Production Method 1

691411-77-5

93457-07-9

Reaction Conditions

1.1 Solvents: Methanol ,  Toluene ;  30 min, -78 °C; 1 h, rt
1.2 Reagents: Ammonium chloride Solvents: Water ;  rt

Reference

Allosteric Regulation of Hsp90α's Activity by Small Molecules Targeting the Middle Domain of the Chaperone

Zhou, Chen; Zhang, Chi; Zhu, Hongwen; Liu, Zhijun; Su, Haixia; et al, iScience, 2020, 23(2),

Production Method 2

691411-77-5

93457-07-9

Reaction Conditions

1.1 Solvents: Toluene ,  Tetrahydrofuran ;  -78 °C → rt; 30 min, rt; rt → 0 °C
1.2 Reagents: Ammonium chloride Solvents: Water ;  0 °C

Reference

Preparation of cyanothiophene derivatives as glucagon antagonists for treating type II diabetes mellitus

, United States, , ,

Production Method 3

93457-07-9

Reaction Conditions

Reference

Synthesis of benzylic ketones and alcohols by electroreductive coupling of benzylic compounds bearing a leaving group other than a halogen with anhydrides and carbonyl compounds

Gal, J.; Folest, J. C.; Troupel, M.; Guitton, P.; Robin, Y., New Journal of Chemistry, 1996, 20(3), 375-83

Production Method 4

108-22-5

554-00-7

93457-07-9

Reaction Conditions

1.1 Reagents: Sodium nitrite ,  Hydrochloric acid Solvents: Water ;  45 min, -5 °C; 15 min, -5 °C
1.2 Reagents: Hydrofluoric acid ,  Boric acid (H3BO3) ;  30 min, -5 °C; 2 h, 0 °C
1.3 Reagents: Sodium acetate Catalysts: Copper oxide (Cu2O) ;  30 min, 20 - 25 °C; 6 h, 20 - 25 °C

Reference

Synthesis and fungicidal activity of novel oxathiapiprolin derivatives

Ding, Chengrong; Pan, Yayun; Yin, Xu; Tan, Chengxia; Wang, Xuedong, Youji Huaxue, 2019, 39(7), 2062-2069

Production Method 5

127138-62-9

93457-07-9

Reaction Conditions

1.1 Catalysts: Acetic anhydride

Reference

Electrosynthesis of benzylic ketones

, France, , ,

Production Method 6

93457-07-9

Reaction Conditions

Reference

Synthesis and biological activity of thiazolidine piperidine nicotinamide compounds

Ding, Chengrong; Pan, Yayun; Yin, Xu; Tan, Chengxia, Youji Huaxue, 2019, 39(7), 2099-2105

2,4-Dichlorophenylacetone Raw materials

• Isopropenyl acetate
• Benzenemethanaminium, 2,4-dichloro-N,N,N-trimethyl-, iodide
• 2-(2,4-Dichlorophenyl)-N-methoxy-N-methylacetamide
• 2,4-Dichloroaniline

2,4-Dichlorophenylacetone Preparation Products

• 2,4-Dichlorophenylacetone (93457-07-9)

• 1. Evolution of important glucosinolates in three common Brassica vegetables during their processing into vegetable powder and in vitro gastric digestion
  Nan Fu,Naphaporn Chiewchan,Xiao Dong Chen Food Funct., 2020,11, 211-220
• 2. Evolving better nanoparticles: Genetic algorithms for optimising cluster geometries
  Dalton Trans., 2003, 4193-4207
• 3. Fc microparticles can modulate the physical extent and magnitude of complement activity?
  David White,Sean R. Stowell Biomater. Sci., 2017,5, 463-474
• 4. Evolution of shape, size, and areal density of a single plane of Si nanocrystals embedded in SiO2 matrix studied by atom probe tomography
  Bin Han,Yasuo Shimizu,Gabriele Seguini,Celia Castro,Gérard Ben Assayag,Koji Inoue,Yasuyoshi Nagai,Sylvie Schamm-Chardon,Michele Perego RSC Adv., 2016,6, 3617-3622
• 5. Evolution of dealloying induced strain in nanoporous gold crystals?
  Ross Harder,David C. Dunand,Ian McNulty Nanoscale, 2017,9, 5686-5693

• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Phenylpropanes
• Solvents and Organic Chemicals Organic Compounds Aldehyde/Ketone

• 88968-75-6(1-(2,3,4-trichlorophenyl)propan-2-one)
• 102052-39-1(1-(2,3-dichlorophenyl)propan-2-one)
• 760191-76-2(2-Octanone, 1-(2-chlorophenyl)-)
• 93457-06-8(2,6-Dichlorophenylacetone)
• 6305-95-9(2-Chlorophenylacetone)
• 92435-52-4(2-Propanone, 1-(2-chlorophenyl)-3-phenyl-)
• 102052-40-4(1-(2,5-Dichlorophenyl)acetone)
• 760191-80-8(2-Butanone, 1-(2-chlorophenyl)-4-phenyl-)
• 98581-93-2(3-(2,4-dichlorophenyl)propanal)
• 1057670-91-3(3-(2,6-dichlorophenyl)propanal)