Production Method 1

3458-28-4

98-88-4

96996-90-6

Reaction Conditions

1.1 Reagents: Pyridine

Reference

2-Methyl-5-tert-butylthiophenol

Picard, Sebastien, e-EROS Encyclopedia of Reagents for Organic Synthesis, 2011, , 1-2

Production Method 2

3458-28-4

98-88-4

96996-90-6

Reaction Conditions

1.1 Reagents: Pyridine ;  rt → 0 °C; 30 min, 0 °C; 0 °C → rt; 12 h, rt

Reference

Automated synthesis of lipo-mannan backbone α(1-6) oligomannoside via glycosyl phosphates: glycosyl tricyclic orthoesters revisited

Liu, Xinyu; Wada, Reiko; Boonyarattanakalin, Siwarutt; Castagner, Bastien; Seeberger, Peter H., Chemical Communications (Cambridge, 2008, (2008), 3510-3512

Production Method 3

96996-90-6

Reaction Conditions

Reference

Synthesis of a Glycosylphosphatidylinositol (GPI) Fragment as a Potential Substrate for Mannoprotein Transglycosidases

Belz, Tyson F., Synlett, 2021, 32(20), 2053-2058

Production Method 4

96996-90-6

Reaction Conditions

Reference

Fragments of biopolymers containing glycosyl phosphate residues. 5. Synthesis of benzyl 2-O- and methyl 4-O-α-D-mannosylphospho-β-D-galactosides and methyl 4-O-α-D-mannosylphospho-α-D-glucoside by hydrogen phosphonate method

Nikolaev, A. V.; Ivanova, I. A.; Shibaev, V. N.; Kochetkov, N. K., Bioorganicheskaya Khimiya, 1990, 16(8), 1105-17

Production Method 5

3458-28-4

98-88-4

96996-90-6

Reaction Conditions

1.1 Reagents: 4-(Dimethylamino)pyridine Solvents: Pyridine ;  6 h, rt
1.2 Reagents: Hydrochloric acid Solvents: Water

Reference

Etiocholanolone and dehydroepiandrosterone glycosylated derivatives useful in treatment of cancer and their preparation

, China, , ,

Production Method 6

3458-28-4

98-88-4

96996-90-6

Reaction Conditions

1.1 Reagents: Triethylamine Catalysts: 4-(Dimethylamino)pyridine Solvents: Dichloromethane ;  0 °C; 24 h, rt
1.2 Reagents: Methanol ;  cooled

Reference

Glycoprotein Mimics with Tunable Functionalization through Global Amino Acid Substitution and Copper Click Chemistry

Seifried, Brian M.; Qi, Wenjing; Yang, Yun Jung; Mai, Danielle J. ; Puryear, Wendy B.; et al, Bioconjugate Chemistry, 2020, 31(3), 554-566

Production Method 7

3458-28-4

98-88-4

96996-90-6

Reaction Conditions

1.1 Catalysts: 4-(Dimethylamino)pyridine Solvents: Pyridine

Reference

Synthesis of four 11-deoxoglycyrrhetinic acid 3,30-bisdesmosides

Wang, Jun; Wen, Weihe; Hu, Xiaoli; Zhu, Yuliang, Nanjing Gongye Daxue Xuebao, 2012, 34(1), 130-134

Production Method 8

3458-28-4

98-88-4

96996-90-6

Reaction Conditions

1.1 Solvents: Pyridine ;  overnight, 0 °C → rt

Reference

Sugar/Steroid/Sugar Conjugates: Sensitivity of Lipid Binding to Sugar Structure

Mbadugha, Bessie N. A.; Menger, Fredric M., Organic Letters, 2003, 5(22), 4041-4044

Production Method 9

50-99-7

98-88-4

96996-90-6

Reaction Conditions

1.1 Solvents: Pyridine ;  0 °C; overnight, rt
1.2 Reagents: Water ;  cooled

Reference

Synthesis of 12-O-Mono- and Diglycosyl-oxystearates, a New Class of Agonists for the C-type Lectin Receptor Mincle

Van Huy, Le; Tanaka, Chiaki; Imai, Takashi; Yamasaki, Sho; Miyamoto, Tomofumi, ACS Medicinal Chemistry Letters, 2019, 10(1), 44-49

