Production Method 1

865605-32-9

865605-35-2

89343-06-6

67385-09-5

Reaction Conditions

1.1 Catalysts: 1,1-Bis(diphenylphosphino)ferrocene ,  Hydrotetrakis(triphenylphosphine)rhodium Solvents: Acetone ;  1 h, reflux

Reference

Equilibrating C-S Bond Formation by C-H and S-S Bond Metathesis. Rhodium-Catalyzed Alkylthiolation Reaction of 1-Alkynes with Disulfides

Arisawa, Mieko; Fujimoto, Kenji; Morinaka, Satoshi; Yamaguchi, Masahiko, Journal of the American Chemical Society, 2005, 127(35), 12226-12227

SILANE, TRIS(1-METHYLETHYL)[(OCTYLTHIO)ETHYNYL]- Raw materials

• Carbamic acid, [2-[[[tris(1-methylethyl)silyl]ethynyl]thio]ethyl]-, 1,1-dimethylethyl ester

SILANE, TRIS(1-METHYLETHYL)[(OCTYLTHIO)ETHYNYL]- Preparation Products

• Triisopropylsilylacetylene (89343-06-6)
• SILANE, TRIS(1-METHYLETHYL)[(OCTYLTHIO)ETHYNYL]- (865605-35-2)
• 2-(Boc-amino)ethanthiol (>90%) (67385-09-5)

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