Production Method 1

394-50-3

96994-70-6

Reaction Conditions

1.1 Reagents: Potassium carbonate Solvents: Dimethylformamide ;  rt → 50 °C; overnight, 50 °C; 50 °C → rt
1.2 Reagents: 3-Chlorobenzoic acid ,  m-Chloroperbenzoic acid Solvents: Dichloromethane ,  Water ;  overnight, rt
1.3 Reagents: Triethylamine Solvents: Methanol ;  rt; 2 - 12 h, rt

Reference

A mild meta-selective C-H alkylation of catechol mono-ethers

Vitaku, Edon; Njardarson, Jon T., European Journal of Organic Chemistry, 2016, 2016(22), 3679-3683

Production Method 2

845829-94-9

96994-70-6

Reaction Conditions

1.1 Reagents: Butyllithium Solvents: Tetrahydrofuran ,  Hexane ;  -75 °C; 30 min, -75 °C
1.2 Reagents: Trimethyl borate ;  5 min, -75 °C
1.3 Reagents: Acetic acid ,  Hydrogen peroxide Solvents: Water ;  30 min, 0 °C; 3 h, rt

Reference

Phenyl acetate derivatives, fluorine-substituted on the phenyl group, as rapid recovery hypnotic agents with reflex depression

Zhang, Heng; Xu, Xiangqing; Chen, Yin; Qiu, Yinli; Liu, Xin; et al, European Journal of Medicinal Chemistry, 2015, 89, 524-539

Production Method 3

74266-68-5

96994-70-6

Reaction Conditions

1.1 Reagents: m-Chloroperbenzoic acid Solvents: Dichloromethane ;  12 h, heated

Reference

The Baeyer-Villiger oxidation of ketones and aldehydes

Krow, Grant R., Organic Reactions (Hoboken, 1993, (1993),

Production Method 4

74266-68-5

96994-70-6

Reaction Conditions

1.1 Reagents: m-Chloroperbenzoic acid Solvents: Dichloromethane

Reference

A new synthesis of 3-fluoroveratrole and 2-fluoro-3,4-dimethoxybenzaldehyde

Ladd, David L.; Gaitanopoulos, Dimitri; Weinstock, Joseph, Synthetic Communications, 1985, 15(1), 61-9

3-Fluoro-2-methoxyphenol Raw materials

• 3-fluoro-2-hydroxybenzaldehyde
• 3-Fluoro-2-methoxybenzaldehdye
• 1-bromo-3-fluoro-2-methoxybenzene

3-Fluoro-2-methoxyphenol Preparation Products

• 3-Fluoro-2-methoxyphenol (96994-70-6)

• 1. An intensified π-hole in beryllium-doped boron nitride meshes: its determinant role in CO2 conversion into hydrocarbon fuels?
  Luis Miguel Azofra,Douglas R. MacFarlane,Chenghua Sun Chem. Commun., 2016,52, 3548-3551
• 2. An artificial photosynthetic system for photoaccumulation of two electrons on a fused dipyridophenazine (dppz)–pyridoquinolinone ligand?
  Philipp Traber,Stephan Kupfer,Stefanie Gr?fe,Isabelle Baussanne,Martine Demeunynck,Jean-Marie Mouesca,Serge Gambarelli,Vincent Artero,Murielle Chavarot-Kerlidou Chem. Sci., 2018,9, 4152-4159
• 3. An amide probe as a selective Al3+ and Fe3+ sensor inside the HeLa and a549 cell lines: Pictet–Spengler reaction for the rapid detection of tryptophan amino acid?
  Bidyut Kumar Kundu,Rinky Singh,Ritudhwaj Tiwari,Debasis Nayak New J. Chem., 2019,43, 4867-4877
• 4. An algal process treatment combined with the Fenton reaction for high concentrations of amoxicillin and cefradine
  Haitao Li,Yu Pan,Zhizhi Wang,Shan Chen,Ruixin Guo,Jianqiu Chen RSC Adv., 2015,5, 100775-100782
• 5. Acenaphthenic hopanoids, a novel series of aromatised
  Teresita Carrillo-Hernández,Philippe Schaeffer,Pierre Albrecht Chem. Commun., 2001, 1976-1977

• Solvents and Organic Chemicals Organic Compounds Benzenoids Phenols Methoxyphenols

• 394-64-9(1-Fluoro-2,3-dimethoxybenzene)
• 73943-41-6(2-Fluoro-6-methoxyphenol)
• 642-22-8(BENZENE, 1,2,3,4-TETRAFLUORO-5,6-DIMETHOXY-)
• 1208078-31-2(4-Fluoro-2,5-dimethoxyphenol)
• 158626-90-5(3,4-Difluoro-2-methoxyphenol)
• 92170-43-9(Benzene,2,3-diethoxy-1,4-difluoro-)
• 96631-22-0(Benzene,2,3-diethoxy-1,4-difluoro-)
• 75626-22-1(3,6-Difluoroguaiacol)
• 1193392-90-3(2,4-Difluoro-6-methoxyphenol)
• 152434-94-1(3,5-Difluoro-2-methoxyphenol)