Production Method 1

94062-49-4

Reaction Conditions

Reference

Non-conventional lignans: coumarinolignans, flavonolignans and stilbenolignans

Begum, Sajeli A.; Sahai, Mahendra; Ray, Anil B., Progress in the Chemistry of Organic Natural Products, 2010, 93, 1-70

Production Method 2

121404-99-7

121404-98-6

94062-49-4

Reaction Conditions

1.1 Reagents: Hydrochloric acid Solvents: Acetic acid ,  Water

Reference

Total synthesis of coumarinolignans, aquillochin (cleomiscosin C) and cleomiscosin D

Tanaka, Hitoshi; Ishihara, Masaya; Ichino, Kazuhiko; Ito, Kazuo, Chemical & Pharmaceutical Bulletin, 1988, 36(10), 3833-7

Production Method 3

94062-49-4

Reaction Conditions

Reference

Synthesis of coumarinolignans through chemical and enzymic oxidation

Lin, Lee Juian; Cordell, Geoffrey A., Journal of the Chemical Society, 1984, (3), 160-1

Production Method 4

574-84-5

537-33-7

94062-49-4

84575-10-0

Reaction Conditions

1.1 Reagents: Silver oxide (Ag2O)

Reference

Synthesis and structure elucidation of coumarinolignans

Lin, Lee Juian; Cordell, Geoffrey A., Journal of Chemical Research, 1988, (12), 396-7

9H-Pyrano[2,3-f]-1,4-benzodioxin-9-one, 2,3-dihydro-2-(4-hydroxy-3,5-dimethoxyphenyl)-3-(hydroxymethyl)-5-methoxy-, (2R,3R)-rel- Raw materials

• rel-8-Hydroxy-7-[(1R,2S)-2-hydroxy-2-(4-hydroxy-3,5-dimethoxyphenyl)-1-(hydroxymethyl)ethoxy]-6-methoxy-2H-1-benzopyran-2-one
• Fraxetin
• Sinapyl Alcohol (>85%)
• rel-8-Hydroxy-7-[(1R,2R)-2-hydroxy-2-(4-hydroxy-3,5-dimethoxyphenyl)-1-(hydroxymethyl)ethoxy]-6-methoxy-2H-1-benzopyran-2-one

9H-Pyrano[2,3-f]-1,4-benzodioxin-9-one, 2,3-dihydro-2-(4-hydroxy-3,5-dimethoxyphenyl)-3-(hydroxymethyl)-5-methoxy-, (2R,3R)-rel- Preparation Products

• 9H-Pyrano[2,3-f]-1,4-benzodioxin-9-one,2,3- dihydro-3-(4-hydroxy-3,5-dimethoxyphenyl)- 2-(hydroxymethyl)-5-methoxy-,(2R,3R)-rel- (84575-10-0)
• 9H-Pyrano[2,3-f]-1,4-benzodioxin-9-one, 2,3-dihydro-2-(4-hydroxy-3,5-dimethoxyphenyl)-3-(hydroxymethyl)-5-methoxy-, (2R,3R)-rel- (94062-49-4)

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• Solvents and Organic Chemicals Organic Compounds Lignans, neolignans and related compounds Coumarinolignans Coumarinolignans
• Solvents and Organic Chemicals Organic Compounds Lignans, neolignans and related compounds Coumarinolignans

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