Production Method 1

501-89-3

87524-66-1

52787-14-1

Reaction Conditions

1.1 Catalysts: Thionyl chloride Solvents: Methanol
1.2 Reagents: Hydrochloric acid Solvents: Water

Reference

A simple method for the preparation of monomethyl esters of dicarboxylic acids by selective esterification of the nonconjugated carboxyl group in the presence of an aromatic or conjugated carboxyl group

Ram, Ram N.; et al, Journal of Chemical Research, 2000, (6), 282-283

Production Method 2

501-89-3

87524-66-1

52787-14-1

Reaction Conditions

1.1 Reagents: Methanol ,  Phosphorus pentoxide ,  Sodium sulfate ,  Copper sulfate

Reference

Use of phosphorus pentoxide. Preparation of half-esters through selective esterification

Banerjee, Amalendu; et al, Journal of the Indian Chemical Society, 1987, 64(1), 34-7

Production Method 3

23786-13-2

87524-66-1

589-18-4

99-94-5

34966-53-5

Reaction Conditions

1.1 Reagents: Sulfuric acid ,  Ozone Catalysts: Manganese diacetate Solvents: Acetic acid ;  20 °C; 20 °C

Reference

Concerning chemistry, reactivity, and mechanism of transition metal catalyzed oxidation of benzylic compounds by means of ozone

Waser, Mario; et al, Journal of Molecular Catalysis A: Chemical, 2005, 236(1-2), 187-193

4-(2-methoxy-2-oxo-ethyl)benzoic acid Raw materials

• 4-Carboxyphenylacetic acid
• Methyl 4-Methylphenylacetate

4-(2-methoxy-2-oxo-ethyl)benzoic acid Preparation Products

• 4-Methylbenzyl alcohol (589-18-4)
• 4-Methoxycarbonylmethyl-benzoic Acid Methyl Ester (52787-14-1)
• 4-Methylbenzoic acid (99-94-5)
• methyl 2-(4-methylphenyl)-2-oxoacetate (34966-53-5)
• 4-(2-methoxy-2-oxo-ethyl)benzoic acid (87524-66-1)

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• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Benzoic acids
• Solvents and Organic Chemicals Organic Compounds Benzenoids Benzene and substituted derivatives Benzoic acids and derivatives Benzoic acids

• 52787-14-1(4-Methoxycarbonylmethyl-benzoic Acid Methyl Ester)
• 14736-50-6(2-(2-methoxy-2-oxo-ethyl)benzoic acid)
• 155380-11-3(methyl 2-(4-(hydroxymethyl)phenyl)acetate)
• 67097-50-1(Benzeneacetic acid, 4-(ethoxycarbonyl)-)
• 107150-74-3(Benzeneacetic acid, 3-(ethoxycarbonyl)-, ethyl ester)
• 168625-39-6(Benzyl 2-(4-formylphenyl)acetate)
• 133017-05-7(Benzeneacetic acid, 4-(propoxycarbonyl)-, propyl ester)
• 22744-12-3(2-(4-methoxycarbonylphenyl)acetic acid)
• 142327-44-4(Methyl 2-(3-formylphenyl)acetate)
• 96524-70-8(Methyl 2-(4-formylphenyl)acetate)