Production Method 1

75039-59-7

85302-17-6

Reaction Conditions

Reference

Reaction of 2-dimethylaminomethylene-1,3-diones with dinucleophiles. I. Synthesis of 1,5-disubstituted 4-acylpyrazoles

Schenone, Pietro; et al, Journal of Heterocyclic Chemistry, 1982, 19(6), 1355-61

Production Method 2

75039-59-7

85302-17-6

Reaction Conditions

1.1 Solvents: Methanol ;  0 °C
2.1 Solvents: Methanol ;  1.5 h, reflux

Reference

Reactions of 2-(N,N-dimethylaminomethylidene)-5,5-dimethyl-1,3-cyclohexanedione with nitrogen-containing nucleophiles

Pakal'nis, V. V.; et al, Vestnik Sankt-Peterburgskogo Universiteta, 2009, (2), 174-179

Production Method 3

85302-17-6

Reaction Conditions

1.1 Solvents: Methanol ;  1.5 h, reflux

Reference

Reactions of 2-(N,N-dimethylaminomethylidene)-5,5-dimethyl-1,3-cyclohexanedione with nitrogen-containing nucleophiles

Pakal'nis, V. V.; et al, Vestnik Sankt-Peterburgskogo Universiteta, 2009, (2), 174-179

Production Method 4

4637-24-5

126-81-8

85302-17-6

Reaction Conditions

Reference

Reaction of 2-dimethylaminomethylene-1,3-diones with dinucleophiles. I. Synthesis of 1,5-disubstituted 4-acylpyrazoles

Schenone, Pietro; et al, Journal of Heterocyclic Chemistry, 1982, 19(6), 1355-61

1,6,6-Trimethyl-1,5,6,7-tetrahydro-indazol-4-one Raw materials

• (dimethoxymethyl)dimethylamine
• 2-Dimethylaminomethylene-5,5-dimethyl-cyclohexane-1,3-dione
• 5,5-dimethylcyclohexane-1,3-dione

1,6,6-Trimethyl-1,5,6,7-tetrahydro-indazol-4-one Preparation Products

• 1,6,6-Trimethyl-1,5,6,7-tetrahydro-indazol-4-one (85302-17-6)

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• Solvents and Organic Chemicals Organic Compounds Organic oxygen compounds Organooxygen compounds Ketones
• Solvents and Organic Chemicals Organic Compounds Organic oxygen compounds Organooxygen compounds Carbonyl compounds Ketones

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