Production Method 1

7325-14-6

97443-80-6

Reaction Conditions

1.1 Reagents: N-Bromosuccinimide Solvents: Acetonitrile ,  Dichloromethane ;  30 min, 0 °C; 0 °C → rt; 12 h, rt

Reference

Chemically amplified resist composition and pattern forming process having high resolution and minimal line edge roughness

, United States, , ,

Production Method 2

108-85-0

97443-80-6

Reaction Conditions

1.1 Reagents: Aluminum chloride ;  5 min, -40 °C; 30 min, -40 °C → rt
1.2 Reagents: Sodium bicarbonate Solvents: Hexane ,  Water
1.3 Reagents: Bromine Solvents: Trimethyl phosphate ;  5 min, 70 °C; 1.5 h, 70 °C

Reference

Enantioselective Synthesis of Highly Substituted Furans by a Copper(II)-Catalyzed Cycloisomerization-Indole Addition Reaction

Rauniyar, Vivek; Wang, Z. Jane; Burks, Heather E.; Toste, F. Dean, Journal of the American Chemical Society, 2011, 133(22), 8486-8489

Production Method 3

7325-14-6

97443-80-6

Reaction Conditions

1.1 Reagents: Bromine Solvents: Chloroform ;  0 °C; 0 °C → rt; 20 h, rt

Reference

Direct catalytic asymmetric synthesis of α-chiral bicyclo[1.1.1]pentanes

Wong, Marie L. J.; Sterling, Alistair J. ; Mousseau, James J.; Duarte, Fernanda ; Anderson, Edward A., Nature Communications, 2021, 12(1),

Production Method 4

7325-14-6

97443-80-6

Reaction Conditions

Reference

Mesomeric dipole moments. VII. Secondary steric effects in 2,4,6-trialkylated acetophenones and nitrobenzenes: dipole moments and carbon-13 NMR spectra

Koudelka, Juraj; Saman, David; Exner, Otto, Collection of Czechoslovak Chemical Communications, 1985, 50(1), 208-14

Production Method 5

7325-14-6

97443-80-6

Reaction Conditions

1.1 Reagents: Bromine Solvents: Chloroform ;  15 min, 0 °C; 0 °C → 40 °C; 3 h, 40 °C

Reference

An Alternative Synthesis of Cycloalkyl-Substituted CPA Catalysts and Application in Asymmetric Protonation Reactions

McLean, Liam A. ; Watson, Allan J. B., European Journal of Organic Chemistry, 2021, 2021(35), 4943-4945

Production Method 6

7325-14-6

97443-80-6

Reaction Conditions

1.1 Reagents: Bromine Solvents: Chloroform ;  10 min, rt → 0 °C; 0 °C → rt; 2 h, rt
1.2 Reagents: Sodium sulfite Solvents: Dichloromethane ,  Water ;  rt

Reference

Enantioselective Halogenative Semi-Pinacol Rearrangement: Extension of Substrate Scope and Mechanistic Investigations

Romanov-Michailidis, Fedor; Romanova-Michaelides, Maria; Pupier, Marion; Alexakis, Alexandre, Chemistry - A European Journal, 2015, 21(14), 5561-5583

Production Method 7

7325-14-6

97443-80-6

Reaction Conditions

1.1 Reagents: Bromine Solvents: Chloroform ;  10 min, 0 °C; 0 °C → rt; 2 h, rt
1.2 Reagents: Sodium sulfite Solvents: Dichloromethane ,  Water

Reference

Enantioselective Organocatalytic Fluorination-Induced Wagner-Meerwein Rearrangement

Romanov-Michailidis, Fedor; Guenee, Laure; Alexakis, Alexandre, Angewandte Chemie, 2013, 52(35), 9266-9270

Production Method 8

7325-14-6

97443-80-6

Reaction Conditions

1.1 Reagents: Bromine Solvents: Chloroform ;  15 min, 0 °C; 0 °C → rt; 2 h, rt

Reference

A New Biarylphosphine Ligand for the Pd-Catalyzed Synthesis of Diaryl Ethers under Mild Conditions

Salvi, Luca; Davis, Nicole R.; Ali, Siraj Z.; Buchwald, Stephen L., Organic Letters, 2012, 14(1), 170-173

Production Method 9

7325-14-6

97443-80-6

Reaction Conditions

1.1 Reagents: Bromine Solvents: Chloroform ;  2 h, 0 °C

Reference

Organocatalytic Kinetic Resolution of Sulfoximines

Dong, Shunxi; Frings, Marcus; Cheng, Hanchao; Wen, Jian; Zhang, Duo; et al, Journal of the American Chemical Society, 2016, 138(7), 2166-2169

1-Bromo-2,4,6-tricyclohexylbenzene Raw materials

• Bromocyclohexane
• 1,3,5-tricyclohexylbenzene

1-Bromo-2,4,6-tricyclohexylbenzene Preparation Products

• 1-Bromo-2,4,6-tricyclohexylbenzene (97443-80-6)

• 1. An algal process treatment combined with the Fenton reaction for high concentrations of amoxicillin and cefradine
  Haitao Li,Yu Pan,Zhizhi Wang,Shan Chen,Ruixin Guo,Jianqiu Chen RSC Adv., 2015,5, 100775-100782
• 2. An Appraisal of pH triggered Bacitracin drug release, through composite hydrogel systems
  RabailGul,MariamMir,MurtazaNAli
• 3. An automatic determination of thoria in thoria-urania mixtures
  Analyst, 1966,91, 208-210
• 4. An amorphous carbon nitride/NiO/CoN-based composite: a highly efficient nonprecious electrode for supercapacitors and the oxygen evolution reaction?
  Huifang Yang,Haoran Guo,Peidong Fan,Xinpan Li,Wenlu Ren,Rui Song Nanoscale, 2020,12, 7024-7034
• 5. An atom efficient route to N-aryl and N-alkyl pyrrolines by transition metal catalysis?
  Supaporn Sawadjoon,Joseph S. M. Samec Org. Biomol. Chem., 2011,9, 2548-2554

• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Bromobenzenes
• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Halobenzenes Bromobenzenes

• 825644-12-0(Benzene, 1-bromo-2,4-bis(1-ethylpropyl)-)
• 255710-07-7(Benzene, 1,4-dibromo-2,5-bis(2-ethylhexyl)-)
• 59734-85-9(1-Bromo-2-(sec-butyl)benzene)
• 61592-95-8(Benzene, 1-bromo-2-(1,1-dimethyl-2-phenylpropyl)-)
• 7462-26-2( )
• 825644-14-2(Benzene, 2-bromo-1,3,5-tris(1-ethylpropyl)-)
• 825644-13-1(Benzene, 2-bromo-1,4-bis(1-ethylpropyl)-)
• 59734-92-8(1-Bromo-2-cyclohexylbenzene)
• 61592-94-7(Benzene, 1-bromo-2-(1,2-dimethyl-2-phenylpropyl)-)
• 344340-82-5(Benzene, 1-bromo-2-[(1R,2R)-2-phenylcyclopropyl]-, rel-)