Production Method 1

1255871-55-6

91065-17-7

Reaction Conditions

1.1 Reagents: Pyridine ,  Trifluoroacetic anhydride Solvents: 1,4-Dioxane ;  0 °C; 3 h, rt
1.2 Reagents: Water

Reference

Thiolate versus Selenolate: Structure, Stability, and Charge Transfer Properties

Ossowski, Jakub; Wachter, Tobias; Silies, Laura; Kind, Martin; Noworolska, Agnieszka; et al, ACS Nano, 2015, 9(4), 4508-4526

Production Method 2

14874-70-5

13715-19-0

91065-17-7

Reaction Conditions

Reference

SRN1 syntheses of bis(phenylthio)- and dicyanonaphthalenes via diazo sulfides

Novi, M.; Garbarino, G.; Petrillo, G.; Dell'Erba, C., Tetrahedron, 1990, 46(6), 2205-12

Production Method 3

1255871-55-6

91065-17-7

Reaction Conditions

1.1 Reagents: Phosphorus oxychloride ;  15 min, 80 °C

Reference

Novel amidrazone derivatives: Design, synthesis and activity evaluation

Zhou, Hua; Wang, Zhi Sen; Liu, Xin Hua; Chen, Fei Hu, Bioorganic & Medicinal Chemistry, 2018, 26(12), 3158-3165

Production Method 4

1255871-55-6

91065-17-7

Reaction Conditions

1.1 Reagents: 2,2,2-Trichloroacetyl chloride ,  Triethylamine Solvents: Dichloromethane ;  0 - 5 °C

Reference

Nickel-Catalyzed Cross-Couplings of Benzylic Pivalates with Arylboroxines: Stereospecific Formation of Diarylalkanes and Triarylmethanes

Zhou, Qi; Srinivas, Harathi D.; Dasgupta, Srimoyee; Watson, Mary P., Journal of the American Chemical Society, 2013, 135(9), 3307-3310

Production Method 5

1255871-55-6

91065-17-7

Reaction Conditions

1.1 Reagents: Pyridine ,  Trifluoroacetic anhydride Solvents: 1,4-Dioxane ;  0 °C; 5 h, rt

Reference

MitoBlue: A Nontoxic and Photostable Blue-Emitting Dye That Selectively Labels Functional Mitochondria

Sanchez, Mateo I.; Martinez-Costas, Jose; Mascarenas, Jose L.; Vazquez, M. Eugenio, ACS Chemical Biology, 2014, 9(12), 2742-2747

Production Method 6

33626-98-1

91065-17-7

Reaction Conditions

1.1 Reagents: Ammonia Solvents: Methanol ;  80 °C
1.2 Reagents: Triethylamine ,  Trifluoroacetic anhydride Solvents: Dichloromethane ;  0 °C → rt

Reference

Synthesis, Structure-Activity Relationship, and Pharmacological Profile of Analogs of The ASIC-3 Inhibitor A-317567

Kuduk, Scott D.; Di Marco, Christina N.; Bodmer-Narkevitch, Vera; Cook, Sean P.; Cato, Matthew J.; et al, ACS Chemical Neuroscience, 2010, 1(1), 19-24

6-Bromo-2-cyanonaphthalene Raw materials

• Borate(1-),tetrafluoro-
• Cuprate(1-), bis(cyano-kC)-, sodium (1:1)
• Methyl 6-Bromo-2-napthoate
• 6-Bromo-2-naphthamide

6-Bromo-2-cyanonaphthalene Preparation Products

• 6-Bromo-2-cyanonaphthalene (91065-17-7)

• 1. Evidence for the intrinsic nature of band-gap states electrochemically observed on atomically flat TiO2(110) surfaces?
  Shintaro Takata,Yoshihiro Miura Phys. Chem. Chem. Phys., 2014,16, 24784-24789
• 2. Emerging enantiomeric resolution materials with homochiral nano-fabrications
  Ji-Ping Wei Nanoscale, 2015,7, 11815-11832
• 3. Fate of single walled carbon nanotubes in wetland ecosystems?
  Joseph H. Bisesi,Tara Sabo-Attwood Environ. Sci.: Nano, 2014,1, 574-583
• 4. Excitation energies from ground-state density-functionals by means of generator coordinates
  A. B. F. da Silva,K. Capelle Phys. Chem. Chem. Phys., 2009,11, 4564-4569
• 5. Emulsion soft templating of carbide-derived carbon nanospheres with controllable porosity for capacitive electrochemical energy storage?
  M. Zeiger,N. J?ckel,P. Strubel,L. Borchardt,R. Reinhold,W. Nickel,J. Eckert,V. Presser,S. Kaskel J. Mater. Chem. A, 2015,3, 17983-17990

• 623-00-7(4-Bromobenzonitrile)
• 139914-16-2(6,7-Dibromo-2-naphthalenecarbonitrile)
• 771534-56-6(4-bromo-2,3,5,6-tetradeuterio-benzonitrile)
• 885227-79-2(7-BROMO-2-NAPHTHONITRILE)
• 92616-49-4(4-Bromonaphthalene-1-carbonitrile)
• 70484-02-5(6-Bromo-2,3-dicyanonaphthalene)
• 79996-86-4(3-bromonaphthalene-1-carbonitrile)
• 91065-16-6(6-Bromonaphthalene-1-carbonitrile)
• 129278-20-2(5-bromonaphthalene-1-carbonitrile)
• 496835-91-7(4-bromonaphthalene-2-carbonitrile)