delaney,George J. Ellames,Eleanor C. Row,Joseph P. A. Harrity Chem. Commun., 2010,46, 5154-5156
-
Eunhak Lim,Jiyoung Heo,Seong Keun Kim Nanoscale, 2019,11, 11369-11378
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