Production Method 1

116922-22-6

845729-43-3

Reaction Conditions

1.1 Reagents: Carbon dioxide Solvents: Acetonitrile ;  5 h, 1 atm, 60 °C
1.2 Reagents: Sodium chlorite Solvents: Water ;  20 min, 60 °C; 2.5 h, 60 °C
1.3 Reagents: Sodium sulfite Solvents: Water

Reference

A Facile Oxidation of Tertiary Amines to Lactams by Using Sodium Chlorite: Process Improvement by Precise pH Adjustment with CO2

Liu, Chaoyang; et al, Synlett, 2022, 33(10), 993-997

Production Method 2

402-67-5

845729-43-3

Reaction Conditions

1.1 Reagents: Potassium carbonate Solvents: Dimethyl sulfoxide ;  2 h, 100 °C
2.1 Reagents: Carbon dioxide Solvents: Acetonitrile ;  5 h, 1 atm, 60 °C
2.2 Reagents: Sodium chlorite Solvents: Water ;  20 min, 60 °C; 2.5 h, 60 °C
2.3 Reagents: Sodium sulfite Solvents: Water

Reference

A Facile Oxidation of Tertiary Amines to Lactams by Using Sodium Chlorite: Process Improvement by Precise pH Adjustment with CO2

Liu, Chaoyang; et al, Synlett, 2022, 33(10), 993-997

4-(3-Nitrophenyl)-3-morpholinone Raw materials

• 4-(3-Nitrophenyl)morpholine
• 1-fluoro-3-nitro-benzene

4-(3-Nitrophenyl)-3-morpholinone Preparation Products

• 4-(3-Nitrophenyl)-3-morpholinone (845729-43-3)

• 1. Enantio- & chemo-selective preparation of enantiomerically enriched aliphatic nitro alcohols using Candida parapsilosis ATCC 7330
  Sowmyalakshmi Venkataraman RSC Adv., 2015,5, 73807-73813
• 2. Fast synthesis of red Li3BaSrLn3(WO4)8:Eu3+ phosphors for white LEDs under near-UV excitation by a microwave-assisted solid state reaction method and photoluminescence studies
  Bo Wei,Zhenyu Liu,Chen Xie,Shu Yang,Wentao Tang,Aiwei Gu,Wing-Tak Wong,Ka-Leung Wong J. Mater. Chem. C, 2015,3, 12322-12327
• 3. Estimates of hydride ion stability in condensed systems: energy of formation and solvation in aqueous and polar-organic solvents
  Craig A. Kelly,David R. Rosseinsky Phys. Chem. Chem. Phys., 2001,3, 2086-2090
• 4. Fc microparticles can modulate the physical extent and magnitude of complement activity?
  David White,Sean R. Stowell Biomater. Sci., 2017,5, 463-474
• 5. Evolution in surface coverage of CH3NH3PbI3?XClXvia heat assisted solvent vapour treatment and their effects on photovoltaic performance of devices
  Dhirendra K. Chaudhary,Pramendra Kumar,Lokendra Kumar RSC Adv., 2016,6, 94731-94738

• Solvents and Organic Chemicals Organic Compounds Organoheterocyclic compounds Oxazinanes Phenylmorpholines
• Solvents and Organic Chemicals Organic Compounds Organoheterocyclic compounds Oxazinanes Morpholines Phenylmorpholines

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