Production Method 1

865-48-5

Reaction Conditions

1.1 Reagents: Sodium amide Solvents: Toluene ;  rt → 110 °C; 1 h, 110 °C

Reference

New synthesis technology of sodium tert-butoxide

Tang, Shucheng; et al, Xiandai Nongyao, 2004, 3(1),

Production Method 2

865-48-5

Reaction Conditions

1.1 Reagents: Sodium Solvents: Hexane ;  1 h, rt → 100 °C; 0.15 MPa, 100 °C; 6 h, 0.15 - 0.2 MPa, 100 °C; 1.5 h, 0.2 MPa → 0.1 MPa, 100 °C

Reference

preparation of di=-tert-butyl dicarbonate using diphosgene and tert-butyl alcohol as starting materials

Li, Jiangao, Shanghai Huagong, 2006, 31(2), 22-27

Production Method 3

865-48-5

Reaction Conditions

1.1 Reagents: Sodium Solvents: 1,2,4-Trimethylbenzene

Reference

Process for preparation of alkali metal alkoxides free of alcohol of crystallization

, German Democratic Republic, , ,

Production Method 4

50-21-5

513-77-9

865-48-5

Reaction Conditions

Reference

Chemical equilibrium in the barium sulfate-sodium carbonate-water system

Alekseeva, E. V.; et al, Khimicheskaya Promyshlennost (Moscow, 1988, (1), 25-7

Production Method 5

865-48-5

865-48-5

Reaction Conditions

1.1 Solvents: Methanol ;  24 h, rt

Reference

A polymer analogous reaction for the formation of imidazolium and NHC based porous polymer networks

Thiel, Kerstin; et al, Polymer Chemistry, 2013, 4(6), 1848-1856

Production Method 6

60532-63-0

107-22-2

865-48-5

Reaction Conditions

1.1 48 h, rt
2.1 Solvents: Methanol ;  24 h, rt

Reference

A polymer analogous reaction for the formation of imidazolium and NHC based porous polymer networks

Thiel, Kerstin; et al, Polymer Chemistry, 2013, 4(6), 1848-1856

Production Method 7

60532-63-0

920-66-1

107-22-2

865-48-5

Reaction Conditions

1.1 Solvents: Glyoxal ;  15 s, rt; 20 s, rt; 5 h, 180 bar, rt → 65 °C
2.1 48 h, rt
3.1 Solvents: Methanol ;  24 h, rt

Reference

A polymer analogous reaction for the formation of imidazolium and NHC based porous polymer networks

Thiel, Kerstin; et al, Polymer Chemistry, 2013, 4(6), 1848-1856

Sodium-t-butoxide Raw materials

• Sodium-t-butoxide
• Lactate
• TAPM
• 1,1,1,3,3,3-Hexafluoro-2-propanol
• Glyoxal
• Barium carbonate

Sodium-t-butoxide Preparation Products

• Sodium-t-butoxide (865-48-5)

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• Other Chemical Reagents Organic Metal Reagents
• Solvents and Organic Chemicals Organic Compounds

• 36809-75-3(Tin(IV) tert-Butoxide)
• 3141-58-0(Ethoxy, 1,1-dimethyl-(9CI))
• 35342-67-7(tert-ButoxycopperDISCONTINUED)
• 32149-57-8(Magnesium tert-butoxide)
• 3934-10-9(2-Propanol, 2-methyl-,rubidium salt (9CI))
• 3934-09-6(Cesium 2-methylpropan-2-olate)
• 33500-15-1(tert-Butyl-1,1,1-d3 Alcohol)
• 33881-97-9(Trisodium;azanide;2-methylpropan-2-olate)
• 24363-36-8(2-Propanol, 2-methyl-, barium salt)
• 10585-27-0(2-Propanol, 2-methyl-, vanadium(4+) salt (9CI))