Production Method 1

170304-76-4

945744-16-1

Reaction Conditions

1.1 Reagents: Sodium hydride Solvents: Dimethylformamide ;  30 min, 0 °C
1.2 22.5 h, rt

Reference

Amyloid β binding saccharide thin film and measurement method of amyloid β

, Japan, , ,

Production Method 2

170304-76-4

945744-16-1

Reaction Conditions

1.1 Reagents: Oxalyl chloride ;  30 min, cooled; overnight, rt

Reference

SNAP/CLIP-Tags and Strain-Promoted Azide-Alkyne Cycloaddition (SPAAC)/Inverse Electron Demand Diels-Alder (IEDDA) for Intracellular Orthogonal/Bioorthogonal Labeling

Macias-Contreras, Miguel; He, Huan; Little, Kevin N.; Lee, Justin P.; Campbell, Ryan P.; et al, Bioconjugate Chemistry, 2020, 31(5), 1370-1381

Production Method 3

170304-76-4

945744-16-1

Reaction Conditions

1.1 Reagents: Oxalyl chloride Solvents: Methanol ;  30 min, 0 °C; 16 h, 0 °C

Reference

Preparation of prenylated antibody-drug conjugates containing branched linkers useful for treating cancer

, World Intellectual Property Organization, , ,

Production Method 4

170304-76-4

945744-16-1

Reaction Conditions

1.1 Reagents: Oxalyl chloride Solvents: Methanol ;  30 min, 0 °C; 16 h, 0 °C

Reference

Preparation of prenylated antibody-drug conjugates containing peptide groups useful for treating cancer

, World Intellectual Property Organization, , ,

Production Method 5

170304-76-4

945744-16-1

Reaction Conditions

1.1 Reagents: Oxalyl chloride Solvents: Methanol ;  30 min, 0 °C; 16 h, 0 °C

Reference

Preparation of prenylated antibody-drug conjugates containing self-immolative groups useful for treating cancer

, World Intellectual Property Organization, , ,

Production Method 6

170304-76-4

945744-16-1

Reaction Conditions

1.1 Reagents: Sodium hydride Solvents: Dimethylformamide ;  30 min, 0 °C
1.2 22.5 h, rt

Reference

Syntheses of sulfo-glycodendrimers using click chemistry and their biological evaluation

Miura, Yoshiko; Onogi, Shunsuke; Fukuda, Tomohiro, Molecules, 2012, 17, 11877-11896

Production Method 7

170304-76-4

945744-16-1

Reaction Conditions

1.1 Reagents: Sodium methoxide Solvents: Methanol ;  20 min, rt
1.2 24 h, rt

Reference

Sugar balls: synthesis and supramolecular assembly of [60]fullerene

Kato, Haruhito; Boettcher, Christoph; Hirsch, Andreas, European Journal of Organic Chemistry, 2007, (16), 2659-2666

Methyl 2-(2-(2-chloroethoxy)ethoxy)acetate Raw materials

• Cl-PEG2-acid

Methyl 2-(2-(2-chloroethoxy)ethoxy)acetate Preparation Products

• Methyl 2-(2-(2-chloroethoxy)ethoxy)acetate (945744-16-1)

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