Production Method 1

4664-13-5

83791-90-6

Reaction Conditions

1.1 Reagents: Phosphorus oxychloride Solvents: N,N-Diethylaniline ;  2 h, 90 - 95 °C
1.2 Reagents: Sodium hydroxide Solvents: Hexane ,  Water ;  pH 2.5

Reference

Regioselective Addition of Mesitol to a 2,4-Dichloropyridine

Ruggeri, Sally Gut; et al, Organic Process Research & Development, 2008, 12(3), 411-413

2,4-Dichloro-3,6-dimethylpyridine Raw materials

• 4-hydroxy-3,6-dimethyl-1,2-dihydropyridin-2-one

2,4-Dichloro-3,6-dimethylpyridine Preparation Products

• 2,4-Dichloro-3,6-dimethylpyridine (83791-90-6)

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• Solvents and Organic Chemicals Organic Compounds Organoheterocyclic compounds Pyridines and derivatives Halopyridines Polyhalopyridines

• 332062-08-5(Fmoc-S-3-amino-4,4-diphenyl-butyric acid)
• 1270529-38-8(1,2,3,4,5,6-Hexahydro-[2,3]bipyridinyl-6-ol)
• 2680771-01-9(4-cyclopentyl-3-{(prop-2-en-1-yloxy)carbonylamino}butanoic acid)
• 2098070-20-1(2-(3-(Pyridin-3-yl)-1H-pyrazol-1-yl)acetimidamide)
• 1444113-98-7(N-(3-cyanothiolan-3-yl)-2-[(2,2,2-trifluoroethyl)sulfanyl]pyridine-4-carboxamide)
• 941977-17-9(N'-(3-chloro-2-methylphenyl)-N-2-(dimethylamino)-2-(naphthalen-1-yl)ethylethanediamide)
• 2138166-62-6(2,2-Difluoro-3-[methyl(2-methylbutyl)amino]propanoic acid)
• 89640-58-4(2-Iodo-4-nitrophenylhydrazine)
• 1449132-38-0(3-Fluoro-5-(2-fluoro-5-methylbenzylcarbamoyl)benzeneboronic acid)
• 2034271-14-0(2-(1H-indol-3-yl)-N-{[6-(thiophen-2-yl)-[1,2,4]triazolo[4,3-b]pyridazin-3-yl]methyl}acetamide)