Production Method 1

69838-89-7

95537-93-2

Reaction Conditions

1.1 Reagents: (T-4)-Trihydro(tetrahydrofuran)boron

Reference

Kinetic Isotope Effects in Cycloreversion of Rhenium (V) Diolates

Gable, Kevin P.; Zhuravlev, Fedor A., Journal of the American Chemical Society, 2002, 124(15), 3970-3979

Production Method 2

32488-43-0

95537-93-2

Reaction Conditions

1.1 Reagents: Magnesium

Reference

Ruthenium-Catalyzed Aromatization of Aromatic Enynes via the 1,2-Migration of Halo and Aryl Groups: A New Process Involving Electrocyclization and Skeletal Rearrangement

Shen, Hung-Chin; Pal, Sitaram; Lian, Jian-Jou; Liu, Rai-Shung, Journal of the American Chemical Society, 2003, 125(51), 15762-15763

Production Method 3

95537-93-2

Reaction Conditions

1.1 Reagents: Diisobutylaluminum hydride Solvents: Dichloromethane ,  Toluene ;  2 h, -78 °C; -78 °C → rt; 4 h, rt
1.2 Reagents: Potassium sodium tartrate ;  30 min, rt

Reference

Nickel-Catalyzed Decarbonylative Alkylidenation of Phthalimides with Trimethylsilyl-Substituted Alkynes

Shiba, Takahiro; Kurahashi, Takuya; Matsubara, Seijiro, Journal of the American Chemical Society, 2013, 135(37), 13636-13639

Production Method 4

1633-56-3

95537-93-2

Reaction Conditions

1.1 Reagents: Acetic anhydride ,  Sodium formate Catalysts: Palladium diacetate ,  CataCXium A Solvents: Dimethylformamide ;  1 h, 30 °C
1.2 Reagents: Triethylamine ;  16 h, 110 °C

Reference

Convenient Palladium-Catalyzed Reductive Carbonylation of Aryl Bromides Under Gas-Free Conditions

Ying, Jun; Fu, Lu-Yang; Zhou, Chao; Qi, Xinxin; Peng, Jin-Bao; et al, European Journal of Organic Chemistry, 2018, 2018(22), 2780-2783

Production Method 5

3228-27-1

95537-93-2

Reaction Conditions

1.1 Reagents: Sodium carbonate ,  Triethylsilane Catalysts: 1,4-Bis(diphenylphosphino)butane ,  Palladium, bis(acetonitrile)dichloro- Solvents: Dimethylformamide ;  20 bar, rt; 20 h, 20 bar, 100 °C; 100 °C → rt

Reference

Palladium-catalyzed carbonylations of aryl bromides using paraformaldehyde. Synthesis of aldehydes and esters

Natte, Kishore; Dumrath, Andreas; Neumann, Helfried; Beller, Matthias, Angewandte Chemie, 2014, 53(38), 10090-10094

Production Method 6

100-66-3

32488-43-0

95537-93-2

Reaction Conditions

1.1 Reagents: Phosphorus oxychloride

Reference

The Vilsmeier reaction of fully conjugated carbocycles and heterocycles

Jones, Gurnos; Stanforth, Stephen P., Organic Reactions (Hoboken, 1997, 49,

Anisaldehyde-13C Raw materials

• Formaldehyde-13C (20% by weight in water)
• 4-Methoxy-7-13C-benzoic Acid
• Formic Acid-13C
• Anisole
• N,N-Dimethylformamide-(carbonyl-13C)

Anisaldehyde-13C Preparation Products

• Anisaldehyde-13C (95537-93-2)

• 1. Fe/Fe3C@C nanoparticles encapsulated in N-doped graphene–CNTs framework as an efficient bifunctional oxygen electrocatalyst for robust rechargeable Zn–air batteries?
  Zhiyan Chen,Nan Wu,Yaobing Wang,Bing Wang,Yingde Wang J. Mater. Chem. A, 2018,6, 516-526
• 2. Essential effect of the electrolyte on the mechanical and chemical degradation of LiNi0.8Co0.15Al0.05O2 cathodes upon long-term cycling??
  Xiaoming Liu,Zachary D. Hood,Wangda Li,Donovan N. Leonard,Arumugam Manthiram,Miaofang Chi J. Mater. Chem. A, 2021,9, 2111-2119
• 3. Fast-Track to Research Data Management in Experimental Material Science-Setting the Ground for Research Group Level Materials Digitalization.
  LarsBanko,AlfredLudwig
• 4. Emulsion technologies for multicellular tumour spheroid radiation assays?
  Kay S. McMillan,Anthony G. McCluskey,Annette Sorensen,Marie Boyd,Michele Zagnoni Analyst, 2016,141, 100-110
• 5. Evolved polymerases facilitate selection of fully 2′-OMe-modified aptamers?
  Zhixia Liu,Tingjian Chen,Floyd E. Romesberg Chem. Sci., 2017,8, 8179-8182

• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Benzoyl derivatives

Anisaldehyde-13C: A Comprehensive Guide to the Isotopically Labeled Flavor Compound (CAS No. 95537-93-2)

In the realm of analytical chemistry and flavor research, Anisaldehyde-13C (CAS No. 95537-93-2) has emerged as a critical tool for scientists seeking precision in isotopic labeling studies. This 13C-labeled variant of 4-methoxybenzaldehyde is widely utilized in mass spectrometry, metabolic pathway tracing, and fragrance formulation. With the growing demand for stable isotope-labeled compounds in pharmaceuticals and food science, Anisaldehyde-13C offers unparalleled accuracy in quantifying molecular interactions.

The compound’s structure features a carbon-13 isotope at the aldehyde group, enhancing its detectability in GC-MS and LC-MS analyses. Researchers frequently search for "Anisaldehyde-13C synthesis" or "CAS 95537-93-2 applications," reflecting its relevance in isotope dilution assays. Recent trends also highlight its role in natural product authentication, addressing consumer concerns about food adulteration and essential oil purity.

From a commercial perspective, Anisaldehyde-13C is pivotal in flavor and fragrance industries, where it aids in differentiating synthetic vs. natural components. SEO-driven queries like "buy Anisaldehyde-13C high purity" or "13C-labeled benzaldehyde derivatives" underscore its market demand. The compound’s non-toxic profile aligns with global shifts toward green chemistry, making it a preferred choice for sustainable research.

Beyond analytics, Anisaldehyde-13C is explored in nutraceutical studies, particularly in tracking phenylpropanoid metabolism. Its compatibility with NMR spectroscopy further expands its utility in structural elucidation. As labs prioritize reproducible data, this isotopologue’s stability ensures minimal interference in complex matrices—answering frequent search queries like "best internal standard for aldehydes."

Regulatory compliance is another hotspot. While Anisaldehyde-13C isn’t classified as hazardous, its handling follows ISO 9001 standards, a detail often searched alongside "CAS 95537-93-2 safety data." The compound’s shelf life and storage conditions (e.g., "Anisaldehyde-13C stability in DMSO") are equally critical for procurement teams.

In summary, Anisaldehyde-13C (CAS No. 95537-93-2) bridges gaps between analytical precision and industrial applications. Its integration into foodomics and pharmacokinetics studies positions it as a future-proof reagent, resonating with today’s emphasis on traceability and molecular transparency.

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