Production Method 1

1216499-22-7

83732-68-7

Reaction Conditions

1.1 Reagents: Sodium nitrite ,  Hydrochloric acid Solvents: Water ;  30 min, -5 °C; 15 min, -5 °C
1.2 Reagents: Cuprous chloride ;  30 min, -5 °C; 16 h, rt
1.3 Reagents: Ammonia Solvents: Water ;  10 °C

Reference

Development of a safe and scalable route towards a tau PET tracer precursor

Bartels, Bjoern; et al, Bioorganic & Medicinal Chemistry, 2018, 26(4), 970-976

2,3-Dichloro-6-methoxypyridine Raw materials

• 2-Chloro-6-methoxypyridin-3-amine hydrochloride

2,3-Dichloro-6-methoxypyridine Preparation Products

• 2,3-Dichloro-6-methoxypyridine (83732-68-7)

• 1. Excellent mechanical performance and enhanced dielectric properties of OBC/SiO2 elastomeric nanocomposites: effect of dispersion of the SiO2 nanoparticles?
  Xing Zhao,Lu Bai,Rui-Ying Bao,Zheng-Ying Liu,Ming-Bo Yang,Wei Yang RSC Adv., 2017,7, 46297-46305
• 2. Evolution of shape, size, and areal density of a single plane of Si nanocrystals embedded in SiO2 matrix studied by atom probe tomography
  Bin Han,Yasuo Shimizu,Gabriele Seguini,Celia Castro,Gérard Ben Assayag,Koji Inoue,Yasuyoshi Nagai,Sylvie Schamm-Chardon,Michele Perego RSC Adv., 2016,6, 3617-3622
• 3. Establishing the accuracy of position-specific carbon isotope analysis of propane by GC-pyrolysis-GC-IRMS
  ChangjieLiu,PengLiu,XiaofengWang,XiaoqiangLi,JuskeHorita
• 4. Fatty acid positional distribution in colostrum and mature milk of women living in Inner Mongolia, North Jiangsu and Guangxi of China?
  Long Deng,Qian Zou,Biao Liu,Wenhui Ye,Chengfei Zhuo,Li Chen,Ze-Yuan Deng,Ya-Wei Fan,Jing Li Food Funct., 2018,9, 4234-4245
• 5. Excess electrons in lithium–ethylamine solutions—density, electrical conductivity and EPR studies
  Phys. Chem. Chem. Phys., 1999,1, 3561-3565

• Solvents and Organic Chemicals Organic Compounds Organoheterocyclic compounds Pyridines and derivatives Halopyridines Polyhalopyridines

• 59023-23-3(2,3,7,8-Tetrachloro-1,4dioxino2,3-b:5,6-b'dipyridine)
• 31557-34-3(Pyridine,2,3,5-trichloro-6-methoxy-)
• 688047-08-7(4,5-Dichloro-2-methoxy-pyridine)
• 10469-13-3(Pyridine, 2,3,5-trichloro-4,6-dimethoxy-)
• 1227572-43-1(2,4-Dichloro-6-methoxypyridine)
• 17228-64-7(2-Chloro-6-methoxypyridine)
• 13473-01-3(5-Chloro-2-methoxypyridine)
• 10163-32-3(Ethanol, 2-[(3,5,6-trichloro-2-pyridinyl)oxy]-)
• 55933-90-9(Pyridine, 2,3,5-trichloro-6-ethoxy-)
• 64557-47-7(PHENOL, 4-[(3,5,6-TRICHLORO-2-PYRIDINYL)OXY]-)