Production Method 1

1260779-86-9

88946-67-2

Reaction Conditions

1.1 Solvents: Dimethylformamide ;  5 h, reflux

Reference

Biosourced vanillin-based building blocks for organic electronic materials

Boivin, Louis-Philippe; Dupont, William; Leclerc, Mario ; Gendron, David, Journal of Organic Chemistry, 2021, 86(23), 16548-16557

Production Method 2

37895-73-1

88946-67-2

Reaction Conditions

Reference

Preparation of phthalocyanines for measuring magnetic fields by electron paramagnetic resonance

, European Patent Organization, , ,

Production Method 3

37895-73-1

88946-67-2

Reaction Conditions

1.1 Catalysts: 1,1-Bis(diphenylphosphino)ferrocene ,  Tris(dibenzylideneacetone)dipalladium Solvents: Dimethylacetamide ;  2 h, 120 °C

Reference

Palladium(II) octaalkoxy- and octaphenoxyphthalocyanines: Synthesis and evaluation as catalysts in the Sonogashira reaction

Platonova, Yana B.; Volov, Alexander N.; Tomilova, Larisa G., Journal of Catalysis, 2019, 373, 222-227

Production Method 4

37895-73-1

88946-67-2

Reaction Conditions

1.1 Reagents: Poly(methylhydrosiloxane) Solvents: Dimethylacetamide ;  rt → 120 °C
1.2 Catalysts: 1,1-Bis(diphenylphosphino)ferrocene ,  Tris(dibenzylideneacetone)dipalladium ;  2.5 h, 120 °C

Reference

Synthesis of phthalonitriles using a palladium catalyst

Iqbal, Zafar; Lyubimtsev, Alexey; Hanack, Michael, Synlett, 2008, (15), 2287-2290

Production Method 5

37895-73-1

88946-67-2

Reaction Conditions

1.1 Solvents: Dimethylformamide ,  Pyridine ;  2 h, heated
1.2 Reagents: Disodium sulfide ;  1 h, rt

Reference

Synthesis and characterization of 2,3,9,10,16,17,23,24-octamethoxyphthalocyanine

Duan, Qingfeng; Bao, Meng; Mou, Zonggang; Chen, Bo; Chen, Yan; et al, Jinan Daxue Xuebao, 2009, 23(3), 241-243

Production Method 6

37895-73-1

88946-67-2

109305-98-8

Reaction Conditions

1.1 Solvents: Dimethylformamide ;  3 h, reflux

Reference

Complementary Syntheses Giving Access to a Full Suite of Differentially Substituted Phthalocyanine-Porphyrin Hybrids

Alkorbi, Faeza; Diaz-Moscoso, Alejandro; Gretton, Jacob; Chambrier, Isabelle; Tizzard, Graham J.; et al, Angewandte Chemie, 2021, 60(14), 7632-7636

4,5-Dimethoxyphthalonitrile Raw materials

• 4,5-Dibromoveratrole
• 2-Iodo-4,5-dimethoxybenzonitrile

4,5-Dimethoxyphthalonitrile Preparation Products

• 4,5-Dimethoxyphthalonitrile (88946-67-2)
• 2-Bromo-4,5-dimethoxybenzonitrile (109305-98-8)

• 1. Fate of single walled carbon nanotubes in wetland ecosystems?
  Joseph H. Bisesi,Tara Sabo-Attwood Environ. Sci.: Nano, 2014,1, 574-583
• 2. Evidence of CO2 molecule acting as an electron acceptor on a nanoporous metal–organic-framework MIL-53 or Cr3+(OH)(O2C–C6H4–CO2)?
  Alexandre Vimont,Arnaud Travert,Philippe Bazin,Jean-Claude Lavalley,Marco Daturi,Christian Serre,Gérard Férey,Sandrine Bourrelly,Philip L. Llewellyn Chem. Commun., 2007, 3291-3293
• 3. Excess electrons in lithium–ethylamine solutions—density, electrical conductivity and EPR studies
  Phys. Chem. Chem. Phys., 1999,1, 3561-3565
• 4. Enabling chloride salts for thermal energy storage: implications of salt purity?
  J. Matthew Kurley,Phillip W. Halstenberg,Abbey McAlister,Stephen Raiman,Richard T. Mayes RSC Adv., 2019,9, 25602-25608
• 5. Exchanged ligands on the surface of a giant cluster: [(MoO3)176(H2O)63(CH3OH)17Hn](32 – n)–
  Chem. Commun., 1998, 1501-1502

• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Dimethoxybenzenes
• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Methoxybenzenes Dimethoxybenzenes

• 2024-83-1(3,4-Dimethoxybenzonitrile)
• 918663-88-4(2,3-Naphthalenedicarbonitrile, 6,7-bis(4-methoxyphenoxy)-)
• 22246-19-1(Benzonitrile, 5-methoxy-2-methyl-)
• 99276-82-1(1,2-Benzenedicarbonitrile, 4,4'-[1,2-phenylenebis(oxy)]bis-)
• 4421-08-3(4-Hydroxy-3-methoxybenzonitrile)
• 52805-46-6(3-hydroxy-4-methoxy-benzonitrile)
• 21883-13-6(4-Methoxy-2-methylbenzonitrile)
• 118132-09-5(1,2-Benzenedicarbonitrile,4,5-diethoxy-)
• 80323-72-4(1,2-Benzenedicarbonitrile, 4-methoxy-)
• 23024-83-1(3,4-dimethoxybenzoic acid nitrile)