Production Method 1

107-96-0

870451-09-5

Reaction Conditions

1.1 Solvents: Acetone

Reference

Mechanistic Aspects of Sterically Stabilized Controlled Radical Inverse Miniemulsion Polymerization

Qi, Genggeng; et al, Macromolecules (Washington, 2009, 42(12), 3906-3916

Production Method 2

79-06-1

870451-09-5

79-06-1

Reaction Conditions

1.1 pH 6, 60 °C; cooled

Reference

Synthesis of Well-Defined Statistical and Diblock Copolymers of Acrylamide and Acrylic Acid by Inverse Miniemulsion RAFT Polymerization

Ouyang, Liu; et al, Macromolecular Chemistry and Physics, 2010, 211(18), 1977-1983

Production Method 3

107-96-0

870451-09-5

Reaction Conditions

1.1 Reagents: Sodium hydroxide Solvents: Water ;  30 min, rt
1.2 rt; overnight, rt
1.3 rt; overnight, rt
1.4 Reagents: Hydrochloric acid Solvents: Water ;  acidified

Reference

Synthesis and Evaluation of New Dicarboxylic Acid Functional Trithiocarbonates: RAFT Synthesis of Telechelic Poly(n-butyl acrylate)s

Wang, Ran; et al, Macromolecules, 2005, 38(23), 9518-9525

Production Method 4

107-96-0

870451-09-5

Reaction Conditions

1.1 Reagents: Sodium hydroxide Solvents: Water ;  30 min, rt
1.2 16 h, rt
1.3 16 h, rt
1.4 Reagents: Hydrochloric acid Solvents: Water ;  pH 3.0

Reference

Dual pH-/thermo-responsive chitosan-based hydrogels prepared using "click" chemistry for colon-targeted drug delivery applications

Hoang, Huong Thi ; et al, Carbohydrate Polymers, 2021, 260,

Production Method 5

107-96-0

870451-09-5

Reaction Conditions

1.1 Reagents: Sodium hydroxide Solvents: Water ;  30 min, 4 °C
1.2 30 min, 4 °C
1.3 Reagents: Sodium hydroxide Solvents: Water ;  overnight, rt
1.4 acidified

Reference

Construction of enzyme-encapsulated fibermats from the cross-linkable copolymers poly(acrylamide)-co-poly(diacetone acrylamide) with the bi-functional cross-linker, adipic acid dihydrazide

Ido, Yuya; et al, Polymer, 2017, 132, 342-352

Production Method 6

90980-77-1

870451-09-5

Reaction Conditions

1.1 Solvents: Dichloromethane ;  48 h, 80 °C

Reference

Synthesis of dual-functional poly(6-azidohexylmethacrylate) brushes by a RAFT agent carrying carboxylic acid end groups

Cimen, Dilek; et al, Journal of Polymer Science, 2015, 53(14), 1696-1706

Production Method 7

107-96-0

870451-09-5

Reaction Conditions

1.1 Reagents: Triethylamine Solvents: Diethyl ether ;  30 min, 0 °C
1.2 Solvents: Diethyl ether ;  2 h, 0 °C; overnight, 0 °C
2.1 Solvents: Dichloromethane ;  48 h, 80 °C

Reference

Synthesis of dual-functional poly(6-azidohexylmethacrylate) brushes by a RAFT agent carrying carboxylic acid end groups

Cimen, Dilek; et al, Journal of Polymer Science, 2015, 53(14), 1696-1706

3-((((1-Carboxyethyl)Thio)Carbonothioyl)Thio)Propanoic Acid Raw materials

• Acrylamide
• 3-Mercaptopropionic acid
• Propanoic acid, 3-[(dithiocarboxy)thio]-

3-((((1-Carboxyethyl)Thio)Carbonothioyl)Thio)Propanoic Acid Preparation Products

• 3-((((1-Carboxyethyl)Thio)Carbonothioyl)Thio)Propanoic Acid (870451-09-5)
• Acrylamide (79-06-1)

• 1. Establishing empirical design rules of nucleic acid templates for the synthesis of silver nanoclusters with tunable photoluminescence and functionalities towards targeted bioimaging applications?
  Jason Y. C. Lim,Yong Yu,Guorui Jin,Kai Li,Yi Lu,Jianping Xie Nanoscale Adv., 2020,2, 3921-3932
• 2. Excimer formation effects and trap-assisted charge recombination loss channels in organic solar cells of perylene diimide dimer acceptors?
  Min Kim,Jae-Joon Lee,Tengling Ye,Panagiotis E. Keivanidis,Kilwon Cho J. Mater. Chem. C, 2020,8, 1686-1696
• 3. Fast-Track to Research Data Management in Experimental Material Science-Setting the Ground for Research Group Level Materials Digitalization.
  LarsBanko,AlfredLudwig
• 4. Esterase-responsive polymeric prodrug-based tumor targeting nanoparticles for improved anti-tumor performance against colon cancer?
  Gang Pan,Yi-jie Bao,Jie Xu,Tao Liu,Cheng Liu,Yan-yan Qiu,Xiao-jing Shi,Hui Yu,Ting-ting Jia,Xia Yuan,Ze-ting Yuan,Yi-jun Cao RSC Adv., 2016,6, 42109-42119
• 5. Exchanged ligands on the surface of a giant cluster: [(MoO3)176(H2O)63(CH3OH)17Hn](32 – n)–
  Chem. Commun., 1998, 1501-1502

• Solvents and Organic Chemicals Organic Compounds Organic acids and derivatives Carboxylic acids and derivatives Dicarboxylic acids and derivatives

• 2098070-20-1(2-(3-(Pyridin-3-yl)-1H-pyrazol-1-yl)acetimidamide)
• 2680771-01-9(4-cyclopentyl-3-{(prop-2-en-1-yloxy)carbonylamino}butanoic acid)
• 1444113-98-7(N-(3-cyanothiolan-3-yl)-2-[(2,2,2-trifluoroethyl)sulfanyl]pyridine-4-carboxamide)
• 332062-08-5(Fmoc-S-3-amino-4,4-diphenyl-butyric acid)
• 1270529-38-8(1,2,3,4,5,6-Hexahydro-[2,3]bipyridinyl-6-ol)
• 941977-17-9(N'-(3-chloro-2-methylphenyl)-N-2-(dimethylamino)-2-(naphthalen-1-yl)ethylethanediamide)
• 2138166-62-6(2,2-Difluoro-3-[methyl(2-methylbutyl)amino]propanoic acid)
• 89640-58-4(2-Iodo-4-nitrophenylhydrazine)
• 1449132-38-0(3-Fluoro-5-(2-fluoro-5-methylbenzylcarbamoyl)benzeneboronic acid)
• 2034271-14-0(2-(1H-indol-3-yl)-N-{[6-(thiophen-2-yl)-[1,2,4]triazolo[4,3-b]pyridazin-3-yl]methyl}acetamide)