Production Method 1

24424-99-5

95932-39-1

95932-40-4

Reaction Conditions

1.1 Solvents: Benzene ;  8 h, reflux

Reference

A novel tert-butoxycarbonylation reagent: 1-tert-butoxy-2-tert-butoxycarbonyl-1,2-dihydroisoquinoline (BBDI)

Saito, Yukako; Ouchi, Hidekazu; Takahata, Hiroki, Tetrahedron, 2006, 62(50), 11599-11607

Production Method 2

24424-99-5

95932-39-1

95932-40-4

Reaction Conditions

1.1 Reagents: Sodium hydroxide Catalysts: Tetrabutylammonium hydrogen sulfate Solvents: Dichloromethane ,  Water

Reference

Phase transfer catalysis in the tert-butyloxycarbonylation of alcohols, phenols, enols, and thiols with di-tert-butyl dicarbonate

Houlihan, F.; Bouchard, F.; Frechet, J. M. J.; Willson, C. G., Canadian Journal of Chemistry, 1985, 63(1), 153-62

Production Method 3

404586-94-3

95932-39-1

Reaction Conditions

1.1 Solvents: Benzene ;  reflux

Reference

2(1H)-Isoquinolinecarboxylic acid, 1-(1,1-dimethylethoxy)-1,1-dimethylethyl ester

Saito, Yukako; Takahata, Hiroki, e-EROS Encyclopedia of Reagents for Organic Synthesis, 2009, 1, 1-2

Production Method 4

404586-94-3

95932-39-1

Reaction Conditions

1.1 Solvents: Benzene

Reference

1-tert-Butoxy-2-tert-butoxycarbonyl-1,2-dihydroisoquinoline: A Novel and Chemoselective tert-Butoxycarbonylation Reagent

Ouchi, Hidekazu; Saito, Yukako; Yamamoto, Yutaka; Takahata, Hiroki, Organic Letters, 2002, 4(4), 585-587

Production Method 5

24424-99-5

95932-39-1

Reaction Conditions

1.1 Reagents: 4-(Dimethylamino)pyridine Solvents: Dichloromethane ;  10 h, rt
1.2 Reagents: Water ;  rt
1.3 Reagents: Hydrogen Catalysts: Palladium Solvents: Ethyl acetate ;  1 d, rt

Reference

Preparation of tricyclic compounds as PARP inhibitors

, World Intellectual Property Organization, , ,

Production Method 6

404586-94-3

95932-39-1

Reaction Conditions

1.1 Solvents: Benzene ;  reflux

Reference

2(1H)-Isoquinolinecarboxylic Acid, 1-(1,1-Dimethylethoxy)-1,1-dimethylethyl Ester

Saito, Yukako; Takahata, Hiroki, e-EROS Encyclopedia of Reagents for Organic Synthesis, 2007, ,

Production Method 7

95932-39-1

Reaction Conditions

Reference

Preparation of cephalosporin derivatives for use as antibacterial agents

, European Patent Organization, , ,

4-aminophenyl tert-butyl carbonate Raw materials

• Di-tert-butyl dicarbonate
• 2(1H)-Isoquinolinecarboxylicacid, 1-(1,1-dimethylethoxy)-, 1,1-dimethylethyl ester

4-aminophenyl tert-butyl carbonate Preparation Products

• Carbonic acid, 4-[[(1,1-dimethylethoxy)carbonyl]amino]phenyl1,1-dimethylethyl ester (95932-40-4)
• 4-aminophenyl tert-butyl carbonate (95932-39-1)

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