Production Method 1

2206-27-1

926-09-0

Reaction Conditions

1.1 Catalysts: Diglyme

Reference

A high yield synthesis of dimethyl sulfide-d6, and preparation of chloro(dimethyl sulfide-d6)gold(I) and trichloro(dimethyl sulfide-d6)gold(III)

Shaw, C. Frank III; Cancro, Margaret P.; Butler, Ian S., Journal of Labelled Compounds and Radiopharmaceuticals, 1979, 16(6), 827-31

Production Method 2

2206-27-1

926-09-0

Reaction Conditions

1.1 Catalysts: Thiophenol

Reference

Practical synthesis of deuterium-labeled methyl sulfide, methyl disulfide, methanethiol, and methanesulfenyl compounds

Kim, Jhong K.; Lingman, Eric; Caserio, Marjorie C., Journal of Organic Chemistry, 1978, 43(23), 4545-6

Production Method 3

2206-27-1

926-09-0

Reaction Conditions

1.1 Reagents: Ammonium bromide ;  reflux

Reference

Electron transfer in peroxide-nucleophile interactions. Reaction of tert-butyl peroxybenzoates with sulfide

Hendrickson, William H. Jr., 1974, , ,

Production Method 4

594-09-2

2206-27-1

926-09-0

676-96-0

Reaction Conditions

1.1 Catalysts: (OC-6-35)-[2,4-Bis(1,1-dimethylethyl)-6-[[rel-(1R,4R)-hexahydro-4-methyl-1H-1,4-… Solvents: DMSO-d6

Reference

Faster oxygen atom transfer catalysis with a tungsten dioxo complex than with its molybdenum analog

Arumuganathan, T.; Mayilmurugan, Ramasamy; Volpe, Manuel; Moesch-Zanetti, Nadia C., Dalton Transactions, 2011, 40(31), 7850-7857

Production Method 5

2206-27-1

926-09-0

87228-53-3

7282-94-2

Reaction Conditions

1.1 30 min, 160 °C

Reference

Direct 1,2-Oxosulfenylation of Acetylenic Sulfones with DMSO

Fu, Duo; Dong, Jun; Wang, Jiayi; Xu, Jiaxi, Asian Journal of Organic Chemistry, 2021, 10(7), 1756-1764

1,1’-Thiobismethane-d3 (Dimethyl Sulfide-d6) Raw materials

• 3mol/L Trimethylphosphine Tetrahydrofuran Solution
• Dimethyl Sulfoxide-d6, 99.9%(High purity)

1,1’-Thiobismethane-d3 (Dimethyl Sulfide-d6) Preparation Products

• Trimethylphosphine oxide (676-96-0)
• Ethanone, 2-[(4-methylphenyl)sulfonyl]-2-(methylthio)-1-phenyl- (87228-53-3)
• Dimethyl Disulfide-d6 (7282-94-2)
• 1,1’-Thiobismethane-d3 (Dimethyl Sulfide-d6) (926-09-0)

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