Production Method 10

3458-28-4

98-88-4

96996-90-6

Reaction Conditions

1.1 Reagents: Pyridine Solvents: Dimethylformamide ,  Dichloromethane

Reference

Cross Metathesis Assisted Solid-Phase Synthesis of Glycopeptoids

Khan, Sharaf Nawaz; Kim, Arim; Grubbs, Robert H.; Kwon, Yong-Uk, Organic Letters, 2012, 14(12), 2952-2955

Production Method 11

96996-90-6

Reaction Conditions

Reference

Sugar derivative and sugar-nucleic acid conjugate

, World Intellectual Property Organization, , ,

Production Method 12

96996-90-6

Reaction Conditions

Reference

Stereospecific mannosylations of myo-inositol: synthesis of manno-myo-inositol fragment of Mycobacterium tuberculosis

Mereyala, Hari Babu; Gaddam, Bapu Reddy, Proceedings - Indian Academy of Sciences, 1994, 106(5), 1225-30

Production Method 13

96996-90-6

Reaction Conditions

Reference

Studies Related to Synthesis of Glycophosphatidylinositol Membrane-Bound Protein Anchors. 5. n-Pentenyl Ortho Esters for Mannan Components

Roberts, Carmichael; Madsen, Robert; Fraser-Reid, Bert, Journal of the American Chemical Society, 1995, 117(5), 1546-53

Production Method 14

96996-90-6

Reaction Conditions

Reference

Blood-brain penetration of 5-hydroxytryptamine derivatives

Fillion, G.; Dupraz, B.; Prudhomme, N.; Huynh-Dinh, T., Bioorganic & Medicinal Chemistry Letters, 1994, 4(12), 1485-90

1,2,3,4,6-Penta-O-benzoyl-D-mannopyranose Raw materials

• D(+)-Glucose
• D(+)-Mannose
• Benzoyl chloride

1,2,3,4,6-Penta-O-benzoyl-D-mannopyranose Preparation Products

• 1,2,3,4,6-Penta-O-benzoyl-D-mannopyranose (96996-90-6)

• 1. Emerging investigator series: heterogeneous reactions of sulfur dioxide on mineral dust nanoparticles: from single component to mixed components?
  Tao Wang,Yangyang Liu,Yue Deng,Hongbo Fu,Jianmin Chen Environ. Sci.: Nano, 2018,5, 1821-1833
• 2. Evolution in surface coverage of CH3NH3PbI3?XClXvia heat assisted solvent vapour treatment and their effects on photovoltaic performance of devices
  Dhirendra K. Chaudhary,Pramendra Kumar,Lokendra Kumar RSC Adv., 2016,6, 94731-94738
• 3. Excited state potential energy surfaces and their interactions in FeIVO active sites
  Shaun D. Wong,Edward I. Solomon Dalton Trans., 2014,43, 17567-17577
• 4. Examination of ammonia–poly(pyrrole) interactions by piezoelectric and conductivity measurements
  Analyst, 1991,116, 1125-1130
• 5. Estimation of activation energy for electroporation and pore growth rate in liquid crystalline and gel phases of lipid bilayers using molecular dynamics simulations?
  Amit Kumar Majhi,Subbarao Kanchi,V. Venkataraman,K. G. Ayappa,Prabal K. Maiti Soft Matter, 2015,11, 8632-8640

• Solvents and Organic Chemicals Organic Compounds Organic acids and derivatives Carboxylic acids and derivatives Pentacarboxylic acids and derivatives

• 12738-64-6(sucrose benzoate)
• 9004-35-7(Cellulose acetate)
• 2098070-20-1(2-(3-(Pyridin-3-yl)-1H-pyrazol-1-yl)acetimidamide)
• 2680771-01-9(4-cyclopentyl-3-{(prop-2-en-1-yloxy)carbonylamino}butanoic acid)
• 1444113-98-7(N-(3-cyanothiolan-3-yl)-2-[(2,2,2-trifluoroethyl)sulfanyl]pyridine-4-carboxamide)
• 332062-08-5(Fmoc-S-3-amino-4,4-diphenyl-butyric acid)
• 1270529-38-8(1,2,3,4,5,6-Hexahydro-[2,3]bipyridinyl-6-ol)
• 941977-17-9(N'-(3-chloro-2-methylphenyl)-N-2-(dimethylamino)-2-(naphthalen-1-yl)ethylethanediamide)
• 2138166-62-6(2,2-Difluoro-3-[methyl(2-methylbutyl)amino]propanoic acid)
• 89640-58-4(2-Iodo-4-nitrophenylhydrazine)