Production Method 1

96-11-7

Reaction Conditions

1.1 Reagents: Bromine Solvents: Carbon tetrachloride ;  -5 °C; 30 min, -5 °C → rt

Reference

Ynamide Carbopalladation: A Flexible Route to Mono-, Bi- and Tricyclic Azacycles

Campbell, Craig D.; Greenaway, Rebecca L.; Holton, Oliver T.; Walker, P. Ross; Chapman, Helen A.; et al, Chemistry - A European Journal, 2015, 21(36), 12627-12639

Production Method 2

96-11-7

Reaction Conditions

1.1 Reagents: Bromine Solvents: Carbon tetrachloride

Reference

1,2,3-Tribromopropane

Johnson, John R.; McEwen, W. L., Organic Syntheses, 1925, , 99-101

Production Method 3

96-11-7

Reaction Conditions

1.1 Reagents: 2409021-39-0 Solvents: Dichloromethane ;  30 min, rt

Reference

Synthesis, crystal structure, Hirshfeld surface analysis, DFT calculations and characterization of 1,3-propanediylbis(triphenylphosphonium) monotribromide as brominating agent of double bonds and phenolic rings

Nokhbeh, Seyed Reza; Gholizadeh, Mostafa ; Salimi, Alireza ; Sparkes, Hazel A., Journal of Molecular Structure, 2020, 1206,

Production Method 4

96-11-7

Reaction Conditions

1.1 Reagents: Phosphonium, (3-bromopropyl)triphenyl-, (tribromide) (1:1) Solvents: Dichloromethane ;  rt; 0.5 h, rt

Reference

Crystal structure, characterization, Hirshfeld surface analysis and DFT studies of two [propane 3-bromo-1-(triphenyl phosphonium)] cations containing bromide (I) and tribromide (II) anions: The anion (II) as a new brominating agent for unsaturated compounds

Nokhbeh, Seyed Reza; Gholizadeh, Mostafa ; Salimi, Alireza ; Sparkes, Hazel A., Journal of Molecular Structure, 2019, 1195, 542-554

Production Method 5

930-40-5

96-11-7

Reaction Conditions

Reference

Halogenation of silylated cyclopropyl derivatives; a convenient synthesis of iodocyclopropane

Grignon-Dubois, Micheline; Dunogues, Jacques; Calas, Raymond, Journal of Chemical Research, 1979, (1), 6-7

Production Method 6

56-81-5

96-11-7

Reaction Conditions

1.1 Reagents: Phosphorus tribromide ;  1 h, 0 °C; rt; 1 h, 60 °C

Reference

Pd-based mesoporous silica catalyst for synthesis of alkanes

, India, , ,

Production Method 7

56-81-5

96-11-7

Reaction Conditions

1.1 Reagents: Phosphorus tribromide ;  1 h, 0 °C; 0 °C → rt; 1 h, 60 °C

Reference

A novel route for the synthesis of alkanes from glycerol in a two step process using a Pd/SBA-15 catalyst

Udayakumar, V.; Pandurangan, A., RSC Advances, 2015, 5(96), 78719-78727

Production Method 8

56-81-5

96-11-7

Reaction Conditions

1.1 Reagents: Sodium bromide ,  Sulfuric acid Solvents: Water ;  cooled; 4 - 5 h, reflux

Reference

Two-component epoxy resin adhesives containing modified polythiols as curing agents and the preparation methods therefor

, China, , ,

Production Method 9

42568-28-5

96-11-7

Reaction Conditions

1.1 Reagents: N-Bromoacetamide Solvents: Dichloromethane

Reference

Homolytic displacement at carbon centers. XII. Regiospecific formation of N-allyl and N-cyclopropylcarbinyl sulfonamides and of allyl and cyclopropyl halides in the reaction of N-halo compounds with organocobaloximes

Johnson, Michael D.; Lampman, Gary M.; Koops, Roger W.; Das Gupta, B., Journal of Organometallic Chemistry, 1987, 326(2), 281-8

Production Method 10

96-11-7

Reaction Conditions

1.1 Reagents: Bromine

Reference

New method of preparing propargyl ether

Kurginyan, K. A.; Kalaidzhyan, A. E.; Arakelova, S. V., Armyanskii Khimicheskii Zhurnal, 1986, 39(8), 529-30

Production Method 11

15796-91-5

96-11-7

Reaction Conditions

1.1 Catalysts: Allyl bromide

Reference

Studies on amines and ammonium compounds. CLXXIV. Bromination of unsaturated compounds with complexes formed between bromine and 1,4-bis(trialkylammonium)-2-butene dihalides

Gyul'nazaryan, A. Kh.; Khachatryan, N. G.; Saakyan, T. A.; Churkina, N. P.; Babayan, A. T., Armyanskii Khimicheskii Zhurnal, 1984, 37(1), 29-33

Production Method 12

96-11-7

Reaction Conditions

1.1 Reagents: Bromine Solvents: Perfluorohexane

Reference

Perfluorohexane as a novel reaction medium for bromination reactions

Pereira, Suzanne; Savage, G. Paul; Simpson, Gregory W., Synthetic Communications, 1995, 25(7), 1023-6

Production Method 13

96-11-7

Reaction Conditions

1.1 Reagents: Bromine Solvents: Carbon tetrachloride ;  2 h, 30 °C

Reference

Copper-Catalyzed Allylation of α,α-Difluoro-Substituted Organozinc Reagents

Zemtsov, Artem A.; Kondratyev, Nikolay S.; Levin, Vitalij V.; Struchkova, Marina I.; Dilman, Alexander D., Journal of Organic Chemistry, 2014, 79(2), 818-822

