Production Method 1

144-62-7

160969-03-9

239463-72-0

885340-14-7

885340-11-4

144-62-7

Reaction Conditions

1.1 Reagents: Sodium carbonate Solvents: tert-Butanol ;  reflux
1.2 Solvents: Isopropanol

Reference

Improved Preparation of Silodosin

Liu, Hui ; Lv, Fei; Liu, Yuan, Organic Preparations and Procedures International, 2019, 51(3), 287-293

Silodosin Dimer 7-Cyano Benzoate Raw materials

• Oxalic acid
• 2-2-(2,2,2-Trifluoroethoxy)phenoxyethyl Methanesulfonate
• 3-{5-[(2r)-2-aminopropyl]-7-cyano-2,3-dihydro-1h-indol-1-yl}propy L Benzoate

Silodosin Dimer 7-Cyano Benzoate Preparation Products

• 7-Descarboxamido, 7-Cyano (R)-Silodosin O-Benzoate (885340-11-4)
• Oxalic acid (144-62-7)
• Silodosin Dimer 7-Cyano Benzoate (885340-14-7)

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