Production Method 1

146743-72-8

817-11-8

Reaction Conditions

1.1 Reagents: Trifluoroacetic acid Solvents: Dichloromethane ;  36 h, rt

Reference

Synthesis of Poly(amino)ester Dendrimers via Active Cyanomethyl Ester Intermediates

Bouillon, Camille; Tintaru, Aura; Monnier, Valerie; Charles, Laurence; Quelever, Gilles; et al, Journal of Organic Chemistry, 2010, 75(24), 8685-8688

Production Method 2

817-11-8

Reaction Conditions

1.1 Reagents: Ammonium hydroxide Solvents: Water ;  0 °C; 30 min, 0 °C; 0 °C → rt; 40 min, rt → reflux; > 1 h, reflux

Reference

The Novel Synthesis of La0.8Sr0.2MnO3 Using the Michael-Addition Directed Hydrogelation of Acrylates for Materials Synthesis (MADHAMS) Method

Walker, Edwin H. Jr.; Apblett, Allen W.; Walker, Ron; Zachary, Adam, Chemistry of Materials, 2004, 16(25), 5336-5343

Production Method 3

2664-61-1

817-11-8

Reaction Conditions

1.1 Reagents: Sodium hydroxide

Reference

General method for the synthesis of trishydroxamic acids

Karunaratne, V.; Hoveyda, H. R.; Orvig, C., Tetrahedron Letters, 1992, 33(14), 1827-30

Production Method 4

146743-72-8

817-11-8

Reaction Conditions

1.1 Reagents: Acetyl chloride Solvents: Dichloromethane ,  Water ;  6 h, rt

Reference

Synthesis and biological evaluation of 3-amino-propan-1-ol based poly(ether imine) dendrimers

Krishna, Thatavarathy Rama; Jain, Samta; Tatu, Utpal S.; Jayaraman, Narayanaswamy, Tetrahedron, 2005, 61(17), 4281-4288

Production Method 5

146743-72-8

817-11-8

Reaction Conditions

1.1 Reagents: Trifluoroacetic acid Solvents: Dichloromethane ;  rt; 24 h, rt

Reference

Synthesis of poly(aminoester) dendrimers via 'click' chemistry in combination with the divergent and convergent strategies

Moreno, Pierre ; Quelever, Gilles; Peng, Ling, Tetrahedron Letters, 2015, 56(26), 4043-4046

Production Method 6

107-94-8

817-11-8

Reaction Conditions

1.1 Reagents: Ammonium chloride Catalysts: Sodium hydroxide Solvents: Water

Reference

Synthesis and study of the structure of anionic forms of nitrilotris(propionic acid) by IR and proton NMR spectroscopy

Zhadanov, B. V.; Tsirul'mikova, N. V.; Polyakova, I. A.; Egorushkina, N. A.; Kaslina, N. A.; et al, Zhurnal Obshchei Khimii, 1985, 55(5), 1149-54

Production Method 7

75-12-7

817-11-8

Reaction Conditions

1.1 Solvents: Isopropanol ;  8 h, 120 °C

Reference

New Synthesis of 3,3',3"-Nitrilotripropionic Acid

Lisin, A. V.; Akhmadullin, R. M.; Akhmadullina, A. G.; Spiridonova, R. R., Russian Journal of Organic Chemistry, 2021, 57(6), 1006-1008

Nitrilotripropionic Acid Raw materials

• β-Alanine, N,N-bis[3-(1,1-dimethylethoxy)-3-oxopropyl]-, 1,1-dimethylethyl ester
• Formamide
• 3-Chloropropanoic acid
• Propanamide, 3,3',3''-nitrilotris-

Nitrilotripropionic Acid Preparation Products

• Nitrilotripropionic Acid (817-11-8)

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• Solvents and Organic Chemicals Organic Compounds Organic acids and derivatives Carboxylic acids and derivatives Tricarboxylic acids and derivatives

• 160844-41-7(b-Alanine,N-(2-aminoethyl)-N-methyl-)
• 57724-25-1(N,N-dipropyl-beta-alanine)
• 6300-04-5(N,N-Dimethyl-beta-alanine)
• 90255-97-3(Ethanaminium, 2-carboxy-N,N,N-trimethyl-, hydroxide (1:1))
• 6458-06-6(2-(dimethylamino)-2-methylpropanoic acid)
• 6972-41-4(b-Alanine, N,N-diethyl-)
• 25741-05-3(1-Aziridinepropanoicacid)
• 15674-67-6(3-(diethylamino)propanoic acid;hydrochloride)
• 244190-31-6(3-Isopropyl(methyl)aminopropanoic acid hydrochloride)
• 13311-39-2(b-Alanine,N,N'-1,2-ethanediylbis[N-(2-carboxyethyl)-)