Production Method 14

96-11-7

Reaction Conditions

1.1 Reagents: 1,4-Dioxane, compd. with bromine (1:1) ;  0 - 5 °C; 0 °C → rt; 10 min, rt
1.2 Reagents: Water ;  cooled

Reference

Dioxane dibromide-mediated solvent-free synthesis of vicinal dibromides

Chaudhuri, Subrata Kumar; Roy, Sanchita; Saha, Manabendra; Bhar, Sanjay, Synthetic Communications, 2007, 37(2), 271-274

Production Method 15

56-81-5

96-11-7

Reaction Conditions

1.1 Reagents: Phosphorus tribromide Solvents: Dimethylformamide ;  25 °C; 20 min, 25 °C; 25 °C → 120 °C; 12 h, 120 °C
1.2 Reagents: Sodium hydroxide Solvents: Water ;  pH 8, 0 °C

Reference

Hyperbranched polyamine carbon dioxide absorbent and preparation method thereof

, China, , ,

Production Method 16

56-81-5

96-11-7

Reaction Conditions

Reference

Synthesis of triglycerides from 1,3-dibromopropan-2-ol

Bhati, Asharam; Hamilton, Richard J.; Steven, David A.; Aneja, Rajender; Padley, Frederick B., Journal of the Chemical Society, 1983, (10), 1553-8

Production Method 17

140200-30-2

96-11-7

1306747-56-7

Reaction Conditions

1.1 25 h, 145 - 155 °C; cooled; rt

Reference

Reaction of polyfluoroarenesulfonyl bromides with allyl bromide. Synthesis of allyl polyfluoroaryl sulfones

Bredikhin, R. A.; Maksimov, A. M.; Platonov, V. E., Russian Journal of Organic Chemistry, 2011, 47(3), 374-378

Production Method 18

96-11-7

Reaction Conditions

1.1 Reagents: Bromine Solvents: Dichloromethane ;  2 - 2.5 h, 0 °C; 0 °C → 20 °C
1.2 Reagents: Sodium thiosulfate Solvents: Water

Reference

Brominated flame retardants and polyurethanes containing the same

, World Intellectual Property Organization, , ,

Production Method 19

96-11-7

Reaction Conditions

Reference

1,2-Dibromo-2-cyano-2-(heterocyclic)alkane compounds and their antimicrobial use

, United States, , ,

Production Method 20

96-11-7

Reaction Conditions

Reference

1,2-Dibromo-2-cyano-(substituted)-alkane antimicrobial compounds

, United States, , ,

1,2,3-Tribromopropane Raw materials

• Cobalt, bis[[2,3-butanedione di(oximato-κN)](1-)]-2-propenyl(pyridine)-, (OC-6-12)- (9CI)
• Silane, cyclopropyltrimethyl-
• Benzenesulfonyl bromide, pentafluoro-
• Glycerol
• 2-Butene-1,4-diaminium, N1,N1,N1,N4,N4,N4-hexamethyl-, bromide (1:2)

1,2,3-Tribromopropane Preparation Products

• 1,2,3-Tribromopropane (96-11-7)
• 1,2,3,4,5-Pentafluoro-6-(2-propen-1-ylsulfonyl)benzene (1306747-56-7)

• 1. Evolution of calcium phosphate precipitation in hanging drop vapor diffusion by in situRaman microspectroscopy
  Gloria Belén Ramírez-Rodríguez,José Manuel Delgado-López,Jaime Gómez-Morales CrystEngComm, 2013,15, 2206-2212
• 2. Evidence for the intrinsic nature of band-gap states electrochemically observed on atomically flat TiO2(110) surfaces?
  Shintaro Takata,Yoshihiro Miura Phys. Chem. Chem. Phys., 2014,16, 24784-24789
• 3. Dissolved oxygen sensor based on fluorescence quenching of oxygen-sensitive ruthenium complexes immobilized in sol–gel-derived porous silica coatings
  Analyst, 1996,121, 785-788
• 4. Enabling high-throughput single-animal gene-expression studies with molecular and micro-scale technologies
  Jason Wan Lab Chip, 2020,20, 4528-4538
• 5. Fe(ii)-Assisted one-pot synthesis of ultra-small core–shell Au–Pt nanoparticles as superior catalysts towards the HER and ORR?
  Yi Cao,Yujiao Xiahou,Lixiang Xing,Xiang Zhang,Hong Li,ChenShou Wu,Haibing Xia Nanoscale, 2020,12, 20456-20466

• Solvents and Organic Chemicals Organic Compounds Organohalogen compounds Organobromides Organobromides
• Solvents and Organic Chemicals Organic Compounds Organohalogen compounds Organobromides
• Solvents and Organic Chemicals Organic Compounds Organic Halides

• 286013-06-7(Propane-2-13C,1,3-dibromo- (9CI))
• 51209-47-3((±)-1,2-Dibromopropane-d6)
• 120404-22-0(1,3-Dibromopropane-d6)
• 16837-83-5(Cyclopropane, 1,2-dibromo-, (1R,2R)-rel-)
• 101916-69-2(1,2-Dibromopropane)
• 66236-50-8(Cyclopropane, 1,2-dibromo-, cis-)
• 78-75-1(1,2-Dibromopropane)
• 19533-50-7(1,2-Dibromocyclopropane)
• 64528-94-5(1,3-Dibromopropane-d4)
• 101916-65-8(Propane, 1,2-dibromo-, (2S)- (9CI))